RU2002131892A - Способ получения галоидированных гидроксидифенильных соединений - Google Patents
Способ получения галоидированных гидроксидифенильных соединений Download PDFInfo
- Publication number
- RU2002131892A RU2002131892A RU2002131892/04A RU2002131892A RU2002131892A RU 2002131892 A RU2002131892 A RU 2002131892A RU 2002131892/04 A RU2002131892/04 A RU 2002131892/04A RU 2002131892 A RU2002131892 A RU 2002131892A RU 2002131892 A RU2002131892 A RU 2002131892A
- Authority
- RU
- Russia
- Prior art keywords
- stage
- compounds
- reaction
- formula
- carried out
- Prior art date
Links
- 150000001875 compounds Chemical class 0.000 title claims 9
- 238000004519 manufacturing process Methods 0.000 title claims 3
- 238000000034 method Methods 0.000 claims 12
- 238000006243 chemical reaction Methods 0.000 claims 4
- 150000002989 phenols Chemical class 0.000 claims 4
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 claims 3
- 238000007254 oxidation reaction Methods 0.000 claims 3
- NHQDETIJWKXCTC-UHFFFAOYSA-N 3-chloroperbenzoic acid Chemical compound OOC(=O)C1=CC=CC(Cl)=C1 NHQDETIJWKXCTC-UHFFFAOYSA-N 0.000 claims 2
- MHAJPDPJQMAIIY-UHFFFAOYSA-N Hydrogen peroxide Chemical compound OO MHAJPDPJQMAIIY-UHFFFAOYSA-N 0.000 claims 2
- KFSLWBXXFJQRDL-UHFFFAOYSA-N Peracetic acid Chemical compound CC(=O)OO KFSLWBXXFJQRDL-UHFFFAOYSA-N 0.000 claims 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 2
- 238000005917 acylation reaction Methods 0.000 claims 2
- RYGMFSIKBFXOCR-UHFFFAOYSA-N Copper Chemical compound [Cu] RYGMFSIKBFXOCR-UHFFFAOYSA-N 0.000 claims 1
- 239000002841 Lewis acid Substances 0.000 claims 1
- WETWJCDKMRHUPV-UHFFFAOYSA-N acetyl chloride Chemical compound CC(Cl)=O WETWJCDKMRHUPV-UHFFFAOYSA-N 0.000 claims 1
- 239000012346 acetyl chloride Substances 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000007513 acids Chemical class 0.000 claims 1
- 150000001266 acyl halides Chemical class 0.000 claims 1
- 239000003054 catalyst Substances 0.000 claims 1
- 239000003795 chemical substances by application Substances 0.000 claims 1
- 229910052802 copper Inorganic materials 0.000 claims 1
- 239000010949 copper Substances 0.000 claims 1
- 239000000645 desinfectant Substances 0.000 claims 1
- -1 halogenated benzene compound Chemical class 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- 230000003301 hydrolyzing effect Effects 0.000 claims 1
- 150000007517 lewis acids Chemical class 0.000 claims 1
- 244000005700 microbiome Species 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000011368 organic material Substances 0.000 claims 1
- 230000001590 oxidative effect Effects 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/45—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by condensation
- C07C45/46—Friedel-Crafts reactions
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C41/00—Preparation of ethers; Preparation of compounds having groups, groups or groups
- C07C41/01—Preparation of ethers
- C07C41/18—Preparation of ethers by reactions not forming ether-oxygen bonds
- C07C41/26—Preparation of ethers by reactions not forming ether-oxygen bonds by introduction of hydroxy or O-metal groups
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C45/00—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds
- C07C45/61—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups
- C07C45/67—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton
- C07C45/68—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms
- C07C45/70—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form
- C07C45/71—Preparation of compounds having >C = O groups bound only to carbon or hydrogen atoms; Preparation of chelates of such compounds by reactions not involving the formation of >C = O groups by isomerisation; by change of size of the carbon skeleton by increase in the number of carbon atoms by reaction with functional groups containing oxygen only in singly bound form being hydroxy groups
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| EP00810382 | 2000-05-04 | ||
| EP00810382.2 | 2000-05-04 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| RU2002131892A true RU2002131892A (ru) | 2004-04-10 |
Family
ID=8174677
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| RU2002131892/04A RU2002131892A (ru) | 2000-05-04 | 2001-04-26 | Способ получения галоидированных гидроксидифенильных соединений |
Country Status (19)
| Country | Link |
|---|---|
| US (1) | US6706930B2 (https=) |
| EP (1) | EP1320516B1 (https=) |
| JP (1) | JP2003531880A (https=) |
| KR (1) | KR100801456B1 (https=) |
| CN (1) | CN1285555C (https=) |
| AR (1) | AR028400A1 (https=) |
| AT (1) | ATE305913T1 (https=) |
| AU (1) | AU2001260254A1 (https=) |
| BR (1) | BR0110458B1 (https=) |
| CZ (1) | CZ20023947A3 (https=) |
| DE (1) | DE60113862T2 (https=) |
| ES (1) | ES2249435T3 (https=) |
| IL (1) | IL152057A0 (https=) |
| MX (1) | MXPA02010291A (https=) |
| RU (1) | RU2002131892A (https=) |
| SK (1) | SK16912002A3 (https=) |
| TW (1) | TWI274748B (https=) |
| WO (1) | WO2001083418A1 (https=) |
| ZA (1) | ZA200209631B (https=) |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20050266095A1 (en) * | 2004-06-01 | 2005-12-01 | Erning Xia | Gentle preservative compositions |
| CN104628537A (zh) * | 2015-02-03 | 2015-05-20 | 武汉工程大学 | 一种2,5-二氯苯酚的合成工艺 |
| CN109020935A (zh) * | 2018-10-11 | 2018-12-18 | 西安近代化学研究所 | 一种二苯并呋喃衍生物及其制备方法 |
| CN113045390A (zh) * | 2021-03-17 | 2021-06-29 | 枣庄市润安制药新材料有限公司 | 一种利用Baeyer-Villiger氧化制备二氯生的方法 |
| CN116589344B (zh) * | 2023-05-17 | 2025-03-07 | 梯尔希(南京)药物研发有限公司 | 一种氘标记二氯生的合成方法 |
Family Cites Families (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| IL123015A (en) | 1997-02-05 | 2003-07-06 | Ciba Sc Holding Ag | Process for the preparation of ortho-substituted halophenols, some new intermediates and disinfectants for protecting organic materials from attack by microorganisms comprising compounds prepared by said process |
| EP1007501A1 (en) | 1997-08-29 | 2000-06-14 | The Dow Chemical Company | Process for producing diphenylethers and esters |
| US20020128522A1 (en) | 1998-10-06 | 2002-09-12 | Teodoro Armando Di | Process for the preparation of 4,4' -dihalogen-o-hydroxydiphenyl compounds |
-
2001
- 2001-04-09 TW TW090108566A patent/TWI274748B/zh not_active IP Right Cessation
- 2001-04-26 CN CNB01809001XA patent/CN1285555C/zh not_active Expired - Fee Related
- 2001-04-26 IL IL15205701A patent/IL152057A0/xx unknown
- 2001-04-26 AT AT01933893T patent/ATE305913T1/de not_active IP Right Cessation
- 2001-04-26 WO PCT/EP2001/004710 patent/WO2001083418A1/en not_active Ceased
- 2001-04-26 ES ES01933893T patent/ES2249435T3/es not_active Expired - Lifetime
- 2001-04-26 EP EP01933893A patent/EP1320516B1/en not_active Expired - Lifetime
- 2001-04-26 MX MXPA02010291A patent/MXPA02010291A/es active IP Right Grant
- 2001-04-26 BR BRPI0110458-6A patent/BR0110458B1/pt not_active IP Right Cessation
- 2001-04-26 US US10/275,022 patent/US6706930B2/en not_active Expired - Fee Related
- 2001-04-26 RU RU2002131892/04A patent/RU2002131892A/ru not_active Application Discontinuation
- 2001-04-26 AU AU2001260254A patent/AU2001260254A1/en not_active Abandoned
- 2001-04-26 KR KR1020027014670A patent/KR100801456B1/ko not_active Expired - Fee Related
- 2001-04-26 SK SK1691-2002A patent/SK16912002A3/sk unknown
- 2001-04-26 DE DE60113862T patent/DE60113862T2/de not_active Expired - Lifetime
- 2001-04-26 JP JP2001580851A patent/JP2003531880A/ja not_active Withdrawn
- 2001-04-26 CZ CZ20023947A patent/CZ20023947A3/cs unknown
- 2001-05-02 AR ARP010102071A patent/AR028400A1/es unknown
-
2002
- 2002-11-27 ZA ZA200209631A patent/ZA200209631B/en unknown
Also Published As
| Publication number | Publication date |
|---|---|
| DE60113862D1 (de) | 2006-02-16 |
| BR0110458A (pt) | 2003-03-11 |
| BR0110458B1 (pt) | 2012-06-12 |
| KR100801456B1 (ko) | 2008-02-11 |
| CN1427811A (zh) | 2003-07-02 |
| IL152057A0 (en) | 2003-05-29 |
| ES2249435T3 (es) | 2006-04-01 |
| JP2003531880A (ja) | 2003-10-28 |
| TWI274748B (en) | 2007-03-01 |
| CZ20023947A3 (cs) | 2003-03-12 |
| AR028400A1 (es) | 2003-05-07 |
| ATE305913T1 (de) | 2005-10-15 |
| US6706930B2 (en) | 2004-03-16 |
| WO2001083418A1 (en) | 2001-11-08 |
| EP1320516B1 (en) | 2005-10-05 |
| KR20020092464A (ko) | 2002-12-11 |
| EP1320516A1 (en) | 2003-06-25 |
| CN1285555C (zh) | 2006-11-22 |
| ZA200209631B (en) | 2003-10-23 |
| SK16912002A3 (sk) | 2003-05-02 |
| AU2001260254A1 (en) | 2001-11-12 |
| US20030163005A1 (en) | 2003-08-28 |
| DE60113862T2 (de) | 2006-04-27 |
| MXPA02010291A (es) | 2003-04-25 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| FA93 | Acknowledgement of application withdrawn (no request for examination) |
Effective date: 20050111 |