RU2558042C2 - Высокочувствительный способ определения количества компонентов, полученных из лекарственных трав - Google Patents
Высокочувствительный способ определения количества компонентов, полученных из лекарственных трав Download PDFInfo
- Publication number
- RU2558042C2 RU2558042C2 RU2013125221/15A RU2013125221A RU2558042C2 RU 2558042 C2 RU2558042 C2 RU 2558042C2 RU 2013125221/15 A RU2013125221/15 A RU 2013125221/15A RU 2013125221 A RU2013125221 A RU 2013125221A RU 2558042 C2 RU2558042 C2 RU 2558042C2
- Authority
- RU
- Russia
- Prior art keywords
- blood plasma
- methanol
- acid
- solid phase
- concentration
- Prior art date
Links
Images
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/48—Biological material, e.g. blood, urine; Haemocytometers
- G01N33/50—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/48—Biological material, e.g. blood, urine; Haemocytometers
- G01N33/50—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing
- G01N33/94—Chemical analysis of biological material, e.g. blood, urine; Testing involving biospecific ligand binding methods; Immunological testing involving narcotics or drugs or pharmaceuticals, neurotransmitters or associated receptors
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N2560/00—Chemical aspects of mass spectrometric analysis of biological material
Landscapes
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Molecular Biology (AREA)
- Urology & Nephrology (AREA)
- Hematology (AREA)
- Biomedical Technology (AREA)
- Chemical & Material Sciences (AREA)
- Immunology (AREA)
- Medicinal Chemistry (AREA)
- Physics & Mathematics (AREA)
- Microbiology (AREA)
- Pathology (AREA)
- Biotechnology (AREA)
- Food Science & Technology (AREA)
- General Physics & Mathematics (AREA)
- Cell Biology (AREA)
- Analytical Chemistry (AREA)
- Biochemistry (AREA)
- General Health & Medical Sciences (AREA)
- Pharmacology & Pharmacy (AREA)
- Bioinformatics & Cheminformatics (AREA)
- Other Investigation Or Analysis Of Materials By Electrical Means (AREA)
- Investigating Or Analysing Biological Materials (AREA)
- Investigating Or Analyzing Non-Biological Materials By The Use Of Chemical Means (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2010-256187 | 2010-11-16 | ||
| JP2010256187A JP5193266B2 (ja) | 2010-11-16 | 2010-11-16 | 生薬由来成分の高感度定量方法 |
| PCT/JP2011/076248 WO2012067090A1 (ja) | 2010-11-16 | 2011-11-15 | 生薬由来成分の高感度定量方法 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| RU2013125221A RU2013125221A (ru) | 2014-12-10 |
| RU2558042C2 true RU2558042C2 (ru) | 2015-07-27 |
Family
ID=46084017
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2013125221/15A RU2558042C2 (ru) | 2010-11-16 | 2011-11-15 | Высокочувствительный способ определения количества компонентов, полученных из лекарственных трав |
Country Status (5)
| Country | Link |
|---|---|
| JP (1) | JP5193266B2 (enExample) |
| KR (1) | KR101476144B1 (enExample) |
| CN (1) | CN103210308B (enExample) |
| RU (1) | RU2558042C2 (enExample) |
| WO (1) | WO2012067090A1 (enExample) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2603363C1 (ru) * | 2015-09-23 | 2016-11-27 | федеральное государственное бюджетное образовательное учреждение высшего образования "Новосибирский государственный медицинский университет" Министерства здравоохранения Российской Федерации (ФГБОУ ВО НГМУ Минздрава России) | Вольтамперометрический способ количественного определения глицирризиновой кислоты в фармацевтических субстанциях |
| RU2700831C1 (ru) * | 2019-01-24 | 2019-09-23 | Федеральное государственное бюджетное учреждение "Научный центр экспертизы средств медицинского применения" Министерства здравоохранения Российской Федерации (ФГБУ "НЦЭСМП" Минздрава России) | Способ количественного определения глицина в биологических лекарственных препаратах методом гидрофильной высокоэффективной жидкостной хроматографии |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR102617148B1 (ko) * | 2016-08-15 | 2023-12-26 | 제넨테크, 인크. | 비이온성 계면활성제 및 폴리펩티드를 포함하는 조성물에서 비이온성 계면활성제를 정량화하기 위한 크로마토그래피 방법 |
| CN107064327A (zh) * | 2016-12-23 | 2017-08-18 | 东北制药集团沈阳第制药有限公司 | 一种检测复方甘草片中吗啡和甘草酸含量的方法 |
| JP7019372B2 (ja) * | 2017-10-19 | 2022-02-15 | 株式会社あすか製薬メディカル | ビタミンd代謝物の選択的測定法 |
| JP7479633B2 (ja) | 2020-12-03 | 2024-05-09 | 株式会社ツムラ | アンバムの分析方法 |
| CN113984916B (zh) * | 2021-09-28 | 2024-04-19 | 天津中医药大学第一附属医院 | 一种正髓丸及正髓丸药材含量测定方法 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5325675B2 (enExample) * | 1973-12-14 | 1978-07-28 | ||
| JPS5251995A (en) * | 1975-10-23 | 1977-04-26 | Rooto Seiyaku Kk | Method of analyzing clycyrrhizin |
| US20050148088A1 (en) * | 2002-04-19 | 2005-07-07 | Eng Shi Ong | Pressurized hot water extraction |
| KR20040099885A (ko) * | 2003-05-20 | 2004-12-02 | 한국과학기술연구원 | 가미자도환의 주요성분 동시 분석방법 |
| WO2008109632A1 (en) * | 2007-03-07 | 2008-09-12 | Sanofi-Aventis U.S. Llc | The quantitative determination of risedronate in urine by spe-lc-ms-ms |
| CN101216465B (zh) * | 2007-12-28 | 2011-01-12 | 北京联合大学生物化学工程学院 | 甘草药材指纹图谱的建立方法及其标准指纹图谱 |
| CN101532994B (zh) * | 2009-04-18 | 2013-02-27 | 姚俊华 | 健脑补肾制剂的含量测定方法 |
| CN101897680A (zh) * | 2009-06-01 | 2010-12-01 | 天津药物研究院 | 液体胶囊制剂、其制备方法及用途 |
-
2010
- 2010-11-16 JP JP2010256187A patent/JP5193266B2/ja active Active
-
2011
- 2011-11-15 CN CN201180054812.9A patent/CN103210308B/zh active Active
- 2011-11-15 WO PCT/JP2011/076248 patent/WO2012067090A1/ja not_active Ceased
- 2011-11-15 KR KR1020137012465A patent/KR101476144B1/ko active Active
- 2011-11-15 RU RU2013125221/15A patent/RU2558042C2/ru active
Non-Patent Citations (1)
| Title |
|---|
| Sakamaki N. Et al. simultaneous determination of stevioside, rebaudioside A and glycyrrhizic acid in foods by HPLC. Перечень данных [он-лайн] fghtkm 2004 [Найдено 06.07.2014] " найдено из Интернет: URL: http://www.ncbi.nlm.nih.gov/pubmed/15272605. О.Б. РУДАКОВ и др. Физико-химические системы сорбат-сорбент-элюент в жидкостной хроматографии. - Воронеж, 2003. С.29-39. Руководство по методам контроля качества и безопастности биологически активных добавок к пище. - М.: Федеральный центр Госсанэпиднадзора Минздрава России, 2004. С.141-142 * |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| RU2603363C1 (ru) * | 2015-09-23 | 2016-11-27 | федеральное государственное бюджетное образовательное учреждение высшего образования "Новосибирский государственный медицинский университет" Министерства здравоохранения Российской Федерации (ФГБОУ ВО НГМУ Минздрава России) | Вольтамперометрический способ количественного определения глицирризиновой кислоты в фармацевтических субстанциях |
| RU2700831C1 (ru) * | 2019-01-24 | 2019-09-23 | Федеральное государственное бюджетное учреждение "Научный центр экспертизы средств медицинского применения" Министерства здравоохранения Российской Федерации (ФГБУ "НЦЭСМП" Минздрава России) | Способ количественного определения глицина в биологических лекарственных препаратах методом гидрофильной высокоэффективной жидкостной хроматографии |
Also Published As
| Publication number | Publication date |
|---|---|
| KR20130076892A (ko) | 2013-07-08 |
| WO2012067090A1 (ja) | 2012-05-24 |
| KR101476144B1 (ko) | 2014-12-24 |
| JP2012107954A (ja) | 2012-06-07 |
| CN103210308A (zh) | 2013-07-17 |
| CN103210308B (zh) | 2015-01-07 |
| JP5193266B2 (ja) | 2013-05-08 |
| RU2013125221A (ru) | 2014-12-10 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| RU2558042C2 (ru) | Высокочувствительный способ определения количества компонентов, полученных из лекарственных трав | |
| JP6736591B2 (ja) | 液体クロマトグラフィー質量分析による体液中のアミノ酸分析 | |
| Busardò et al. | Ultra-high performance liquid chromatography tandem mass spectrometry (UHPLC–MS/MS) for determination of GHB, precursors and metabolites in different specimens: application to clinical and forensic cases | |
| Kubica et al. | Modern approach for determination of lactulose, mannitol and sucrose in human urine using HPLC–MS/MS for the studies of intestinal and upper digestive tract permeability | |
| Huang et al. | Pharmacokinetics and tissue distribution of five bufadienolides from the Shexiang Baoxin pill following oral administration to mice | |
| Klepacki et al. | Amino acids in a targeted versus a non-targeted metabolomics LC-MS/MS assay. Are the results consistent? | |
| Chang et al. | Simultaneous determination of four phenolic acids and seven alkaloids in rat plasma after oral administration of traditional Chinese medicinal preparation Jinqi Jiangtang Tablet by LC-ESI–MS/MS | |
| Zhang et al. | Determination of 25-OH-PPD in rat plasma by high-performance liquid chromatography–mass spectrometry and its application in rat pharmacokinetic studies | |
| Skillman et al. | Identification of suvorexant in blood using lc–ms-ms: Important considerations for matrix effects and quantitative interferences in targeted assays | |
| Surendran et al. | A LC-MS/MS method for simultaneous estimation of a novel anti-diabetic combination of saxagliptin and dapagliflozin using a polarity switch approach: application to in vivo rat pharmacokinetic study | |
| Dai et al. | Comparative pharmacokinetics of acteoside from total glycoside extracted from leaves of Rehmannia and Dihuangye total glycoside capsule in normal and diabetic nephropathy rats | |
| Tettey-Amlalo et al. | Rapid UPLC–MS/MS method for the determination of ketoprofen in human dermal microdialysis samples | |
| Schleiff et al. | An isocratic HPLC-UV analytical procedure for assessment of glutathione and its related substances | |
| Park et al. | Validated LC‐MS/MS method for quantification of gabapentin in human plasma: application to pharmacokinetic and bioequivalence studies in Korean volunteers | |
| JP7753359B2 (ja) | ヒト血漿中のリゼルギン酸ジエチルアミド(lsd)及び2,3-ジヒドロ-3-ヒドロキシ-2-オキソリセルギド(o-h-lsd)を定量化するための方法 | |
| Kim et al. | Pharmacokinetics, tissue distribution, and tentative metabolite identification of sauchinone in mice by microsampling and HPLC-MS/MS methods | |
| Wen et al. | LC-MS/MS-based method for simultaneous quantification of known chemicals and metabolites of Alpiniae oxyphyllae Fructus extract in rat plasma and its application in a pharmacokinetic study | |
| RU2705363C1 (ru) | Способ определения лекарственного препарата метформин в смешанной слюне пациента, страдающего сахарным диабетом | |
| Zhu et al. | Pharmacokinetics and bioavailability study of two ondansetron oral soluble film formulations in fasting healthy male Chinese volunteers | |
| Yaroshenko et al. | Chromatographic determination of sildenafil in blood plasma using spectrophotometric and mass-spectrometric detection | |
| Arafat et al. | Determination of loperamide in human plasma and saliva by liquid chromatography–tandem mass spectrometry | |
| Pan et al. | Simultaneous determination of forsythin and its major metabolites in human plasma via liquid chromatography-tandem mass spectrometry | |
| Zhang et al. | Quantitative analysis of biomarkers of liver and kidney injury in serum and urine using ultra‐fast liquid chromatography with tandem mass spectrometry coupled with a hydrophilic interaction chromatography column: Application to monitor injury induced by Euphorbiae pekinensis Radix | |
| Park et al. | Rapid quantification of levosulpiride in human plasma using RP‐HPLC‐MS/MS for pharmacokinetic and bioequivalence study | |
| WO2014126207A1 (ja) | 試料中の有機酸の検出方法 |