PL86751B1 - - Google Patents
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- Publication number
- PL86751B1 PL86751B1 PL1973167687A PL16768773A PL86751B1 PL 86751 B1 PL86751 B1 PL 86751B1 PL 1973167687 A PL1973167687 A PL 1973167687A PL 16768773 A PL16768773 A PL 16768773A PL 86751 B1 PL86751 B1 PL 86751B1
- Authority
- PL
- Poland
- Prior art keywords
- dye
- fluidized bed
- aqueous
- iii
- vat
- Prior art date
Links
- 239000000975 dye Substances 0.000 claims description 74
- 238000000034 method Methods 0.000 claims description 44
- 238000002360 preparation method Methods 0.000 claims description 34
- 239000000047 product Substances 0.000 claims description 32
- 239000000203 mixture Substances 0.000 claims description 27
- 238000001035 drying Methods 0.000 claims description 23
- 238000010410 dusting Methods 0.000 claims description 21
- 238000009472 formulation Methods 0.000 claims description 20
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 16
- 239000002270 dispersing agent Substances 0.000 claims description 15
- 238000004043 dyeing Methods 0.000 claims description 15
- 239000007921 spray Substances 0.000 claims description 15
- 239000000428 dust Substances 0.000 claims description 11
- 239000000843 powder Substances 0.000 claims description 10
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 claims description 9
- 239000000725 suspension Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 8
- 238000012360 testing method Methods 0.000 claims description 8
- 238000005119 centrifugation Methods 0.000 claims description 6
- 239000007859 condensation product Substances 0.000 claims description 6
- 239000013011 aqueous formulation Substances 0.000 claims description 5
- 239000003795 chemical substances by application Substances 0.000 claims description 5
- 238000005243 fluidization Methods 0.000 claims description 5
- 238000004519 manufacturing process Methods 0.000 claims description 5
- 239000000984 vat dye Substances 0.000 claims description 5
- 239000002253 acid Substances 0.000 claims description 4
- 239000000853 adhesive Substances 0.000 claims description 4
- WSFSSNUMVMOOMR-NJFSPNSNSA-N methanone Chemical compound O=[14CH2] WSFSSNUMVMOOMR-NJFSPNSNSA-N 0.000 claims description 4
- GEHJYWRUCIMESM-UHFFFAOYSA-L sodium sulfite Chemical compound [Na+].[Na+].[O-]S([O-])=O GEHJYWRUCIMESM-UHFFFAOYSA-L 0.000 claims description 4
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 claims description 3
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 3
- 230000001070 adhesive effect Effects 0.000 claims description 3
- 239000004202 carbamide Substances 0.000 claims description 3
- 238000001914 filtration Methods 0.000 claims description 3
- WHOZNOZYMBRCBL-OUKQBFOZSA-N (2E)-2-Tetradecenal Chemical compound CCCCCCCCCCC\C=C\C=O WHOZNOZYMBRCBL-OUKQBFOZSA-N 0.000 claims description 2
- 229920001732 Lignosulfonate Polymers 0.000 claims description 2
- 239000003085 diluting agent Substances 0.000 claims description 2
- 239000004744 fabric Substances 0.000 claims description 2
- PSZYNBSKGUBXEH-UHFFFAOYSA-N naphthalene-1-sulfonic acid Chemical compound C1=CC=C2C(S(=O)(=O)O)=CC=CC2=C1 PSZYNBSKGUBXEH-UHFFFAOYSA-N 0.000 claims description 2
- 229940044654 phenolsulfonic acid Drugs 0.000 claims description 2
- 235000010265 sodium sulphite Nutrition 0.000 claims description 2
- 239000000126 substance Substances 0.000 claims description 2
- 230000008878 coupling Effects 0.000 claims 3
- 238000010168 coupling process Methods 0.000 claims 3
- 238000005859 coupling reaction Methods 0.000 claims 3
- ZLCUIOWQYBYEBG-UHFFFAOYSA-N 1-Amino-2-methylanthraquinone Chemical compound C1=CC=C2C(=O)C3=C(N)C(C)=CC=C3C(=O)C2=C1 ZLCUIOWQYBYEBG-UHFFFAOYSA-N 0.000 claims 1
- AZXGXVQWEUFULR-UHFFFAOYSA-N 2',4',5',7'-tetrabromofluorescein Chemical compound OC(=O)C1=CC=CC=C1C1=C2C=C(Br)C(=O)C(Br)=C2OC2=C(Br)C(O)=C(Br)C=C21 AZXGXVQWEUFULR-UHFFFAOYSA-N 0.000 claims 1
- DPJCXCZTLWNFOH-UHFFFAOYSA-N 2-nitroaniline Chemical compound NC1=CC=CC=C1[N+]([O-])=O DPJCXCZTLWNFOH-UHFFFAOYSA-N 0.000 claims 1
- QPQKUYVSJWQSDY-CCEZHUSRSA-N 4-(phenylazo)aniline Chemical compound C1=CC(N)=CC=C1\N=N\C1=CC=CC=C1 QPQKUYVSJWQSDY-CCEZHUSRSA-N 0.000 claims 1
- RTNPPPQVXREFKX-UHFFFAOYSA-N 4-hydroxy-1-methylquinolin-2-one Chemical compound C1=CC=C2C(O)=CC(=O)N(C)C2=C1 RTNPPPQVXREFKX-UHFFFAOYSA-N 0.000 claims 1
- SQBCSDZTDXLTLE-UHFFFAOYSA-N 5-nitro-2,1-benzothiazol-3-amine Chemical compound C1=CC([N+]([O-])=O)=CC2=C(N)SN=C21 SQBCSDZTDXLTLE-UHFFFAOYSA-N 0.000 claims 1
- 150000001875 compounds Chemical class 0.000 claims 1
- 238000002347 injection Methods 0.000 claims 1
- 239000007924 injection Substances 0.000 claims 1
- UCANIZWVDIFCHH-UHFFFAOYSA-N n-(9,10-dioxoanthracen-1-yl)-7-oxobenzo[e]perimidine-4-carboxamide Chemical compound O=C1C2=CC=CC=C2C2=NC=NC3=C2C1=CC=C3C(=O)NC1=CC=CC2=C1C(=O)C1=CC=CC=C1C2=O UCANIZWVDIFCHH-UHFFFAOYSA-N 0.000 claims 1
- 239000001048 orange dye Substances 0.000 claims 1
- 239000000049 pigment Substances 0.000 claims 1
- UGCDBQWJXSAYIL-UHFFFAOYSA-N vat blue 6 Chemical compound O=C1C2=CC=CC=C2C(=O)C(C=C2Cl)=C1C1=C2NC2=C(C(=O)C=3C(=CC=CC=3)C3=O)C3=CC(Cl)=C2N1 UGCDBQWJXSAYIL-UHFFFAOYSA-N 0.000 claims 1
- 238000013467 fragmentation Methods 0.000 description 6
- 238000006062 fragmentation reaction Methods 0.000 description 6
- 238000000227 grinding Methods 0.000 description 6
- 239000011324 bead Substances 0.000 description 5
- 239000012530 fluid Substances 0.000 description 5
- 239000006185 dispersion Substances 0.000 description 4
- 238000005507 spraying Methods 0.000 description 4
- 230000000052 comparative effect Effects 0.000 description 3
- 239000010419 fine particle Substances 0.000 description 3
- 238000001694 spray drying Methods 0.000 description 3
- 150000007513 acids Chemical class 0.000 description 2
- 230000015572 biosynthetic process Effects 0.000 description 2
- 239000002775 capsule Substances 0.000 description 2
- 238000004140 cleaning Methods 0.000 description 2
- 239000000986 disperse dye Substances 0.000 description 2
- 239000008187 granular material Substances 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 239000003973 paint Substances 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 239000003826 tablet Substances 0.000 description 2
- 238000010998 test method Methods 0.000 description 2
- 238000009736 wetting Methods 0.000 description 2
- 239000004117 Lignosulphonate Substances 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000007864 aqueous solution Substances 0.000 description 1
- 239000007900 aqueous suspension Substances 0.000 description 1
- 239000011805 ball Substances 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000009833 condensation Methods 0.000 description 1
- 230000005494 condensation Effects 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 230000006866 deterioration Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 239000012065 filter cake Substances 0.000 description 1
- 239000011521 glass Substances 0.000 description 1
- 238000005469 granulation Methods 0.000 description 1
- 230000003179 granulation Effects 0.000 description 1
- 238000010438 heat treatment Methods 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000004898 kneading Methods 0.000 description 1
- 229920005610 lignin Polymers 0.000 description 1
- 235000019357 lignosulphonate Nutrition 0.000 description 1
- 239000007788 liquid Substances 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- 239000011049 pearl Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000011164 primary particle Substances 0.000 description 1
- 230000002035 prolonged effect Effects 0.000 description 1
- 238000004064 recycling Methods 0.000 description 1
- 238000005096 rolling process Methods 0.000 description 1
- 239000013049 sediment Substances 0.000 description 1
- 238000007873 sieving Methods 0.000 description 1
- 239000002002 slurry Substances 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 238000009987 spinning Methods 0.000 description 1
- 230000006641 stabilisation Effects 0.000 description 1
- 238000011105 stabilization Methods 0.000 description 1
- 238000003756 stirring Methods 0.000 description 1
- 238000003860 storage Methods 0.000 description 1
- LSNNMFCWUKXFEE-UHFFFAOYSA-L sulfite Chemical compound [O-]S([O-])=O LSNNMFCWUKXFEE-UHFFFAOYSA-L 0.000 description 1
- 150000003460 sulfonic acids Chemical class 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 239000010409 thin film Substances 0.000 description 1
- 238000003466 welding Methods 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0071—Process features in the making of dyestuff preparations; Dehydrating agents; Dispersing agents; Dustfree compositions
- C09B67/0092—Dyes in solid form
- C09B67/0095—Process features in the making of granulates
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Drying Of Solid Materials (AREA)
- Detergent Compositions (AREA)
- Coloring (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Processes Of Treating Macromolecular Substances (AREA)
- Adhesives Or Adhesive Processes (AREA)
- Manufacturing Of Micro-Capsules (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE2263968A DE2263968C3 (de) | 1972-12-29 | 1972-12-29 | Verfahren zur Herstellung von nichtstaubenden oder praktisch nichtstaubenden Farbstoffkörnern |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| PL86751B1 true PL86751B1 (en:Method) | 1976-06-30 |
Family
ID=5865722
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL1973167687A PL86751B1 (en:Method) | 1972-12-29 | 1973-12-28 |
Country Status (16)
| Country | Link |
|---|---|
| US (1) | US3879855A (en:Method) |
| JP (1) | JPS5753383B2 (en:Method) |
| AU (1) | AU476972B2 (en:Method) |
| BE (1) | BE809134A (en:Method) |
| BR (1) | BR7310174D0 (en:Method) |
| CH (1) | CH579624A5 (en:Method) |
| CS (1) | CS190416B2 (en:Method) |
| DD (1) | DD108317A5 (en:Method) |
| DE (1) | DE2263968C3 (en:Method) |
| DK (1) | DK138548C (en:Method) |
| ES (1) | ES421915A1 (en:Method) |
| FR (1) | FR2212401B1 (en:Method) |
| GB (1) | GB1449283A (en:Method) |
| IT (1) | IT1000383B (en:Method) |
| NL (1) | NL7317620A (en:Method) |
| PL (1) | PL86751B1 (en:Method) |
Families Citing this family (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4146466A (en) * | 1975-08-21 | 1979-03-27 | British Leyland Uk Limited | Apparatus for use in producing a fluidized bed of granular material |
| CH635862A5 (de) * | 1977-10-15 | 1983-04-29 | Ciba Geigy Ag | Verfahren zur granulierung von pigmenten. |
| EP0024654A1 (de) * | 1979-08-22 | 1981-03-11 | Ciba-Geigy Ag | Granulate von faserreaktiven Farbstoffen und Verfahren zu ihrer Herstellung |
| FR2468633A1 (fr) * | 1979-09-21 | 1981-05-08 | Ugine Kuhlmann | Procede de preparation de colorants complexes metalliferes azoiques 1/2 dissymetriques monosulfones sous forme de granules non poussiereux, solubles dans l'eau et granules ainsi obtenus |
| US4560747A (en) * | 1979-10-30 | 1985-12-24 | Ciba Geigy Corporation | Process for producing granulates of water-soluble dyes by fluidized bed granulation |
| JPS57171429A (en) * | 1981-04-13 | 1982-10-22 | Glatt Gmbh | Rotary disk type granulator |
| CH652940A5 (de) * | 1982-01-09 | 1985-12-13 | Sandoz Ag | Verfahren zur herstellung nicht staubender granulate und vorrichtung hierfuer. |
| JPS59196726A (ja) * | 1983-04-19 | 1984-11-08 | Okawara Mfg Co Ltd | 連続流動層造粒装置 |
| CH658667A5 (de) * | 1984-05-04 | 1986-11-28 | Ciba Geigy Ag | Verfahren zur herstellung von farbstoffgranulaten. |
| US4670993A (en) * | 1984-08-16 | 1987-06-09 | E.C.C. America Inc. | Method for fluidizing fine kaolin particles |
| US4663859A (en) * | 1985-10-04 | 1987-05-12 | Ciba-Geigy Corporation | Method for improving strength of dry dye particles and reducing explosion hazards |
| DE3635313A1 (de) * | 1986-10-17 | 1988-04-28 | Bayer Ag | Verfahren zur herstellung von granulaten |
| US5143671A (en) * | 1990-10-31 | 1992-09-01 | Eastman Kodak Company | Fluidized bed process for treating pigments |
| WO2000005292A1 (de) * | 1998-07-21 | 2000-02-03 | Vantico Ag | Rieselfähige granulate |
| DE60035906D1 (de) * | 2000-12-29 | 2007-09-20 | Roha Dyechem Private Ltd | Verfahren zur herstellung nahrungsfarbstoffen in granulatform |
| EP1870649A1 (en) * | 2006-06-20 | 2007-12-26 | Octapharma AG | Lyophilisation targetting defined residual moisture by limited desorption energy levels |
| CN101942225A (zh) * | 2010-08-27 | 2011-01-12 | 江苏亚邦染料股份有限公司 | 一种环保型蓝色还原染料及其商品化制造方法 |
| CH706388A2 (de) * | 2012-04-28 | 2013-10-31 | Michael Geisinger | Verfahren zur Vorrichtung zur Eindickung von flüssigen Lösungen, zur Trocknung des eingedampften Konzentrates, wie auch feuchter Schüttgüter. |
Family Cites Families (21)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US1837772A (en) * | 1927-04-11 | 1931-12-22 | British Dyestuffs Corp Ltd | Process for the preparation of solid bodies in finely divided states |
| GB676721A (en) * | 1949-03-03 | 1952-07-30 | Celanese Corp | Dyestuff powders |
| DE858093C (de) * | 1949-06-16 | 1952-12-04 | Ciba Geigy | Verfahren zur Herstellung trockener Pigmentpraeparate |
| CH353678A (de) * | 1957-06-12 | 1961-04-15 | Ciba Geigy | Verfahren zur Gewinnung eines Granulates bei der Zerstäubungstrocknung von flüssigen oder pastenförmigen Stoffen oder von Filterkuchen und Einrichtung zur Durchführung des Verfahrens |
| DE1204919B (de) * | 1959-03-02 | 1965-11-11 | Acna | Verfahren zum Herstellen feinverteilter Teilchen von unloeslichen organischen Farbstoffen und Pigmenten |
| US3212197A (en) * | 1961-06-08 | 1965-10-19 | James R Crawford | Drying method and apparatus |
| DE1241985B (de) * | 1962-01-17 | 1967-06-08 | Basf Ag | Verfahren zur Herstellung von stickstoffhaltigen Kondensationsprodukten |
| US3156520A (en) * | 1963-04-01 | 1964-11-10 | American Can Co | Dyestuffs and alkali metal salts of wood sugar acids and lignin sulfonates |
| CH431576A (de) * | 1964-01-07 | 1967-03-15 | Inventa Ag | Verfahren zum Granulieren von stickstoffhaltigen Düngemitteln |
| GB1052156A (en:Method) * | 1964-05-04 | |||
| FR1441832A (fr) * | 1964-06-01 | 1966-06-10 | Ciba Geigy | Agents de dispersion pour colorants difficilement solubles ou insolubles dans l'eau |
| GB1026329A (en) * | 1964-08-13 | 1966-04-20 | Dow Chemical Co | Preparation of pelletized solid materials |
| GB1168692A (en) * | 1966-02-28 | 1969-10-29 | Ogilvie Flour Mills Company Lt | Process and Apparatus for Preparing Free-Flowing and Readily Dispersible Products from Finely Powdered Materials. |
| CA852210A (en) * | 1966-09-26 | 1970-09-22 | Benko Julius | Lignin dispersing agents and methods of making the same |
| CH508708A (de) * | 1968-06-14 | 1971-06-15 | Ciba Geigy Ag | Präparat und deren Verwendung zur Herstellung gefärbter Gebilde |
| GB1277110A (en) * | 1968-08-21 | 1972-06-07 | Sincat Spa | The treatment of particles in a fluidised bed |
| DE1792355A1 (de) * | 1968-08-23 | 1971-06-03 | Bayer Ag | Pigmentfarbstoff-Granulierung |
| DE2032926C3 (de) * | 1970-07-03 | 1975-11-27 | Hoechst Ag, 6000 Frankfurt | Dispergiermittel für die Feinverteilung und Stabilisierung von Farbstoffen und Farbstoffpräparationen |
| GB1381495A (en) * | 1971-06-18 | 1975-01-22 | Struthers Scient International | Fluidized bed process and apparatus |
| US3748103A (en) * | 1971-06-25 | 1973-07-24 | Allied Chem | Process for the production of hydrous granular sodium silicate |
| US3748745A (en) * | 1971-11-29 | 1973-07-31 | Ici Ltd | Dyestuff manufacture |
-
1972
- 1972-12-29 DE DE2263968A patent/DE2263968C3/de not_active Expired
-
1973
- 1973-12-18 AU AU63726/73A patent/AU476972B2/en not_active Expired
- 1973-12-18 FR FR7345231A patent/FR2212401B1/fr not_active Expired
- 1973-12-18 GB GB5851373A patent/GB1449283A/en not_active Expired
- 1973-12-19 US US426371A patent/US3879855A/en not_active Expired - Lifetime
- 1973-12-21 NL NL7317620A patent/NL7317620A/xx not_active Application Discontinuation
- 1973-12-21 DD DD175612A patent/DD108317A5/xx unknown
- 1973-12-21 DK DK700273A patent/DK138548C/da not_active IP Right Cessation
- 1973-12-21 CH CH1811373A patent/CH579624A5/xx not_active IP Right Cessation
- 1973-12-21 IT IT54549/73A patent/IT1000383B/it active
- 1973-12-27 BR BR10174/73A patent/BR7310174D0/pt unknown
- 1973-12-27 JP JP48144623A patent/JPS5753383B2/ja not_active Expired
- 1973-12-27 BE BE139295A patent/BE809134A/xx not_active IP Right Cessation
- 1973-12-28 CS CS739056A patent/CS190416B2/cs unknown
- 1973-12-28 PL PL1973167687A patent/PL86751B1/pl unknown
- 1973-12-29 ES ES421915A patent/ES421915A1/es not_active Expired
Also Published As
| Publication number | Publication date |
|---|---|
| GB1449283A (en) | 1976-09-15 |
| FR2212401A1 (en:Method) | 1974-07-26 |
| DK138548C (da) | 1979-02-26 |
| DE2263968C3 (de) | 1984-09-13 |
| BE809134A (fr) | 1974-06-27 |
| ES421915A1 (es) | 1976-04-01 |
| BR7310174D0 (pt) | 1974-08-15 |
| CH579624A5 (en:Method) | 1976-09-15 |
| AU6372673A (en) | 1975-06-19 |
| DD108317A5 (en:Method) | 1974-09-12 |
| NL7317620A (en:Method) | 1974-07-02 |
| CS190416B2 (en) | 1979-05-31 |
| DE2263968A1 (de) | 1974-07-11 |
| JPS4999526A (en:Method) | 1974-09-20 |
| IT1000383B (it) | 1976-03-30 |
| AU476972B2 (en) | 1976-10-07 |
| FR2212401B1 (en:Method) | 1979-05-04 |
| US3879855A (en) | 1975-04-29 |
| DK138548B (da) | 1978-09-25 |
| JPS5753383B2 (en:Method) | 1982-11-12 |
| DE2263968B2 (de) | 1975-02-20 |
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