RU2017113966A - Простые полиэфирамины на основе 1, 3-диспиртов - Google Patents

Простые полиэфирамины на основе 1, 3-диспиртов Download PDF

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RU2017113966A
RU2017113966A RU2017113966A RU2017113966A RU2017113966A RU 2017113966 A RU2017113966 A RU 2017113966A RU 2017113966 A RU2017113966 A RU 2017113966A RU 2017113966 A RU2017113966 A RU 2017113966A RU 2017113966 A RU2017113966 A RU 2017113966A
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formula
mixture
ethers
carbon atoms
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Зофиа ЭБЕРТ
Бьерн ЛУДОЛЬФ
Кристиан АЙДАМСХАУС
Стефано Сциалла
Кевин КРИСМАС
ВАУН Ами АЙХШТАДТ
Брайан Дж. ЛАФНЭЙН
Дарен РИЗ
Франк ХЮЛЬСКЕТТЕР
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Басф Се
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Claims (34)

1. Смесь простых эфираминов, содержащая по меньшей мере 90% массовых, в пересчете на общую массу этой смеси простых эфираминов, амина формулы (I) и/или (II),
Figure 00000001
Figure 00000002
в которых R1-R12 независимо друг от друга выбираются из H, алкила, цилокалкила, арила, алкиларила или арилалкила, причем по меньшей мере один из R1-R6 и по меньшей мере один из R7-R12 отличается от H,
причем A1-A9 независимо друг от друга выбираются из линейных или разветвленных алкиленов, имеющих от 2 до 18 атомов углерода, предпочтительно 2-10 атомов углерода, наиболее предпочтительно 2-5 атомов углерода,
причем Z1-Z4 независимо друг от друга выбираются из OH или CH2CH2CH2NH2, NH2, NHR' или NR'Rʺ, причем степень аминирования составляет <50%, причем R' и Rʺ независимо друг от друга выбираются из алкиленов, имеющих от 2 до 6 атомов углерода, и причем сумма x+y находится в диапазоне от 2 до 200, причем x≥1 и y≥1; и x1+y1 находится в диапазоне от 2 до 200, предпочтительно 2-20, наиболее предпочтительно 2-10, причем x1≥1 и y1≥1.
2. Смесь простых эфираминов по п. 1, причем эта смесь простых эфираминов содержит по меньшей мере 95% массовых, в пересчете на общую массу смеси простых эфираминов, амина формулы (I) и/или (II).
3. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) x+y находится в диапазоне от 2 до 20.
4. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) x+y находится в диапазоне от 3 до 20.
5. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) степень аминирования находится в диапазоне от 30% до <50%.
6. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) A1-A9 независимо друг от друга выбираются из группы, состоящей из этилена, пропилена или бутилена.
7. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) каждый из A1-A9 является пропиленом.
8. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) R1, R2, R5, R6, R7, R8, R11 и R12 представляют собой H, a R3, R4, R9 и R10 независимо друг от друга выбираются из алкила с 1-16 атомами углерода или арила.
9. Смесь простых эфираминов по п. 1, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) R1, R2, R5, R6, R7, R8, R11 и R12 представляют собой H, a R3, R4, R9 и R10 независимо друг от друга выбираются из бутильной группы, этильной группы, метильной группы, пропильной группы или фенильной группы.
10. Смесь простых эфираминов по любому из пп. 1-6, причем в вышеуказанном простом полиэфирамине формулы (I) или формулы (II) каждый из R3 и R9 является этильной группой, каждый из R1, R2, R5, R6, R7, R8, R11 и R12 представляет собой H, каждый из R4 и R10 представляет собой бутильную группу.
11. Смесь простых эфираминов по любому из пп. 1-9, причем простой полиэфирамин формулы (I) или формулы (II) имеет среднемассовую молекулярную массу примерно от 290 до примерно 1000 грамм/моль.
12. Смесь простых эфираминов по любому из пп. 1-9, причем простой полиэфирамин формулы (I) или формулы (II) является вступившим в реакцию с кислотой.
13. Способ получения смеси простых эфираминов, содержащей по меньшей мере 90% массовых, в пересчете на общую массу этой смеси простых эфираминов, простого эфирамина формулы (I) и/или (II), включающий следующие стадии:
а) взаимодействие 1,3-диола формулы (III) с алкиленоксидами с 2-18 атомами углерода, причем молярное соотношение 1,3-диола и алкиленоксидов с 2-18 атомами углерода находится в диапазоне от 1:2 до 1:10,
Figure 00000003
причем R1-R6 независимо друг от друга представляют собой H, алкил, циклоалкил, арил, алкиларил, арилалакил, и по меньшей мере одна группа, выбранная среди R1-R6, отличается от H, с последующим или
b1) аминированием алкоксилированных 1,3-диолов с помощью аммиака, или
b2) восстановительным цианоэтилированием алкоксилированных 1,3-диолов.
14. Способ по п. 13, причем молярное соотношение 1,3-диола и алкиленоксидов с 2-18 атомами углерода находится в диапазоне от 1:3 до 1:8.
15. Способ по п. 13, причем молярное соотношение 1,3-диола и алкиленоксидов с 2-18 атомами углерода находится в диапазоне от 1:4 до 1:6.
16. Способ по п. 13, причем алкиленоксиды с 2-18 атомами углерода выбираются из группы, состоящей из этиленоксида, пропиленоксида, бутиленоксида или их смеси.
17. Способ по п. 13, причем алкиленоксид с 2-18 атомами углерода представляет собой пропиленоксид.
18. Способ по любому из пп. 13-16, причем 1,3-диол формулы (III) выбирается из группы, состоящей из 2-бутил-2-этил-1,3-пропандиола, 2-метил-2-пропил-1,3-пропандиола, 2-метил-2-фенил-1,3-пропандиола, 2,2-диметил-1,3-пропандиола, 2-этил-1,3-гександиола.
19. Способ по любому из пп. 13-17, причем аминирование осуществляется в присутствии катализатора, содержащего медь, никель или кобальт.
20. Способ по п. 19, причем каталитически активный материал катализаторов перед их восстановлением водородом содержит соединения кислорода с алюминием, медью, никелем и кобальтом, и в диапазоне от 0,2 до 5,0% массовых соединений кислорода с оловом, рассчитанных как SnO.
21. Применение смеси простых эфираминов по любому из пп. 1-12 в средствах личной гигиены.
22. Применение смеси простых эфираминов по любому из пп. 1-12 в шампунях и композициях для мытья тела.
23. Применение смеси простых эфираминов по любому из пп. 1-12 в качестве отверждающего агента для эпоксидных смол или в качестве реагента в получении полимеров.
24. Применение смеси простых эфираминов по любому из пп. 1-12 в полиуретанах, полимочевинах и в качестве термопластичных полиамидных клеящих веществ.
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