RU2143485C1 - Method of vodka "kaznacheiskaya" production - Google Patents

Abstract

FIELD: liqueur and vodka industry. SUBSTANCE: water is softened and mixed with rectified ethyl alcohol "LUX". Succinic acid in the amount of 0.09-0.15 kg and sodium hydrocarbonate in the amount of 0.18-0.3 kg per 1000 dal are dissolved in softened water separately. Solutions are mixed, and mixture is kept for 30-40 min, filtered and filtrate is added to aqueous-alcoholic liquid. The latter is purified with activated carbon and fed into finishing tank where fructose solution is added in the amount of 2.8-3.2 kg per 1000 dal. Ready vodka is stirred, filtered finally and fed to pouring. Addition of components at indicated amounts at the definite stages of technological process, i. e. a mixture of succinic acid and sodium hydrocarbonate as kept filtrate at indicated ratio to an aqueous-alcoholic liquid and fructose to ready vodka promotes to decrease the content of organic compounds (fusel oil, methanol) that cause alcohol withdrawal syndrome. Obtained vodka has high organoleptic indices. EFFECT: improved quality, decreased cost, improved technology, broadened assortment of vodkas. 1 tbl, 3 ex

Description

 The invention relates to the alcoholic beverage industry.

 A known method of producing vodka, providing for the preparation of sorting of rectified ethyl alcohol "Extra" and drinking corrected water, filtering through a charcoal filter, introducing sugar and a solution of succinic acid into vodka in vodka and bottling (RU, patent 2064492, class C 12 G 3 / 06, 1996).

 Although the vodka obtained by the known method has a prophylactic effect on the human body in particularly difficult and extreme conditions, the presence of a large amount of sugar in it will increase the cost of sugar, increase the cost of the product, and the presence of only two components in the composition of vodka - sugar and succinic acid - gives originality in the taste and aroma of vodka.

 Widely known are methods of producing a wide variety of vodkas, where, in order to improve their performance, sodium bicarbonate is introduced into sorting (Recipes for alcoholic beverages and vodkas. Moscow, Light and Food Industry, 1981, p. 269). Sodium bicarbonate is introduced by known methods together with acetic acid until neutral. However, the resulting vodka have not high organoleptic characteristics.

 Closest to the proposed method is the production of vodka, which involves softening water, obtaining sorting by mixing softened water with rectified ethyl alcohol "LUX", introducing into the sorting glucose and fructose, which are previously dissolved in softened water and filtered, as well as the infusion of sprouted oat grains, treatment with activated carbon impregnated silver and filtration before bottling (RU, patent 2098474, class C 12 G 3/06, 1997).

 The disadvantage of this method is the complexity of its implementation, associated with the presence of activated carbon impregnated with silver, as well as the need for additional equipment for germinating grain sprouts, which complicates the technological process of production of vodka and increases its cost, and the introduction of fructose into sorting rather than into finished vodka, can lead to its losses during further processing, which will affect the organoleptic characteristics of vodka. The introduction of glucose along with fructose will also increase the cost of vodka.

 The technical result of the proposed method is to increase the manufacturability of the method while expanding the range of vodkas, reducing the cost of producing vodka, which allows to reduce the hangover syndrome.

This is achieved by the fact that the method of producing vodka, which involves the correction of drinking water, obtaining sorting by mixing the corrected water with rectified ethyl alcohol "LUX", introducing an aqueous solution of fructose, treating with active carbon and filtering, according to the invention, an aqueous solution of fructose is introduced into the finished vodka, and succinic acid and sodium bicarbonate in the ratio 1: 2, each of which is dissolved in corrected water before being added to the sorting and the solutions are mixed, kept for 30-40 minutes, fil they are consumed with the subsequent introduction of the filtrate, and the finished vodka has the following ratio of ingredients, kg per 1000 gave the finished product:
Succinic acid - 0.09 - 0.15
Fructose - 2.8 - 3.2
Sodium bicarbonate - 0.18 - 0.3
Rectified ethyl alcohol "Lux" and corrected drinking water - Else
It should be noted that the synergism of the methods of the method is as follows. When the filtrates of succinic acid and sodium bicarbonate are aged, these components are assimilated in water, and in the presence of sodium bicarbonate, the adaptogenic ability of succinic acid increases. When this mixture is added to the sorting, the selective effect of coal on various impurities is accelerated: aldehydes, esters, fusel oils, acids, and the esterification process is intensified, that is, the formation of aromatic esters and acetals.

 Fructose accelerates this process in the finished vodka, forms the final taste, and in the presence of the entire set of introduced ingredients, the content of methanol and fusel oils is reduced, and the finished vodka can reduce the hangover syndrome.

 The production method of vodka is as follows.

For the preparation of KAZNACHEYSKAYA vodka, they use:
- rectified ethyl alcohol "LUX" according to GOST 5962-67;
- drinking water according to GOST 2874-82 with a hardness of up to 1 mol / m ³ for natural un softened water and up to 0.2 mol / m ³ for recovered water;
- fructose, approved for use by the bodies of the State Sanitary and Epidemiological Supervision of the Russian Federation (Hygienic certificate N III-II / 773 of 06.29.95);
- succinic acid according to GOST 6341-75;
- sodium bicarbonate in accordance with GOST 2156-76;
- shredded activated charcoal grade BAU-A according to GOST 6217-74.

 Succinic acid and sodium bicarbonate are dissolved separately in fixed water, mixed, filtered, aged for 30-40 minutes and the filtrate is introduced into sorting.

 A water-alcohol solution (sorting) is prepared in such a way as to obtain vodka with a strength of 40%.

 The resulting sorting is thoroughly mixed, passed through a coal-cleaning battery with a filtration rate of up to 40 dal / h for fresh coal and up to 30 dal / h for regenerated. The resulting vodka is sent to a finishing vat.

 Fructose is dissolved in softened water in a ratio of 1: 1 and introduced into the finishing vat.

The finished vodka is mixed, corrected, if necessary, filtered and sent for bottling. Ready vodka has the following ratio of ingredients, kg per 1000 gave the finished product:
Succinic acid - 0.09 - 0.15
Fructose - 2.8 - 3.2
Sodium bicarbonate - 0.18 - 0.3
Rectified ethyl alcohol "Lux" and corrected drinking water - Else
Example 1-3. KAZNACHEYSKAYA vodka is obtained by the method described above, and the table shows the ingredients for all examples and the exposure time of a mixture of solutions of succinic acid and sodium bicarbonate, introduced into the sorting as a filtrate.

 The proposed method is technological, effective, improves the organoleptic characteristics of vodka and reduces its toxic properties, since the combination of the introduced ingredients promotes the formation of compounds that neutralize the influence of harmful organic impurities (methanol, fusel oils).

 The proposed method reduces the cost of vodka and expands the range of vodkas to reduce the hangover syndrome.

Claims (1)

A method of producing vodka, involving softening drinking water, obtaining sorting by mixing softened water with rectified ethyl alcohol "LUX", introducing an aqueous solution of fructose, treating with active carbon and filtering vodka, characterized in that the aqueous solution of fructose is introduced into the finished vodka before filtration, and in sorting, before treating it with activated carbon, succinic acid and sodium bicarbonate are set in a ratio of 1: 2 in the form of a mixture filtrate, which is obtained by dissolving each ingredient in softened water, mixing solutions, holding the mixture for 30-40 minutes and filtering it, while the finished vodka has the following ratio of ingredients, kg per 1000 gave the finished product:
Succinic acid - 0.09 - 0.15
Fructose - 2.8 - 3.2
Sodium bicarbonate - 0.18 - 0.3
Rectified ethyl alcohol "LUX" and corrected drinking water - Else

Images