NO319309B1 - Fremgangsmate for fremstilling av en vandig losning av fritt hydroksylamin - Google Patents
Fremgangsmate for fremstilling av en vandig losning av fritt hydroksylamin Download PDFInfo
- Publication number
- NO319309B1 NO319309B1 NO19982847A NO982847A NO319309B1 NO 319309 B1 NO319309 B1 NO 319309B1 NO 19982847 A NO19982847 A NO 19982847A NO 982847 A NO982847 A NO 982847A NO 319309 B1 NO319309 B1 NO 319309B1
- Authority
- NO
- Norway
- Prior art keywords
- hydroxylamine
- solution
- column
- stripping
- salt
- Prior art date
Links
- AVXURJPOCDRRFD-UHFFFAOYSA-N Hydroxylamine Chemical compound ON AVXURJPOCDRRFD-UHFFFAOYSA-N 0.000 title claims abstract description 151
- 239000007864 aqueous solution Substances 0.000 title claims abstract description 15
- 238000004519 manufacturing process Methods 0.000 title description 5
- 239000000243 solution Substances 0.000 claims abstract description 89
- 238000000034 method Methods 0.000 claims abstract description 46
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 26
- 150000003839 salts Chemical class 0.000 claims abstract description 21
- 238000004821 distillation Methods 0.000 claims description 43
- 239000003381 stabilizer Substances 0.000 claims description 17
- 239000012266 salt solution Substances 0.000 claims description 14
- 238000003776 cleavage reaction Methods 0.000 claims description 5
- 230000007017 scission Effects 0.000 claims description 5
- FAPWRFPIFSIZLT-UHFFFAOYSA-M Sodium chloride Chemical compound [Na+].[Cl-] FAPWRFPIFSIZLT-UHFFFAOYSA-M 0.000 claims description 2
- 238000002360 preparation method Methods 0.000 claims description 2
- 238000000354 decomposition reaction Methods 0.000 abstract description 7
- 230000008646 thermal stress Effects 0.000 abstract 1
- HEMHJVSKTPXQMS-UHFFFAOYSA-M Sodium hydroxide Chemical compound [OH-].[Na+] HEMHJVSKTPXQMS-UHFFFAOYSA-M 0.000 description 21
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 description 12
- 239000011521 glass Substances 0.000 description 11
- VGYYSIDKAKXZEE-UHFFFAOYSA-L hydroxylammonium sulfate Chemical compound O[NH3+].O[NH3+].[O-]S([O-])(=O)=O VGYYSIDKAKXZEE-UHFFFAOYSA-L 0.000 description 10
- 229910000378 hydroxylammonium sulfate Inorganic materials 0.000 description 10
- 239000002585 base Substances 0.000 description 9
- PMZURENOXWZQFD-UHFFFAOYSA-L Sodium Sulfate Chemical compound [Na+].[Na+].[O-]S([O-])(=O)=O PMZURENOXWZQFD-UHFFFAOYSA-L 0.000 description 7
- BFNBIHQBYMNNAN-UHFFFAOYSA-N ammonium sulfate Chemical compound N.N.OS(O)(=O)=O BFNBIHQBYMNNAN-UHFFFAOYSA-N 0.000 description 7
- 229910052921 ammonium sulfate Inorganic materials 0.000 description 7
- 235000011130 ammonium sulphate Nutrition 0.000 description 7
- 229910052938 sodium sulfate Inorganic materials 0.000 description 7
- 235000011152 sodium sulphate Nutrition 0.000 description 7
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 6
- 229910021529 ammonia Inorganic materials 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 238000000926 separation method Methods 0.000 description 6
- NBYLBWHHTUWMER-UHFFFAOYSA-N 2-Methylquinolin-8-ol Chemical compound C1=CC=C(O)C2=NC(C)=CC=C21 NBYLBWHHTUWMER-UHFFFAOYSA-N 0.000 description 5
- 238000006243 chemical reaction Methods 0.000 description 5
- 238000002156 mixing Methods 0.000 description 5
- 230000001476 alcoholic effect Effects 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 238000010992 reflux Methods 0.000 description 4
- 239000005725 8-Hydroxyquinoline Substances 0.000 description 3
- KWYUFKZDYYNOTN-UHFFFAOYSA-M Potassium hydroxide Chemical compound [OH-].[K+] KWYUFKZDYYNOTN-UHFFFAOYSA-M 0.000 description 3
- -1 alkaline earth metal sulfates Chemical class 0.000 description 3
- JFDZBHWFFUWGJE-UHFFFAOYSA-N benzonitrile Chemical compound N#CC1=CC=CC=C1 JFDZBHWFFUWGJE-UHFFFAOYSA-N 0.000 description 3
- 150000002500 ions Chemical class 0.000 description 3
- 229960003540 oxyquinoline Drugs 0.000 description 3
- 238000012856 packing Methods 0.000 description 3
- 239000002244 precipitate Substances 0.000 description 3
- MCJGNVYPOGVAJF-UHFFFAOYSA-N quinolin-8-ol Chemical compound C1=CN=C2C(O)=CC=CC2=C1 MCJGNVYPOGVAJF-UHFFFAOYSA-N 0.000 description 3
- 238000003756 stirring Methods 0.000 description 3
- 239000000126 substance Substances 0.000 description 3
- FCKYPQBAHLOOJQ-NXEZZACHSA-N 2-[[(1r,2r)-2-[bis(carboxymethyl)amino]cyclohexyl]-(carboxymethyl)amino]acetic acid Chemical compound OC(=O)CN(CC(O)=O)[C@@H]1CCCC[C@H]1N(CC(O)=O)CC(O)=O FCKYPQBAHLOOJQ-NXEZZACHSA-N 0.000 description 2
- VEXZGXHMUGYJMC-UHFFFAOYSA-N Hydrochloric acid Chemical compound Cl VEXZGXHMUGYJMC-UHFFFAOYSA-N 0.000 description 2
- 239000007832 Na2SO4 Substances 0.000 description 2
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 description 2
- 229920002873 Polyethylenimine Polymers 0.000 description 2
- QAOWNCQODCNURD-UHFFFAOYSA-N Sulfuric acid Chemical compound OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 description 2
- 150000001298 alcohols Chemical class 0.000 description 2
- 150000001450 anions Chemical class 0.000 description 2
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 description 2
- 238000009835 boiling Methods 0.000 description 2
- AXCZMVOFGPJBDE-UHFFFAOYSA-L calcium dihydroxide Chemical compound [OH-].[OH-].[Ca+2] AXCZMVOFGPJBDE-UHFFFAOYSA-L 0.000 description 2
- 239000000920 calcium hydroxide Substances 0.000 description 2
- 229910001861 calcium hydroxide Inorganic materials 0.000 description 2
- BRPQOXSCLDDYGP-UHFFFAOYSA-N calcium oxide Chemical compound [O-2].[Ca+2] BRPQOXSCLDDYGP-UHFFFAOYSA-N 0.000 description 2
- 239000000292 calcium oxide Substances 0.000 description 2
- ODINCKMPIJJUCX-UHFFFAOYSA-N calcium oxide Inorganic materials [Ca]=O ODINCKMPIJJUCX-UHFFFAOYSA-N 0.000 description 2
- OSGAYBCDTDRGGQ-UHFFFAOYSA-L calcium sulfate Chemical compound [Ca+2].[O-]S([O-])(=O)=O OSGAYBCDTDRGGQ-UHFFFAOYSA-L 0.000 description 2
- 150000001768 cations Chemical class 0.000 description 2
- 150000001875 compounds Chemical class 0.000 description 2
- 238000004455 differential thermal analysis Methods 0.000 description 2
- NXPHCVPFHOVZBC-UHFFFAOYSA-N hydroxylamine;sulfuric acid Chemical compound ON.OS(O)(=O)=O NXPHCVPFHOVZBC-UHFFFAOYSA-N 0.000 description 2
- 229910021645 metal ion Inorganic materials 0.000 description 2
- 239000007769 metal material Substances 0.000 description 2
- WQGWDDDVZFFDIG-UHFFFAOYSA-N pyrogallol Chemical compound OC1=CC=CC(O)=C1O WQGWDDDVZFFDIG-UHFFFAOYSA-N 0.000 description 2
- 239000002002 slurry Substances 0.000 description 2
- IATRAKWUXMZMIY-UHFFFAOYSA-N strontium oxide Chemical compound [O-2].[Sr+2] IATRAKWUXMZMIY-UHFFFAOYSA-N 0.000 description 2
- 238000004065 wastewater treatment Methods 0.000 description 2
- GOUILHYTHSOMQJ-UHFFFAOYSA-N 2(5H)-Furanone,5-ethyl Chemical compound CCC1OC(=O)C=C1 GOUILHYTHSOMQJ-UHFFFAOYSA-N 0.000 description 1
- SLRMQYXOBQWXCR-UHFFFAOYSA-N 2154-56-5 Chemical compound [CH2]C1=CC=CC=C1 SLRMQYXOBQWXCR-UHFFFAOYSA-N 0.000 description 1
- NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 1
- VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 1
- KCXVZYZYPLLWCC-UHFFFAOYSA-N EDTA Chemical class OC(=O)CN(CC(O)=O)CCN(CC(O)=O)CC(O)=O KCXVZYZYPLLWCC-UHFFFAOYSA-N 0.000 description 1
- 206010020751 Hypersensitivity Diseases 0.000 description 1
- YXOLAZRVSSWPPT-UHFFFAOYSA-N Morin Chemical compound OC1=CC(O)=CC=C1C1=C(O)C(=O)C2=C(O)C=C(O)C=C2O1 YXOLAZRVSSWPPT-UHFFFAOYSA-N 0.000 description 1
- FULZLIGZKMKICU-UHFFFAOYSA-N N-phenylthiourea Chemical compound NC(=S)NC1=CC=CC=C1 FULZLIGZKMKICU-UHFFFAOYSA-N 0.000 description 1
- 239000002253 acid Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- 229910052783 alkali metal Inorganic materials 0.000 description 1
- 229910052784 alkaline earth metal Inorganic materials 0.000 description 1
- 125000002947 alkylene group Chemical group 0.000 description 1
- 230000007815 allergy Effects 0.000 description 1
- 229910000147 aluminium phosphate Inorganic materials 0.000 description 1
- 235000011114 ammonium hydroxide Nutrition 0.000 description 1
- 239000008346 aqueous phase Substances 0.000 description 1
- 150000001553 barium compounds Chemical class 0.000 description 1
- MXOQNVMDKHLYCZ-UHFFFAOYSA-N benzamidoxime Chemical compound ON=C(N)C1=CC=CC=C1 MXOQNVMDKHLYCZ-UHFFFAOYSA-N 0.000 description 1
- 239000012267 brine Substances 0.000 description 1
- 239000000919 ceramic Substances 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 125000002993 cycloalkylene group Chemical group 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 239000012153 distilled water Substances 0.000 description 1
- 238000000909 electrodialysis Methods 0.000 description 1
- 238000005868 electrolysis reaction Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- IFQUWYZCAGRUJN-UHFFFAOYSA-N ethylenediaminediacetic acid Chemical compound OC(=O)CNCCNCC(O)=O IFQUWYZCAGRUJN-UHFFFAOYSA-N 0.000 description 1
- 238000001704 evaporation Methods 0.000 description 1
- 230000008020 evaporation Effects 0.000 description 1
- 239000002360 explosive Substances 0.000 description 1
- 239000012527 feed solution Substances 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 229930003944 flavone Natural products 0.000 description 1
- 150000002213 flavones Chemical class 0.000 description 1
- 235000011949 flavones Nutrition 0.000 description 1
- NILJXUMQIIUAFY-UHFFFAOYSA-N hydroxylamine;nitric acid Chemical compound ON.O[N+]([O-])=O NILJXUMQIIUAFY-UHFFFAOYSA-N 0.000 description 1
- QFUVRXBMUCPEMV-UHFFFAOYSA-N hydroxythiourea Chemical compound NC(=S)NO QFUVRXBMUCPEMV-UHFFFAOYSA-N 0.000 description 1
- 238000009776 industrial production Methods 0.000 description 1
- 150000007529 inorganic bases Chemical class 0.000 description 1
- 229910052500 inorganic mineral Inorganic materials 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 210000004379 membrane Anatomy 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 239000011707 mineral Substances 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 125000000896 monocarboxylic acid group Chemical group 0.000 description 1
- UXOUKMQIEVGVLY-UHFFFAOYSA-N morin Natural products OC1=CC(O)=CC(C2=C(C(=O)C3=C(O)C=C(O)C=C3O2)O)=C1 UXOUKMQIEVGVLY-UHFFFAOYSA-N 0.000 description 1
- 235000007708 morin Nutrition 0.000 description 1
- 210000004400 mucous membrane Anatomy 0.000 description 1
- 125000001997 phenyl group Chemical group [H]C1=C([H])C([H])=C(*)C([H])=C1[H] 0.000 description 1
- 239000004033 plastic Substances 0.000 description 1
- 229920000333 poly(propyleneimine) Polymers 0.000 description 1
- 150000008442 polyphenolic compounds Polymers 0.000 description 1
- 239000012716 precipitator Substances 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 229940079877 pyrogallol Drugs 0.000 description 1
- VBHKTXLEJZIDJF-UHFFFAOYSA-N quinalizarin Chemical compound C1=CC(O)=C2C(=O)C3=C(O)C(O)=CC=C3C(=O)C2=C1O VBHKTXLEJZIDJF-UHFFFAOYSA-N 0.000 description 1
- HREHOXSRYOZKNT-UHFFFAOYSA-N quinolin-2-ylmethanol Chemical class C1=CC=CC2=NC(CO)=CC=C21 HREHOXSRYOZKNT-UHFFFAOYSA-N 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000012216 screening Methods 0.000 description 1
- 239000011734 sodium Substances 0.000 description 1
- HPALAKNZSZLMCH-UHFFFAOYSA-M sodium;chloride;hydrate Chemical compound O.[Na+].[Cl-] HPALAKNZSZLMCH-UHFFFAOYSA-M 0.000 description 1
- FNXKBSAUKFCXIK-UHFFFAOYSA-M sodium;hydrogen carbonate;8-hydroxy-7-iodoquinoline-5-sulfonic acid Chemical class [Na+].OC([O-])=O.C1=CN=C2C(O)=C(I)C=C(S(O)(=O)=O)C2=C1 FNXKBSAUKFCXIK-UHFFFAOYSA-M 0.000 description 1
- 239000007787 solid Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 150000003438 strontium compounds Chemical class 0.000 description 1
- 150000003467 sulfuric acid derivatives Chemical class 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 239000002351 wastewater Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1409—Preparation
- C01B21/1445—Preparation of hydoxylamine from its salts
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/143—Fractional distillation or use of a fractionation or rectification column by two or more of a fractionation, separation or rectification step
- B01D3/146—Multiple effect distillation
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/34—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping with one or more auxiliary substances
- B01D3/38—Steam distillation
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1463—Concentration
-
- C—CHEMISTRY; METALLURGY
- C01—INORGANIC CHEMISTRY
- C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
- C01B21/00—Nitrogen; Compounds thereof
- C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
- C01B21/14—Hydroxylamine; Salts thereof
- C01B21/1472—Separation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Inorganic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Vaporization, Distillation, Condensation, Sublimation, And Cold Traps (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Compounds Of Unknown Constitution (AREA)
- Seasonings (AREA)
- Gas Separation By Absorption (AREA)
- Extraction Or Liquid Replacement (AREA)
- Disintegrating Or Milling (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19547758 | 1995-12-20 | ||
| US08/688,281 US5837107A (en) | 1995-12-20 | 1996-07-29 | Process for production of aqueous solutions of free hydroxylamine |
| PCT/EP1996/005773 WO1997022551A1 (fr) | 1995-12-20 | 1996-12-20 | Procede de preparation de solutions aqueuses d'hydroxylamine libre |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO982847D0 NO982847D0 (no) | 1998-06-19 |
| NO982847L NO982847L (no) | 1998-08-17 |
| NO319309B1 true NO319309B1 (no) | 2005-07-11 |
Family
ID=26021480
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO19982847A NO319309B1 (no) | 1995-12-20 | 1998-06-19 | Fremgangsmate for fremstilling av en vandig losning av fritt hydroksylamin |
| NO19982849A NO322631B1 (no) | 1995-12-20 | 1998-06-19 | Fremgangsmate for separering av middels hoytkokende fraksjoner fra en blanding av lavt-, middels- og hoytkokende fraksjoner |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO19982849A NO322631B1 (no) | 1995-12-20 | 1998-06-19 | Fremgangsmate for separering av middels hoytkokende fraksjoner fra en blanding av lavt-, middels- og hoytkokende fraksjoner |
Country Status (16)
| Country | Link |
|---|---|
| EP (2) | EP0868398B1 (fr) |
| JP (2) | JP2000505033A (fr) |
| CN (2) | CN1102531C (fr) |
| AT (1) | ATE222565T1 (fr) |
| AU (2) | AU707648B2 (fr) |
| BR (2) | BR9612053A (fr) |
| CA (2) | CA2239791C (fr) |
| DE (2) | DE59609239D1 (fr) |
| DK (1) | DK0868399T3 (fr) |
| ES (2) | ES2177828T3 (fr) |
| HR (1) | HRP960601B1 (fr) |
| IL (2) | IL124737A (fr) |
| NO (2) | NO319309B1 (fr) |
| PT (1) | PT868399E (fr) |
| TR (2) | TR199801154T2 (fr) |
| WO (2) | WO1997022550A1 (fr) |
Families Citing this family (29)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE19725851A1 (de) * | 1997-06-18 | 1998-12-24 | Basf Ag | Verfahren zur Herstellung hochreiner, wässriger Hydroxylaminlösungen |
| US5788946A (en) * | 1997-07-16 | 1998-08-04 | Ashland Inc. | Purification of hydroxylamine |
| DE19733681A1 (de) | 1997-08-04 | 1999-02-11 | Basf Ag | Verfahren zur Herstellung einer wäßrigen Lösung von freiem Hydroxylamin |
| DE19806578A1 (de) | 1998-02-17 | 1999-08-19 | Basf Ag | Verfahren zur Herstellung wäßriger, im wesentlichen metallionenfreier Hydroxylaminlösungen |
| US6235162B1 (en) | 1998-05-28 | 2001-05-22 | Sachem, Inc. | Ultrapure hydroxylamine compound solutions and process of making same |
| DE19936594A1 (de) | 1999-08-04 | 2001-02-08 | Basf Ag | Verfahren zur Herstellung von hochreinen stabilisierten Hydroxylaminlösungen |
| DE10004818A1 (de) * | 2000-02-04 | 2001-08-09 | Basf Ag | Verfahren zum Recycling hydroxylaminhaltiger Stripperlösungen |
| JP3503115B2 (ja) * | 2000-06-27 | 2004-03-02 | 東レ・ファインケミカル株式会社 | フリーヒドロキシルアミン水溶液の製造方法 |
| DE10037774A1 (de) * | 2000-08-03 | 2002-02-14 | Bayer Ag | Verfahren und Vorrichtung zur Gewinnung organischer Substanzen aus einem diese Substanzen enthaltenden Gasgemisch |
| DE10131788A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
| DE10134389A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
| DE10131787A1 (de) * | 2001-07-04 | 2003-01-16 | Basf Ag | Verfahren zur Herstellung einer salzfreien, wässrigen Hydroxylaminlösung |
| DE10314492B4 (de) * | 2003-03-27 | 2008-10-16 | Domo Caproleuna Gmbh | Verfahren zur Herstellung einer wässrigen Lösung von Hydroxylamin |
| TW200508176A (en) * | 2003-08-13 | 2005-03-01 | Showa Denko Kk | Process for producing hydroxylamine |
| WO2005016817A2 (fr) | 2003-08-13 | 2005-02-24 | Showa Denko K. K. | Procede de production d'hydroxylamine |
| JP4578885B2 (ja) * | 2003-08-13 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
| FR2860223B1 (fr) * | 2003-09-26 | 2005-12-16 | Jean Pierre Schirmann | Procede de fabrication de solutions aqueuses d'hydroxylamine base |
| US7396519B2 (en) | 2004-01-26 | 2008-07-08 | San Fu Chemical Company, Ltd. | Preparation of a high purity and high concentration hydroxylamine free base |
| JP2005239702A (ja) * | 2004-01-28 | 2005-09-08 | Showa Denko Kk | ヒドロキシルアミンの製造方法 |
| JP2006056742A (ja) * | 2004-08-19 | 2006-03-02 | Hosoya Fireworks Co Ltd | 硝酸ヒドロキシルアミン水溶液の製造方法 |
| JP4578988B2 (ja) * | 2005-01-21 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
| JP4578999B2 (ja) * | 2005-02-10 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
| JP4578998B2 (ja) * | 2005-02-10 | 2010-11-10 | 昭和電工株式会社 | ヒドロキシルアミンの製造方法 |
| JP2006219343A (ja) * | 2005-02-10 | 2006-08-24 | Showa Denko Kk | ヒドロキシルアミンの製造方法 |
| DE102005032430A1 (de) * | 2005-07-12 | 2007-01-25 | Bayer Materialscience Ag | Verfahren zur Herstellung von Toluylendiamin |
| US11014883B2 (en) | 2016-05-26 | 2021-05-25 | Exxonmobil Chemical Patents Inc. | Production of cyclic imides suitable for oxidation catalysis |
| WO2017204935A1 (fr) | 2016-05-26 | 2017-11-30 | Exxonmobil Chemical Patents Inc. | Production d'imides cycliques appropriés pour la catalyse d'oxydation |
| US10584096B2 (en) | 2016-10-18 | 2020-03-10 | Exxonmobil Chemical Patents Inc. | Cyclic imide slurry compositions |
| CN108946741B (zh) * | 2017-05-17 | 2020-05-12 | 新特能源股份有限公司 | 多晶硅冷氢化工艺中的含硅高沸物的回收工艺方法及冷氢化工艺 |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US4111759A (en) * | 1976-07-08 | 1978-09-05 | United States Steel Corporation | Process for separating ammonia and acid gases from waste waters containing fixed ammonia salts |
| JPS597313B2 (ja) * | 1980-02-08 | 1984-02-17 | チツソエンジニアリング株式会社 | アルコ−ルの蒸溜装置 |
| DE3302525A1 (de) * | 1983-01-26 | 1984-07-26 | Basf Ag, 6700 Ludwigshafen | Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes |
| DE3528463A1 (de) * | 1985-08-08 | 1987-02-19 | Basf Ag | Verfahren zur herstellung von waessrigen loesungen von freiem hydroxylamin |
| DE3814255A1 (de) * | 1988-04-27 | 1989-11-09 | Metallgesellschaft Ag | Vorrichtung zum desodorieren von organischen fluessigkeiten |
| US5266290A (en) * | 1992-07-10 | 1993-11-30 | Thiokol Corporation | Process for making high purity hydroxylammonium nitrate |
| DE4324410C1 (de) * | 1993-07-21 | 1994-08-04 | Enviro Consult Ingenieurgesell | Verfahren zum Entfernen von Ammonium aus dem Zentratwasser einer biologischen Abwasserreinigungsanlage |
| US5385646A (en) * | 1993-09-03 | 1995-01-31 | Farmland Industries, Inc. | Method of treating chemical process effluent |
-
1996
- 1996-12-19 HR HR960601A patent/HRP960601B1/xx not_active IP Right Cessation
- 1996-12-20 ES ES96944615T patent/ES2177828T3/es not_active Expired - Lifetime
- 1996-12-20 CN CN96199954A patent/CN1102531C/zh not_active Expired - Lifetime
- 1996-12-20 PT PT96944616T patent/PT868399E/pt unknown
- 1996-12-20 AT AT96944616T patent/ATE222565T1/de active
- 1996-12-20 AU AU13040/97A patent/AU707648B2/en not_active Expired
- 1996-12-20 EP EP96944615A patent/EP0868398B1/fr not_active Expired - Lifetime
- 1996-12-20 EP EP96944616A patent/EP0868399B1/fr not_active Expired - Lifetime
- 1996-12-20 BR BR9612053A patent/BR9612053A/pt not_active IP Right Cessation
- 1996-12-20 CA CA002239791A patent/CA2239791C/fr not_active Expired - Lifetime
- 1996-12-20 AU AU13039/97A patent/AU704998B2/en not_active Expired
- 1996-12-20 BR BR9612073A patent/BR9612073A/pt not_active IP Right Cessation
- 1996-12-20 IL IL12473796A patent/IL124737A/en not_active IP Right Cessation
- 1996-12-20 CA CA002239253A patent/CA2239253C/fr not_active Expired - Lifetime
- 1996-12-20 JP JP9522524A patent/JP2000505033A/ja active Pending
- 1996-12-20 WO PCT/EP1996/005772 patent/WO1997022550A1/fr active IP Right Grant
- 1996-12-20 IL IL12473996A patent/IL124739A/en not_active IP Right Cessation
- 1996-12-20 ES ES96944616T patent/ES2181933T3/es not_active Expired - Lifetime
- 1996-12-20 CN CN96199143A patent/CN1104376C/zh not_active Expired - Lifetime
- 1996-12-20 TR TR1998/01154T patent/TR199801154T2/xx unknown
- 1996-12-20 DE DE59609239T patent/DE59609239D1/de not_active Expired - Lifetime
- 1996-12-20 TR TR1998/01163T patent/TR199801163T2/xx unknown
- 1996-12-20 DE DE59609580T patent/DE59609580D1/de not_active Expired - Lifetime
- 1996-12-20 DK DK96944616T patent/DK0868399T3/da active
- 1996-12-20 WO PCT/EP1996/005773 patent/WO1997022551A1/fr active IP Right Grant
- 1996-12-20 JP JP52252397A patent/JP4376969B2/ja not_active Expired - Lifetime
-
1998
- 1998-06-19 NO NO19982847A patent/NO319309B1/no not_active IP Right Cessation
- 1998-06-19 NO NO19982849A patent/NO322631B1/no not_active IP Right Cessation
Also Published As
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| NO319309B1 (no) | Fremgangsmate for fremstilling av en vandig losning av fritt hydroksylamin | |
| US5837107A (en) | Process for production of aqueous solutions of free hydroxylamine | |
| US6299734B1 (en) | Preparation of an aqueous solution of free hydroxylamine | |
| JPH07115849B2 (ja) | 遊離ヒドロキシルアミン水溶液の製造方法 | |
| US6153799A (en) | Method for producing highly pure aqueous hydroxylamine solutions | |
| KR100887259B1 (ko) | 염을 함유하지 않는 히드록실아민 수용액의 제조 방법 | |
| MXPA98004788A (en) | Preparation of aqueous solutions of hydroxylamine li | |
| US7425247B2 (en) | Method for producing an aqueous solution hydroxylamine | |
| MXPA99011383A (en) | Method for producing highly pure aqueous hydroxylamine solutions | |
| US4138559A (en) | Recovery of chlorine and cyanuric acid values from polychloroisocyanuric acids and salts thereof | |
| MXPA00000993A (en) | Method for producing an aqueous solution of free hydroxylamine | |
| JP2004533392A (ja) | 無塩ヒドロキシルアミン水溶液の製造方法 | |
| WO1984002898A1 (fr) | Purification d'hydroxydes de metaux alcalins | |
| RU2256606C1 (ru) | Способ получения водного раствора гидроксиламина | |
| MXPA03011366A (es) | Procedimiento para obtencion de una solucion de hidroxilamina acuosa, exentade sal. | |
| EP0134208A4 (fr) | Purification d'hydroxydes de metaux alcalins. |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| MK1K | Patent expired |