NO322699B1 - Fremgangsmate for a separere og konsentrere gallium og eventuelt indium fra andre komponenter - Google Patents
Fremgangsmate for a separere og konsentrere gallium og eventuelt indium fra andre komponenter Download PDFInfo
- Publication number
- NO322699B1 NO322699B1 NO20000204A NO20000204A NO322699B1 NO 322699 B1 NO322699 B1 NO 322699B1 NO 20000204 A NO20000204 A NO 20000204A NO 20000204 A NO20000204 A NO 20000204A NO 322699 B1 NO322699 B1 NO 322699B1
- Authority
- NO
- Norway
- Prior art keywords
- gallium
- jarosite
- indium
- solution
- iron
- Prior art date
Links
- 229910052733 gallium Inorganic materials 0.000 title claims abstract description 110
- GYHNNYVSQQEPJS-UHFFFAOYSA-N Gallium Chemical compound [Ga] GYHNNYVSQQEPJS-UHFFFAOYSA-N 0.000 title claims abstract description 109
- 229910052738 indium Inorganic materials 0.000 title claims abstract description 67
- APFVFJFRJDLVQX-UHFFFAOYSA-N indium atom Chemical compound [In] APFVFJFRJDLVQX-UHFFFAOYSA-N 0.000 title claims abstract description 67
- 238000000034 method Methods 0.000 title claims description 38
- 229910052935 jarosite Inorganic materials 0.000 claims abstract description 75
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims abstract description 20
- 239000002244 precipitate Substances 0.000 claims abstract description 20
- 238000006386 neutralization reaction Methods 0.000 claims abstract description 18
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 claims abstract description 16
- 239000000920 calcium hydroxide Substances 0.000 claims abstract description 16
- 229910001861 calcium hydroxide Inorganic materials 0.000 claims abstract description 16
- VTHJTEIRLNZDEV-UHFFFAOYSA-L magnesium dihydroxide Chemical compound [OH-].[OH-].[Mg+2] VTHJTEIRLNZDEV-UHFFFAOYSA-L 0.000 claims abstract description 10
- 239000000347 magnesium hydroxide Substances 0.000 claims abstract description 10
- 229910001862 magnesium hydroxide Inorganic materials 0.000 claims abstract description 10
- 229910000373 gallium sulfate Inorganic materials 0.000 claims abstract description 5
- SBDRYJMIQMDXRH-UHFFFAOYSA-N gallium;sulfuric acid Chemical compound [Ga].OS(O)(=O)=O SBDRYJMIQMDXRH-UHFFFAOYSA-N 0.000 claims abstract description 5
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 28
- 229910052782 aluminium Inorganic materials 0.000 claims description 26
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 26
- 229910052742 iron Inorganic materials 0.000 claims description 14
- -1 iron (III) ions Chemical class 0.000 claims description 14
- 150000001768 cations Chemical class 0.000 claims description 13
- 238000001556 precipitation Methods 0.000 claims description 10
- 239000007788 liquid Substances 0.000 claims description 9
- 239000002245 particle Substances 0.000 claims description 9
- QAOWNCQODCNURD-UHFFFAOYSA-L Sulfate Chemical compound [O-]S([O-])(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-L 0.000 claims description 8
- 239000007787 solid Substances 0.000 claims description 8
- 239000002253 acid Substances 0.000 claims description 7
- 229910052732 germanium Inorganic materials 0.000 claims description 7
- GNPVGFCGXDBREM-UHFFFAOYSA-N germanium atom Chemical compound [Ge] GNPVGFCGXDBREM-UHFFFAOYSA-N 0.000 claims description 7
- 239000007795 chemical reaction product Substances 0.000 claims description 6
- DNUARHPNFXVKEI-UHFFFAOYSA-K gallium(iii) hydroxide Chemical compound [OH-].[OH-].[OH-].[Ga+3] DNUARHPNFXVKEI-UHFFFAOYSA-K 0.000 claims description 6
- 229910021513 gallium hydroxide Inorganic materials 0.000 claims description 5
- 239000000047 product Substances 0.000 claims description 5
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 4
- 239000011707 mineral Substances 0.000 claims description 4
- 238000003756 stirring Methods 0.000 claims description 4
- 238000005406 washing Methods 0.000 claims description 2
- 239000003153 chemical reaction reagent Substances 0.000 claims 1
- 150000002259 gallium compounds Chemical class 0.000 claims 1
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 abstract description 27
- 229910052725 zinc Inorganic materials 0.000 abstract description 27
- 239000011701 zinc Substances 0.000 abstract description 27
- 238000002386 leaching Methods 0.000 abstract description 22
- 239000003513 alkali Substances 0.000 abstract description 4
- 238000007670 refining Methods 0.000 abstract description 4
- 239000000243 solution Substances 0.000 description 91
- HEMHJVSKTPXQMS-UHFFFAOYSA-M sodium hydroxide Inorganic materials [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 17
- 238000010586 diagram Methods 0.000 description 15
- 239000002585 base Substances 0.000 description 13
- 238000006243 chemical reaction Methods 0.000 description 12
- 238000000605 extraction Methods 0.000 description 11
- 239000000203 mixture Substances 0.000 description 10
- 239000012535 impurity Substances 0.000 description 8
- 238000000926 separation method Methods 0.000 description 8
- 238000011084 recovery Methods 0.000 description 7
- 239000000126 substance Substances 0.000 description 7
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 6
- 239000004411 aluminium Substances 0.000 description 5
- 238000005868 electrolysis reaction Methods 0.000 description 5
- 238000004519 manufacturing process Methods 0.000 description 5
- VTYYLEPIZMXCLO-UHFFFAOYSA-L Calcium carbonate Chemical compound [Ca+2].[O-]C([O-])=O VTYYLEPIZMXCLO-UHFFFAOYSA-L 0.000 description 4
- 230000002829 reductive effect Effects 0.000 description 4
- VTLYFUHAOXGGBS-UHFFFAOYSA-N Fe3+ Chemical compound [Fe+3] VTLYFUHAOXGGBS-UHFFFAOYSA-N 0.000 description 3
- 230000000694 effects Effects 0.000 description 3
- 238000010438 heat treatment Methods 0.000 description 3
- 229910001449 indium ion Inorganic materials 0.000 description 3
- 238000005342 ion exchange Methods 0.000 description 3
- 235000014413 iron hydroxide Nutrition 0.000 description 3
- NCNCGGDMXMBVIA-UHFFFAOYSA-L iron(ii) hydroxide Chemical compound [OH-].[OH-].[Fe+2] NCNCGGDMXMBVIA-UHFFFAOYSA-L 0.000 description 3
- 229910052751 metal Inorganic materials 0.000 description 3
- 239000002184 metal Substances 0.000 description 3
- 239000003960 organic solvent Substances 0.000 description 3
- 239000011347 resin Substances 0.000 description 3
- 229920005989 resin Polymers 0.000 description 3
- 239000011734 sodium Substances 0.000 description 3
- UQSXHKLRYXJYBZ-UHFFFAOYSA-N Iron oxide Chemical compound [Fe]=O UQSXHKLRYXJYBZ-UHFFFAOYSA-N 0.000 description 2
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 238000003723 Smelting Methods 0.000 description 2
- 230000002378 acidificating effect Effects 0.000 description 2
- 239000008346 aqueous phase Substances 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229910000019 calcium carbonate Inorganic materials 0.000 description 2
- 238000000975 co-precipitation Methods 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 239000012141 concentrate Substances 0.000 description 2
- 239000008151 electrolyte solution Substances 0.000 description 2
- 239000000706 filtrate Substances 0.000 description 2
- 238000001914 filtration Methods 0.000 description 2
- 238000011835 investigation Methods 0.000 description 2
- 150000002500 ions Chemical class 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 230000035484 reaction time Effects 0.000 description 2
- 239000004065 semiconductor Substances 0.000 description 2
- 229910021653 sulphate ion Inorganic materials 0.000 description 2
- NWUYHJFMYQTDRP-UHFFFAOYSA-N 1,2-bis(ethenyl)benzene;1-ethenyl-2-ethylbenzene;styrene Chemical compound C=CC1=CC=CC=C1.CCC1=CC=CC=C1C=C.C=CC1=CC=CC=C1C=C NWUYHJFMYQTDRP-UHFFFAOYSA-N 0.000 description 1
- 229910001218 Gallium arsenide Inorganic materials 0.000 description 1
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 239000003637 basic solution Substances 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 150000001732 carboxylic acid derivatives Chemical class 0.000 description 1
- 239000003518 caustics Substances 0.000 description 1
- 239000002738 chelating agent Substances 0.000 description 1
- 230000000052 comparative effect Effects 0.000 description 1
- 239000000356 contaminant Substances 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- MSNWSDPPULHLDL-UHFFFAOYSA-K ferric hydroxide Chemical compound [OH-].[OH-].[OH-].[Fe+3] MSNWSDPPULHLDL-UHFFFAOYSA-K 0.000 description 1
- 229910052602 gypsum Inorganic materials 0.000 description 1
- 239000010440 gypsum Substances 0.000 description 1
- XLYOFNOQVPJJNP-UHFFFAOYSA-M hydroxide Chemical compound [OH-] XLYOFNOQVPJJNP-UHFFFAOYSA-M 0.000 description 1
- 239000003456 ion exchange resin Substances 0.000 description 1
- 229920003303 ion-exchange polymer Polymers 0.000 description 1
- 239000004973 liquid crystal related substance Substances 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- 239000012074 organic phase Substances 0.000 description 1
- 238000010979 pH adjustment Methods 0.000 description 1
- 230000001376 precipitating effect Effects 0.000 description 1
- 230000005070 ripening Effects 0.000 description 1
- 229910052708 sodium Inorganic materials 0.000 description 1
- 239000007790 solid phase Substances 0.000 description 1
- 239000002562 thickening agent Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
- C22B3/20—Treatment or purification of solutions, e.g. obtained by leaching
- C22B3/44—Treatment or purification of solutions, e.g. obtained by leaching by chemical processes
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B19/00—Obtaining zinc or zinc oxide
- C22B19/20—Obtaining zinc otherwise than by distilling
- C22B19/26—Refining solutions containing zinc values, e.g. obtained by leaching zinc ores
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
- C22B58/00—Obtaining gallium or indium
-
- C—CHEMISTRY; METALLURGY
- C25—ELECTROLYTIC OR ELECTROPHORETIC PROCESSES; APPARATUS THEREFOR
- C25C—PROCESSES FOR THE ELECTROLYTIC PRODUCTION, RECOVERY OR REFINING OF METALS; APPARATUS THEREFOR
- C25C1/00—Electrolytic production, recovery or refining of metals by electrolysis of solutions
- C25C1/16—Electrolytic production, recovery or refining of metals by electrolysis of solutions of zinc, cadmium or mercury
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
- Y02P10/00—Technologies related to metal processing
- Y02P10/20—Recycling
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Mechanical Engineering (AREA)
- Geology (AREA)
- Life Sciences & Earth Sciences (AREA)
- General Life Sciences & Earth Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Environmental & Geological Engineering (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Electrochemistry (AREA)
- Manufacture And Refinement Of Metals (AREA)
- Separation Using Semi-Permeable Membranes (AREA)
- Transition And Organic Metals Composition Catalysts For Addition Polymerization (AREA)
- External Artificial Organs (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP00833999A JP3784187B2 (ja) | 1999-01-14 | 1999-01-14 | 溶液中のＧａ，Ｉｎの分離濃縮法 |
| JP27615199A JP3810963B2 (ja) | 1999-09-29 | 1999-09-29 | Ｇａの分離濃縮方法 |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO20000204D0 NO20000204D0 (no) | 2000-01-14 |
| NO20000204L NO20000204L (no) | 2000-07-17 |
| NO322699B1 true NO322699B1 (no) | 2006-11-27 |
Family
ID=26342836
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO20000204A NO322699B1 (no) | 1999-01-14 | 2000-01-14 | Fremgangsmate for a separere og konsentrere gallium og eventuelt indium fra andre komponenter |
Country Status (7)
| Country | Link |
|---|---|
| US (1) | US6319483B1 (de) |
| EP (1) | EP1020537B1 (de) |
| AT (1) | ATE250146T1 (de) |
| AU (1) | AU756317B2 (de) |
| CA (1) | CA2295468C (de) |
| DE (1) | DE60005226T2 (de) |
| NO (1) | NO322699B1 (de) |
Families Citing this family (15)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| TWI239552B (en) * | 2001-02-06 | 2005-09-11 | Sumitomo Chemical Co | Methods for producing indium-containing aqueous solutions containing reduced amounts of metal impurities |
| PE20021021A1 (es) * | 2001-03-08 | 2002-11-08 | Billiton Sa Ltd | Recuperacion de metales desde materiales conteniendo jarosita |
| RU2218244C1 (ru) * | 2002-04-05 | 2003-12-10 | Акционерное общество открытого типа "Челябинский электролитный цинковый завод" | Способ получения индиевого порошка высокой чистоты |
| FI118226B (fi) * | 2005-12-29 | 2007-08-31 | Outokumpu Technology Oyj | Menetelmä harvinaisten metallien talteenottamiseksi sinkin liuotusprosessissa |
| CN101195873B (zh) * | 2007-09-28 | 2010-12-15 | 黄昌海 | 从水溶液中沉淀镓 |
| CA2721518C (en) | 2010-11-26 | 2013-02-05 | Neo Material Technologies Inc. | Treatment of indium gallium alloys and recovery of indium and gallium |
| CN104603307B (zh) | 2012-08-31 | 2021-03-09 | 学校法人法政大学 | 金属化合物的浓缩方法 |
| CN103555946B (zh) * | 2013-11-15 | 2016-05-04 | 紫金矿业集团股份有限公司 | 一种含镓酸性溶液选择性富集制备富镓渣的方法 |
| CZ305491B6 (cs) * | 2013-12-19 | 2015-10-29 | Vysoká škola chemicko-technologická v Praze | Koncentrační separace india a galia z roztoků obsahujících měď srážením kyselinou šťavelovou |
| FI128281B (en) * | 2016-12-15 | 2020-02-28 | Teknologian Tutkimuskeskus Vtt Oy | Processing of metal-containing industrial waste material |
| DE102017107097B4 (de) | 2017-04-03 | 2024-02-08 | Technische Universität Bergakademie Freiberg | Verfahren zur Abtrennung von Indium aus metallhaltigen, wässrigen Lösungen |
| DE102017213956B3 (de) | 2017-08-10 | 2018-12-06 | Technische Universität Bergakademie Freiberg | Verfahren zur Gewinnung von Indium aus wässrigen, metallhaltigen Lösungen |
| CN110938754A (zh) * | 2018-09-21 | 2020-03-31 | 日立金属株式会社 | 镓的回收方法 |
| CN112430737A (zh) * | 2020-10-29 | 2021-03-02 | 深圳市中金岭南有色金属股份有限公司丹霞冶炼厂 | 一种从萃取沉镓渣中回收镓的方法 |
| EP4279619A1 (de) * | 2022-05-19 | 2023-11-22 | Helmholtz-Zentrum Dresden - Rossendorf e.V. | Verfahren zur abscheidung von indium, germanium und/oder gallium aus eisen |
Family Cites Families (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2574008A (en) | 1946-12-30 | 1951-11-06 | Pechiney Prod Chimiques Sa | Method of extracting gallium oxide from aluminous substances |
| NO123248B (de) | 1969-10-02 | 1971-10-18 | Norske Zinkkompani As | |
| CA1076364A (en) | 1976-04-15 | 1980-04-29 | Cominco Ltd. | Process for concentrating and recovering gallium |
| JPS59193230A (ja) | 1983-04-18 | 1984-11-01 | Dowa Mining Co Ltd | ＧａおよびＩｎ微量含有物質からのＧａおよびＩｎの回収方法 |
| WO1988003912A1 (en) | 1986-11-26 | 1988-06-02 | Resource Technology Associates | Process for recovering metal values from ferrite wastes |
| JPH0269319A (ja) | 1988-09-02 | 1990-03-08 | Agency Of Ind Science & Technol | アルミニウム塩を主成分とする水溶液よりガリウムを分離する方法 |
-
2000
- 2000-01-12 US US09/481,506 patent/US6319483B1/en not_active Expired - Fee Related
- 2000-01-13 DE DE2000605226 patent/DE60005226T2/de not_active Expired - Lifetime
- 2000-01-13 EP EP20000100678 patent/EP1020537B1/de not_active Expired - Lifetime
- 2000-01-13 AT AT00100678T patent/ATE250146T1/de not_active IP Right Cessation
- 2000-01-14 AU AU11356/00A patent/AU756317B2/en not_active Ceased
- 2000-01-14 CA CA 2295468 patent/CA2295468C/en not_active Expired - Fee Related
- 2000-01-14 NO NO20000204A patent/NO322699B1/no not_active IP Right Cessation
Also Published As
| Publication number | Publication date |
|---|---|
| DE60005226T2 (de) | 2004-04-08 |
| ATE250146T1 (de) | 2003-10-15 |
| CA2295468C (en) | 2006-08-01 |
| NO20000204L (no) | 2000-07-17 |
| EP1020537A1 (de) | 2000-07-19 |
| CA2295468A1 (en) | 2000-07-14 |
| AU1135600A (en) | 2000-07-20 |
| AU756317B2 (en) | 2003-01-09 |
| DE60005226D1 (de) | 2003-10-23 |
| EP1020537B1 (de) | 2003-09-17 |
| NO20000204D0 (no) | 2000-01-14 |
| US6319483B1 (en) | 2001-11-20 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MM1K | Lapsed by not paying the annual fees |