PL393606A1 - Sposób wytwarzania dichloropropanoli z gliceryny - Google Patents
Sposób wytwarzania dichloropropanoli z glicerynyInfo
- Publication number
- PL393606A1 PL393606A1 PL393606A PL39360611A PL393606A1 PL 393606 A1 PL393606 A1 PL 393606A1 PL 393606 A PL393606 A PL 393606A PL 39360611 A PL39360611 A PL 39360611A PL 393606 A1 PL393606 A1 PL 393606A1
- Authority
- PL
- Poland
- Prior art keywords
- dichloropropanols
- stream
- hydrochlorination
- stage
- directed
- Prior art date
Links
- PEDCQBHIVMGVHV-UHFFFAOYSA-N Glycerine Chemical compound OCC(O)CO PEDCQBHIVMGVHV-UHFFFAOYSA-N 0.000 title abstract 11
- XEPXTKKIWBPAEG-UHFFFAOYSA-N 1,1-dichloropropan-1-ol Chemical class CCC(O)(Cl)Cl XEPXTKKIWBPAEG-UHFFFAOYSA-N 0.000 title abstract 6
- 238000000034 method Methods 0.000 title abstract 2
- 235000011187 glycerol Nutrition 0.000 title 1
- 238000007038 hydrochlorination reaction Methods 0.000 abstract 5
- QTBSBXVTEAMEQO-UHFFFAOYSA-N Acetic acid Chemical compound CC(O)=O QTBSBXVTEAMEQO-UHFFFAOYSA-N 0.000 abstract 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 abstract 3
- 230000002378 acidificating effect Effects 0.000 abstract 2
- 239000003054 catalyst Substances 0.000 abstract 2
- 238000006243 chemical reaction Methods 0.000 abstract 2
- 238000004821 distillation Methods 0.000 abstract 2
- 239000012451 post-reaction mixture Substances 0.000 abstract 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 abstract 1
- 238000005660 chlorination reaction Methods 0.000 abstract 1
- 238000011437 continuous method Methods 0.000 abstract 1
- ZZUFCTLCJUWOSV-UHFFFAOYSA-N furosemide Chemical compound C1=C(Cl)C(S(=O)(=O)N)=CC(C(O)=O)=C1NCC1=CC=CO1 ZZUFCTLCJUWOSV-UHFFFAOYSA-N 0.000 abstract 1
- IXCSERBJSXMMFS-UHFFFAOYSA-N hydrogen chloride Substances Cl.Cl IXCSERBJSXMMFS-UHFFFAOYSA-N 0.000 abstract 1
- 229910000041 hydrogen chloride Inorganic materials 0.000 abstract 1
- 238000004519 manufacturing process Methods 0.000 abstract 1
- 238000000926 separation method Methods 0.000 abstract 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/62—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring by introduction of halogen; by substitution of halogen atoms by other halogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Priority Applications (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL393606A PL215730B1 (pl) | 2011-01-10 | 2011-01-10 | Sposób wytwarzania dichloropropanoli z gliceryny |
| PCT/PL2012/000001 WO2012096585A2 (en) | 2011-01-10 | 2012-01-04 | Method for production of dichloropropanols from glycerol |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| PL393606A PL215730B1 (pl) | 2011-01-10 | 2011-01-10 | Sposób wytwarzania dichloropropanoli z gliceryny |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| PL393606A1 true PL393606A1 (pl) | 2012-07-16 |
| PL215730B1 PL215730B1 (pl) | 2014-01-31 |
Family
ID=45768275
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| PL393606A PL215730B1 (pl) | 2011-01-10 | 2011-01-10 | Sposób wytwarzania dichloropropanoli z gliceryny |
Country Status (2)
| Country | Link |
|---|---|
| PL (1) | PL215730B1 (pl) |
| WO (1) | WO2012096585A2 (pl) |
Families Citing this family (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN112573997A (zh) * | 2020-12-03 | 2021-03-30 | 浙江镇洋发展股份有限公司 | 一种从粗二氯丙醇中分离氯化氢的工艺及其分离设备 |
| CN113731332A (zh) * | 2021-09-09 | 2021-12-03 | 黄山五环科技有限公司 | 一种甘油法生产环氧树脂的氯化氢供应设备及其供应方法 |
Family Cites Families (18)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| PL198551A1 (pl) | 1977-05-31 | 1978-04-10 | Wyzsza Szkola Morska | Uklad jednofazowego regulowanego zasilacza tyrystorowego o podwyzszonej czestotliwosci |
| JPH0643354B2 (ja) * | 1989-08-10 | 1994-06-08 | ダイソー株式会社 | ２，３―ジクロロ―１―プロパノールの連続的製法及びその装置 |
| CZ20032346A3 (cs) | 2003-09-01 | 2005-04-13 | Spolek Pro Chemickou A Hutní Výrobu,A.S. | Způsob přípravy dichlorpropanolů z glycerinu |
| ATE511498T1 (de) * | 2003-11-20 | 2011-06-15 | Solvay | Verfahren zur herstellung von dichlorpropanol aus glycerin und einem chlorinierungsmittel in anwesenheit von einem katalysator ausgewählt aus adipin- und glutarsaeure |
| FR2868419B1 (fr) * | 2004-04-05 | 2008-08-08 | Solvay Sa Sa Belge | Procede de fabrication de dichloropropanol |
| WO2006020234A1 (en) | 2004-07-21 | 2006-02-23 | Dow Global Technologies Inc. | Conversion of a multihydroxylated-aliphatic hydrocarbon or ester thereof to a chlorohydrin |
| CA2608720A1 (en) | 2005-05-20 | 2006-09-28 | Solvay (Societe Anonyme) | Method for making chlorohydrin in corrosion-resistant equipment |
| WO2008074733A1 (en) | 2006-12-19 | 2008-06-26 | Akzo Nobel N.V. | Process for the catalytic halogenation of a hydroxylated organic compound |
| KR20100016454A (ko) * | 2007-04-12 | 2010-02-12 | 다우 글로벌 테크놀로지스 인크. | 클로로하이드린 제조 방법 및 장치 |
| PL210903B1 (pl) * | 2007-08-17 | 2012-03-30 | Zakłady Chemiczne Zachem Społka Akcyjna | Sposób otrzymywania monochloropropandioli i dichloropropanoli |
| PL211897B1 (pl) | 2007-10-05 | 2012-07-31 | Inst Ciężkiej Syntezy Organicznej Blachownia | Sposób wytwarzania mieszaniny 1,3- i 2,3-dichloropropanoli |
| KR101488052B1 (ko) | 2007-11-19 | 2015-01-29 | 꼰세르 엣세.삐.아. | 글리세린의 디클로로히드린 및 에피클로로히드린으로의 전환법 |
| TWI339654B (en) * | 2007-12-04 | 2011-04-01 | Chang Chun Plastics Co Ltd | Process and apparatus for continuous preparing dichloropropanol |
| KR100881344B1 (ko) | 2007-12-12 | 2009-02-02 | 삼성정밀화학 주식회사 | 헤테로폴리산 촉매를 사용하여 글리세롤로부터디클로로프로판올을 제조하는 방법 |
| RU2358964C1 (ru) | 2007-12-27 | 2009-06-20 | Общество с ограниченной ответственностью "Синтез-2" | Способ получения дихлорпропанолов |
| DE102008007622A1 (de) | 2008-02-04 | 2009-08-06 | Biopetrol Industries Ag | Verfahren zur Herstellung von Epichlorhydrin aus Glyzerin |
| WO2009104961A2 (en) * | 2008-02-21 | 2009-08-27 | Bouwe De Jong | Process for the preparation of a dichloropropanol product |
| KR101067494B1 (ko) * | 2008-12-31 | 2011-09-27 | 삼성정밀화학 주식회사 | 디클로로프로판올의 선택도가 향상된, 글리세롤을 사용하는디클로로프로판올의 제조방법 |
-
2011
- 2011-01-10 PL PL393606A patent/PL215730B1/pl unknown
-
2012
- 2012-01-04 WO PCT/PL2012/000001 patent/WO2012096585A2/en not_active Ceased
Also Published As
| Publication number | Publication date |
|---|---|
| WO2012096585A2 (en) | 2012-07-19 |
| WO2012096585A3 (en) | 2012-11-08 |
| PL215730B1 (pl) | 2014-01-31 |
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