RU2177031C1 - Method of vodka production - Google Patents

Abstract

FIELD: alcoholic beverage industry, particularly, production of "Velikaya Rossiya" vodka. SUBSTANCE: Mixing of alcohol and water is carried out in mixer with the following additional mixing in centrifugal pump. Flows of alcohol and water are simultaneously entered the mixer wherever high turbulence is created due to counter motion of flows. It provides for favorable hydrodynamic conditions for mixing and dissolving alcohol in water. Prepared aqueous-alcoholic solution escapes from mixer with knowingly increased content of alcohol by 0.5-1.5%. For preparing standard strength of aqueous-alcoholic solution, additional flow of water is introduced in pipeline connected mixer with centrifugal pump. Said solution is directed to carbon-cleaning battery consisting of three series-connected columns-adsorbers for processing with activated carbon under conditions of pseudoboiling layer. Aqueous-alcoholic solution is fed by pump from the last column-adsorber to hydraulic cyclone where large carbon particles are separated. Then vodka is directed to filtering installations consisting of frame flannel filters (filters of preliminary coarse filtering) and filters of final (fine) filtering with hydraulically compressed layer of quartz sand with grain size of 200-500 mcm. Cloudberry stems infusion is prepared by one-time infusion in aqueous-alcoholic liquid. Infusion of cloudberry stems, xylitol preliminarily dissolved in some quantity of softened water, sugar in the form of sugar syrup with 65.8% concentration preliminarily filtered are introduced in vodka in finishing tank. Content of tank is thoroughly mixed after introduction of each ingredient, corrected, if necessary, and directed for bottling with obligatory control filtration. Prepared vodka "Velikaya Rossiya" contains the following ingredients per 1000 dal: xylitol, 1.8-2.2 kg; infusion of the Ist decantation of cloudberry stems, 1-2 l; 65.8% sugar syrup, 8-8.1 l; ethyl rectified alcohol "Extra" and potable corrected water, the balance, up to 40% strength. EFFECT: broadened assortment of vodkas with treatment-and-prophylactic properties in case of diabetes; higher biological value of vodka due to synergistic interaction of ingredients and methods of production. 3 cl, 1 tbl, 3 ex

Description

 The invention relates to the distillery industry and can be used in the production of vodka "GREAT RUSSIA".

 A known method for the production of vodka, providing for the preparation of sorting of rectified ethyl alcohol "Lux" and drinking corrected water, filtering the sorting through activated carbon, introducing fructose, xylitol and tartaric acid in the form of aqueous solutions into the vat, filtering the blend and bottling (RF, patent, 2130058, CL C 12 G 3/06, 1999).

 The disadvantage of this method is its high cost.

 The introduction of xylitol in combination with aromatic alcohol of kvass wort concentrate and sugar syrup is known (RF, patent 2034019, class C 12 G 3/06, 1995).

 A disadvantage of the known vodka is its insufficiently high organoleptic characteristics.

 Closest to the proposed method is the production of vodka, which involves the preparation of a hydroalcoholic liquid from rectified ethyl alcohol "Extra" and corrected drinking water, mixing sorting, cleaning through a coal-cleaning battery, introducing a solution of honey, sugar and infusion of cloudberry stalks into a litter vat 1 draining, checking and adjusting the fortress, control filtration and bottling (RF patent 2142004, class C 12 G 3/06, 1999).

 And although the well-known vodka is enriched with a complex of biologically active substances of cloudberries and honey, the presence of sugar and honey in it does not allow the use of vodka for therapeutic and preventive purposes for patients with diabetes.

 The problem solved by the invention is to replace part of the sugar with xylitol and, while maintaining the high biological value of vodka, use it for therapeutic and preventive purposes.

 The technical result is the expansion of the range of vodkas with therapeutic and prophylactic properties for diabetes and the preservation of high biological value.

The problem and the technical result are achieved in the method of producing vodka, which provides for the preparation of a water-alcohol mixture from rectified ethyl alcohol “Extra” and drinking corrected water, purifying it in a coal-cleaning battery, filtering, introducing sugar in the form of sugar syrup with a concentration of 65.8% - in the finishing vat, as well as introducing into the finishing vodka 1 discharge of cloudberry stalks, pre-filtered, final filtration and bottling, in addition to that with sugar syrup concentration of 65, Xylitol, previously dissolved in corrected drinking water, is introduced into the liqueur vat with 8% and the infusions of cloudberry stalks, preliminary filtering of each introduced ingredient and mixing after introduction into the liqueur vat, and the ingredients included in vodka are used in the following ratio, per 1000 gave:
Xylitol, kg - 1.8 - 2.2
Infusion 1 plum of cloudberry stalks, l - 1 - 2
Sugar syrup 65.8%, l - 8 - 8.1
Rectified ethyl alcohol "Extra" and corrected drinking water - The rest is 40% to the fortress
It is advisable to prepare the water-alcohol mixture in two successive stages under turbulization conditions with countercurrent movement of the flows of alcohol and drinking water corrected, while in the first stage the sources are mixed in the mixer to the sorting strength by 0.5-1.5% higher than the standard one, and by the second is adjusted to standard in a centrifugal pump with an additional stream of corrected water.

 It is recommended that filtering after cleaning the sorting through a coal-cleaning battery be carried out in three successive stages, the first of which separates large particles of coal on a hydrocyclone, the second - pre-cleaning on frame flannel filters, and the third - fine filtering through a hydrated compressed filter layer of silica sand with a grain size of 200-500 microns.

 The production method of vodka "GREAT RUSSIA" is as follows.

 The mixing of alcohol and water is carried out in a mixer, followed by additional mixing in a centrifugal pump.

 Streams of alcohol and water flow simultaneously into the mixer. There, as a result of the oncoming movement of the jets, high turbulence is created, which provides favorable hydrodynamic conditions for the mixing and dissolution of alcohol in water.

 The resulting water-alcohol solution leaves the mixer with a deliberately increased alcohol content of 0.5-1.5%. The water-alcohol solution is brought to the standard strength by introducing an additional stream of water into the pipeline connecting the mixer to the centrifugal pump.

 The resulting sorting is sent to a coal-cleaning battery consisting of 3 series-connected adsorber columns for treating with active carbon in a pseudo-boiling layer. From the last adsorber column, a water-alcohol solution is pumped into a hydrocyclone, where large coal particles are separated. Next, the vodka goes to filtration units, consisting of frame flannel filters (pre-filters) and final (fine) filters with a hydraulically compressed filter layer of quartz sand with a grain size of 200-500 microns.

 Cloudberry stalk infusion is prepared by a single infusion in an aqueous-alcoholic liquid.

 The infusion of cloudberry stalks, xylitol, previously dissolved in a small amount of softened water, sugar in the form of sugar syrup with a concentration of 65.8%, pre-filtered, is introduced into the vodka located in the finishing vat.

 The contents of the tub are thoroughly mixed after each ingredient is added, if necessary, adjusted and sent to the bottling with the obligatory control filtering.

Ready-made vodka "GREAT RUSSIA" contains the following ingredients per 1000 dal:
Xylitol, kg - 1.8 - 2.2
Infusion 1 plum of cloudberry stalks, l - 1 - 2
Sugar syrup 65.8%, l - 8 - 8.1
Rectified ethyl alcohol "Extra" and corrected drinking water - The rest is 40% to the fortress
Example 1. Mixing rectified ethyl alcohol "Extra" and drinking water corrected with a hardness of up to 0.2 mol / m ^{3 is} carried out in two stages: first in a mixer, and then in a centrifugal pump when the jets move counter-clockwise under turbulence conditions with a volume ratio of alcohol flows and water equal to 1: 1.38-1.44.

 The resulting water-alcohol solution leaves the mixer with a deliberately increased alcohol content of 0.5%. A water-alcohol solution is brought to a standard strength by introducing an additional stream of water into the pipeline connecting the mixer to the centrifugal pump.

 The resulting sorting is sent to a coal-cleaning battery consisting of 3 series-connected adsorber columns for treating with active carbon in a pseudo-boiling layer.

 The intensity of the source of sorting when loading activated carbon into an adsorber column in an amount of 110 kg is 4.5 l / (m • s).

 From the last adsorber column, a water-alcohol solution is pumped into a hydrocyclone, where large coal particles are separated. Next, vodka goes to filtration plants, consisting of frame flannel filters (filters with a preliminary cleaning pipe) and final (fine) filters with a hydraulically compressed filter layer of silica sand with a grain size of 200 microns.

 Technological parameters for obtaining the infusion of cloudberry stalks are given in the table.

 The infusion of cloudberry stalks, xylitol, previously dissolved in a small amount of softened water, sugar in the form of sugar syrup with a concentration of 65.8%, pre-filtered, is introduced into the vodka located in the finishing vat.

 The contents of the vat are thoroughly mixed after each ingredient is added, and sent for bottling with mandatory control filtration.

The following ingredients are used per 1000 dal of vodka:
Xylitol, kg - 2.0
Infusion 1 plum of cloudberry stalks, l - 1.5
Sugar syrup, l - 8.05
Rectified ethyl alcohol "Extra" and corrected drinking water - The rest is 40% to the fortress
Example 2. The method of production of vodka "GREAT RUSSIA" is carried out according to example 1. In the first stage, the strength of the water-alcohol solution is 41.5%. In the third stage, the final filtration is carried out through a layer of silica sand with a grain size of 500 μm. The ratio of ingredients per 1000 gave vodka is as follows:
Xylitol, kg - 1.8
Infusion 1 plum of cloudberry stalks, l - 1.0
65.8% sugar syrup - 8.0
Rectified ethyl alcohol "Extra and corrected drinking water - Else 40% to the fortress
Example 3. The production method of vodka "GREAT RUSSIA" is carried out according to example 1, but the ratio of ingredients per 1000 gave vodka the following:
Xylitol, kg - 2.2
Infusion 1 plum of cloudberry stalks, l - 2.0
Sugar syrup 65.8% - 8.1
Rectified ethyl alcohol "Extra" and corrected drinking water - The rest is 40% to the fortress
The proposed method allows to obtain vodka with therapeutic and prophylactic properties and preserve its biological value through the joint use of the ingredients included in it, and the methods of the method, which, exhibiting a synergistic effect, not only enrich it with a complex of biologically active substances of the widest spectrum of action contained in cloudberry stalks (glucose, fructose, carotene, pectin, tannins, malic, citric and ascorbic acids and others), but also accelerates the assimilation of xylitol in water-alcohol commercial environment, as well as somewhat ennoble its too sweet-sugary taste.

 Vodka "GREAT RUSSIA" expands the range of vodkas with therapeutic and prophylactic effect and the range of vodka fighters, as diabetics can use it.

Claims (2)

1. A method for the production of vodka, involving the preparation of sorting by mixing rectified ethyl alcohol “Extra” and drinking corrected water, purifying it in a coal-cleaning battery, filtering, introducing 1 plum of cloudberry stalks, which are pre-filtered, and 65.8% sugar syrup, final filtration and bottling, characterized in that xylitol, previously dissolved in corrected drinking water and filtered, is added to the liqueur vat, and sugar syrup before being introduced it is also filtered into the liqueur vat, while after introducing into the liqueur vat each ingredient is mixed in the following quantitative ratio of the ingredients introduced into vodka per 1000 gave the finished product:
Xylitol, kg - 1.8-2.2
Infusion 1 plum of cloudberry stalks, l - 1-2
Sugar syrup 65.8%, l - 8-8.1
Rectified ethyl alcohol "Extra" and corrected drinking water - The rest is 40% to the fortress
2. The method according to claim 1, characterized in that the preparation of the water-alcohol mixture is carried out in two successive stages under turbulent flows with countercurrent stirring, mixing alcohol and water flows in the first stage until the sorting strength is 0.5-1, 5% higher than the standard, and on the second - adjusted to standard in a centrifugal pump by introducing an additional stream of water into it.  3. The method according to claim 1 or 2, characterized in that the filtering after cleaning sorting through a coal-cleaning battery is carried out in three successive stages, the first of which separates large particles of coal on a hydrocyclone, the second - preliminary cleaning on frame flannel filters, and on the third - the final fine cleaning through a hydraulic compressed filter layer of silica sand with a grain size of 200-500 microns.

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