NO311594B1 - Fremgangsmåte for kromatografisk analyse av hydrokarboner, og fremgangsmåte for raffinering av en petroleumhydrokarbontilförsel - Google Patents
Fremgangsmåte for kromatografisk analyse av hydrokarboner, og fremgangsmåte for raffinering av en petroleumhydrokarbontilförsel Download PDFInfo
- Publication number
- NO311594B1 NO311594B1 NO19902324A NO902324A NO311594B1 NO 311594 B1 NO311594 B1 NO 311594B1 NO 19902324 A NO19902324 A NO 19902324A NO 902324 A NO902324 A NO 902324A NO 311594 B1 NO311594 B1 NO 311594B1
- Authority
- NO
- Norway
- Prior art keywords
- solvent
- aromatic
- aromatics
- polar
- stationary phase
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims description 121
- 229930195733 hydrocarbon Natural products 0.000 title claims description 64
- 150000002430 hydrocarbons Chemical class 0.000 title claims description 64
- 238000004587 chromatography analysis Methods 0.000 title claims description 28
- 230000008569 process Effects 0.000 title claims description 27
- 238000007670 refining Methods 0.000 title claims description 21
- 239000003209 petroleum derivative Substances 0.000 title claims description 9
- 239000002904 solvent Substances 0.000 claims description 155
- 125000003118 aryl group Chemical group 0.000 claims description 92
- 150000001875 compounds Chemical class 0.000 claims description 62
- 239000004215 Carbon black (E152) Substances 0.000 claims description 59
- 230000005526 G1 to G0 transition Effects 0.000 claims description 51
- 239000000203 mixture Substances 0.000 claims description 47
- 238000002835 absorbance Methods 0.000 claims description 42
- 239000001257 hydrogen Substances 0.000 claims description 29
- 229910052739 hydrogen Inorganic materials 0.000 claims description 29
- 229920006395 saturated elastomer Polymers 0.000 claims description 25
- 239000000126 substance Substances 0.000 claims description 24
- 238000010828 elution Methods 0.000 claims description 22
- 238000010521 absorption reaction Methods 0.000 claims description 16
- 238000012544 monitoring process Methods 0.000 claims description 14
- 238000012546 transfer Methods 0.000 claims description 6
- 238000009826 distribution Methods 0.000 claims description 5
- -1 aminopropyl Chemical group 0.000 claims description 4
- 125000002887 hydroxy group Chemical group [H]O* 0.000 claims description 4
- 230000001678 irradiating effect Effects 0.000 claims description 3
- JOERSAVCLPYNIZ-UHFFFAOYSA-N 2,4,5,7-tetranitrofluoren-9-one Chemical compound O=C1C2=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C2C2=C1C=C([N+](=O)[O-])C=C2[N+]([O-])=O JOERSAVCLPYNIZ-UHFFFAOYSA-N 0.000 claims description 2
- 238000011112 process operation Methods 0.000 claims description 2
- DIAYUOIZRJQFTN-UHFFFAOYSA-N 2-(1,1,2,2-tetrachloropropyl)isoindole-1,3-dione Chemical compound C1=CC=C2C(=O)N(C(Cl)(Cl)C(Cl)(Cl)C)C(=O)C2=C1 DIAYUOIZRJQFTN-UHFFFAOYSA-N 0.000 claims 1
- ZQWKEKVAVFYMDI-UHFFFAOYSA-N 3,3-dinitro-2-(oxiran-2-ylmethyl)-1-phenylbutan-1-one Chemical compound [N+](=O)([O-])C(C(CC1CO1)C(C1=CC=CC=C1)=O)(C)[N+](=O)[O-] ZQWKEKVAVFYMDI-UHFFFAOYSA-N 0.000 claims 1
- 239000003921 oil Substances 0.000 description 75
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 description 51
- 239000000523 sample Substances 0.000 description 51
- 239000000463 material Substances 0.000 description 38
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 description 36
- 238000004128 high performance liquid chromatography Methods 0.000 description 30
- UFHFLCQGNIYNRP-UHFFFAOYSA-N Hydrogen Chemical compound [H][H] UFHFLCQGNIYNRP-UHFFFAOYSA-N 0.000 description 27
- 230000004044 response Effects 0.000 description 26
- 239000007789 gas Substances 0.000 description 25
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 21
- 239000000243 solution Substances 0.000 description 21
- 238000000926 separation method Methods 0.000 description 20
- 238000004458 analytical method Methods 0.000 description 18
- 239000003480 eluent Substances 0.000 description 18
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 description 17
- 239000002994 raw material Substances 0.000 description 17
- MWPLVEDNUUSJAV-UHFFFAOYSA-N anthracene Chemical compound C1=CC=CC2=CC3=CC=CC=C3C=C21 MWPLVEDNUUSJAV-UHFFFAOYSA-N 0.000 description 16
- 238000000149 argon plasma sintering Methods 0.000 description 15
- 230000008859 change Effects 0.000 description 15
- 230000006870 function Effects 0.000 description 15
- 239000000047 product Substances 0.000 description 15
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 14
- 238000004821 distillation Methods 0.000 description 14
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 description 14
- 238000011084 recovery Methods 0.000 description 14
- 150000001491 aromatic compounds Chemical class 0.000 description 13
- 238000002347 injection Methods 0.000 description 13
- 239000007924 injection Substances 0.000 description 13
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 12
- 230000008033 biological extinction Effects 0.000 description 12
- 229910052799 carbon Inorganic materials 0.000 description 12
- 230000003197 catalytic effect Effects 0.000 description 12
- VPUGDVKSAQVFFS-UHFFFAOYSA-N coronene Chemical compound C1=C(C2=C34)C=CC3=CC=C(C=C3)C4=C4C3=CC=C(C=C3)C4=C2C3=C1 VPUGDVKSAQVFFS-UHFFFAOYSA-N 0.000 description 12
- 239000007787 solid Substances 0.000 description 12
- 230000000875 corresponding effect Effects 0.000 description 10
- 238000005984 hydrogenation reaction Methods 0.000 description 10
- 230000014759 maintenance of location Effects 0.000 description 10
- 238000004519 manufacturing process Methods 0.000 description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 9
- 238000001514 detection method Methods 0.000 description 9
- 238000009835 boiling Methods 0.000 description 8
- 238000004523 catalytic cracking Methods 0.000 description 8
- 150000002390 heteroarenes Chemical class 0.000 description 8
- 239000003463 adsorbent Substances 0.000 description 7
- 238000005336 cracking Methods 0.000 description 7
- 239000012530 fluid Substances 0.000 description 7
- 238000006467 substitution reaction Methods 0.000 description 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
- 150000004945 aromatic hydrocarbons Chemical class 0.000 description 6
- 230000008901 benefit Effects 0.000 description 6
- 230000006872 improvement Effects 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 238000004811 liquid chromatography Methods 0.000 description 6
- 239000010687 lubricating oil Substances 0.000 description 6
- 238000002156 mixing Methods 0.000 description 6
- 239000003208 petroleum Substances 0.000 description 6
- 239000002798 polar solvent Substances 0.000 description 6
- 230000002829 reductive effect Effects 0.000 description 6
- 230000000717 retained effect Effects 0.000 description 6
- 239000000377 silicon dioxide Substances 0.000 description 6
- 238000001228 spectrum Methods 0.000 description 6
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 5
- QGJOPFRUJISHPQ-UHFFFAOYSA-N Carbon disulfide Chemical compound S=C=S QGJOPFRUJISHPQ-UHFFFAOYSA-N 0.000 description 5
- NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 5
- 239000010426 asphalt Substances 0.000 description 5
- 230000033228 biological regulation Effects 0.000 description 5
- 239000003054 catalyst Substances 0.000 description 5
- 238000009903 catalytic hydrogenation reaction Methods 0.000 description 5
- 239000013067 intermediate product Substances 0.000 description 5
- 239000011347 resin Substances 0.000 description 5
- 229920005989 resin Polymers 0.000 description 5
- 229930195734 saturated hydrocarbon Natural products 0.000 description 5
- 238000005292 vacuum distillation Methods 0.000 description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 description 4
- 238000005481 NMR spectroscopy Methods 0.000 description 4
- ATUOYWHBWRKTHZ-UHFFFAOYSA-N Propane Chemical compound CCC ATUOYWHBWRKTHZ-UHFFFAOYSA-N 0.000 description 4
- 125000000217 alkyl group Chemical group 0.000 description 4
- WDECIBYCCFPHNR-UHFFFAOYSA-N chrysene Chemical compound C1=CC=CC2=CC=C3C4=CC=CC=C4C=CC3=C21 WDECIBYCCFPHNR-UHFFFAOYSA-N 0.000 description 4
- 239000000571 coke Substances 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 238000005194 fractionation Methods 0.000 description 4
- 125000005842 heteroatom Chemical group 0.000 description 4
- YNPNZTXNASCQKK-UHFFFAOYSA-N phenanthrene Chemical compound C1=CC=C2C3=CC=CC=C3C=CC2=C1 YNPNZTXNASCQKK-UHFFFAOYSA-N 0.000 description 4
- 230000005855 radiation Effects 0.000 description 4
- 238000005070 sampling Methods 0.000 description 4
- 238000000935 solvent evaporation Methods 0.000 description 4
- 229910052717 sulfur Inorganic materials 0.000 description 4
- 239000011593 sulfur Substances 0.000 description 4
- 238000012360 testing method Methods 0.000 description 4
- 238000000870 ultraviolet spectroscopy Methods 0.000 description 4
- 238000002211 ultraviolet spectrum Methods 0.000 description 4
- 238000011144 upstream manufacturing Methods 0.000 description 4
- UFWIBTONFRDIAS-UHFFFAOYSA-N Naphthalene Chemical group C1=CC=CC2=CC=CC=C21 UFWIBTONFRDIAS-UHFFFAOYSA-N 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 3
- 238000004939 coking Methods 0.000 description 3
- 230000007423 decrease Effects 0.000 description 3
- 230000003247 decreasing effect Effects 0.000 description 3
- 238000001704 evaporation Methods 0.000 description 3
- 230000008020 evaporation Effects 0.000 description 3
- 238000005259 measurement Methods 0.000 description 3
- 230000004048 modification Effects 0.000 description 3
- 238000012986 modification Methods 0.000 description 3
- 229910052757 nitrogen Inorganic materials 0.000 description 3
- 230000036961 partial effect Effects 0.000 description 3
- 125000003367 polycyclic group Chemical group 0.000 description 3
- 238000004611 spectroscopical analysis Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- OFBQJSOFQDEBGM-UHFFFAOYSA-N Pentane Chemical compound CCCCC OFBQJSOFQDEBGM-UHFFFAOYSA-N 0.000 description 2
- YTPLMLYBLZKORZ-UHFFFAOYSA-N Thiophene Chemical compound C=1C=CSC=1 YTPLMLYBLZKORZ-UHFFFAOYSA-N 0.000 description 2
- 239000000356 contaminant Substances 0.000 description 2
- DIOQZVSQGTUSAI-UHFFFAOYSA-N decane Chemical compound CCCCCCCCCC DIOQZVSQGTUSAI-UHFFFAOYSA-N 0.000 description 2
- 230000001419 dependent effect Effects 0.000 description 2
- 230000001627 detrimental effect Effects 0.000 description 2
- 238000010586 diagram Methods 0.000 description 2
- IYYZUPMFVPLQIF-UHFFFAOYSA-N dibenzothiophene Chemical compound C1=CC=C2C3=CC=CC=C3SC2=C1 IYYZUPMFVPLQIF-UHFFFAOYSA-N 0.000 description 2
- ZUOUZKKEUPVFJK-UHFFFAOYSA-N diphenyl Chemical compound C1=CC=CC=C1C1=CC=CC=C1 ZUOUZKKEUPVFJK-UHFFFAOYSA-N 0.000 description 2
- SNRUBQQJIBEYMU-UHFFFAOYSA-N dodecane Chemical compound CCCCCCCCCCCC SNRUBQQJIBEYMU-UHFFFAOYSA-N 0.000 description 2
- 230000005274 electronic transitions Effects 0.000 description 2
- 238000000105 evaporative light scattering detection Methods 0.000 description 2
- 238000000605 extraction Methods 0.000 description 2
- GVEPBJHOBDJJJI-UHFFFAOYSA-N fluoranthene Chemical compound C1=CC(C2=CC=CC=C22)=C3C2=CC=CC3=C1 GVEPBJHOBDJJJI-UHFFFAOYSA-N 0.000 description 2
- 238000011010 flushing procedure Methods 0.000 description 2
- 239000000295 fuel oil Substances 0.000 description 2
- 238000007306 functionalization reaction Methods 0.000 description 2
- DCAYPVUWAIABOU-UHFFFAOYSA-N hexadecane Chemical compound CCCCCCCCCCCCCCCC DCAYPVUWAIABOU-UHFFFAOYSA-N 0.000 description 2
- CBFCDTFDPHXCNY-UHFFFAOYSA-N icosane Chemical compound CCCCCCCCCCCCCCCCCCCC CBFCDTFDPHXCNY-UHFFFAOYSA-N 0.000 description 2
- UAEPNZWRGJTJPN-UHFFFAOYSA-N methylcyclohexane Chemical compound CC1CCCCC1 UAEPNZWRGJTJPN-UHFFFAOYSA-N 0.000 description 2
- 238000012856 packing Methods 0.000 description 2
- 239000002245 particle Substances 0.000 description 2
- 238000001556 precipitation Methods 0.000 description 2
- 238000004886 process control Methods 0.000 description 2
- 238000012545 processing Methods 0.000 description 2
- 230000000750 progressive effect Effects 0.000 description 2
- 238000011002 quantification Methods 0.000 description 2
- 238000000611 regression analysis Methods 0.000 description 2
- 230000001105 regulatory effect Effects 0.000 description 2
- 230000002441 reversible effect Effects 0.000 description 2
- 238000012163 sequencing technique Methods 0.000 description 2
- 239000003079 shale oil Substances 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 239000011800 void material Substances 0.000 description 2
- XIIAYQZJNBULGD-UHFFFAOYSA-N (5alpha)-cholestane Natural products C1CC2CCCCC2(C)C2C1C1CCC(C(C)CCCC(C)C)C1(C)CC2 XIIAYQZJNBULGD-UHFFFAOYSA-N 0.000 description 1
- ODHYDPYRIQKHCI-UHFFFAOYSA-N 1,2,3,4,5,6,7,8,9,10,11,12-dodecahydrotriphenylene Chemical group C1CCCC2=C1C(CCCC1)=C1C1=C2CCCC1 ODHYDPYRIQKHCI-UHFFFAOYSA-N 0.000 description 1
- DXBHBZVCASKNBY-UHFFFAOYSA-N 1,2-Benz(a)anthracene Chemical compound C1=CC=C2C3=CC4=CC=CC=C4C=C3C=CC2=C1 DXBHBZVCASKNBY-UHFFFAOYSA-N 0.000 description 1
- CIWBSHSKHKDKBQ-JLAZNSOCSA-N Ascorbic acid Chemical compound OC[C@H](O)[C@H]1OC(=O)C(O)=C1O CIWBSHSKHKDKBQ-JLAZNSOCSA-N 0.000 description 1
- 101150080661 Ear1 gene Proteins 0.000 description 1
- 241000084490 Esenbeckia delta Species 0.000 description 1
- 241000282326 Felis catus Species 0.000 description 1
- 101000613565 Homo sapiens PRKC apoptosis WT1 regulator protein Proteins 0.000 description 1
- 101001113471 Homo sapiens Proteinase-activated receptor 4 Proteins 0.000 description 1
- BZLVMXJERCGZMT-UHFFFAOYSA-N Methyl tert-butyl ether Chemical compound COC(C)(C)C BZLVMXJERCGZMT-UHFFFAOYSA-N 0.000 description 1
- 101150081376 NR1D1 gene Proteins 0.000 description 1
- 102100023170 Nuclear receptor subfamily 1 group D member 1 Human genes 0.000 description 1
- CTQNGGLPUBDAKN-UHFFFAOYSA-N O-Xylene Chemical compound CC1=CC=CC=C1C CTQNGGLPUBDAKN-UHFFFAOYSA-N 0.000 description 1
- 102100032341 PCNA-interacting partner Human genes 0.000 description 1
- 101710196737 PCNA-interacting partner Proteins 0.000 description 1
- ISWSIDIOOBJBQZ-UHFFFAOYSA-N Phenol Chemical compound OC1=CC=CC=C1 ISWSIDIOOBJBQZ-UHFFFAOYSA-N 0.000 description 1
- 102100023710 Proteinase-activated receptor 4 Human genes 0.000 description 1
- 101000603960 Rattus norvegicus Nuclear receptor subfamily 1 group D member 2 Proteins 0.000 description 1
- 229910000831 Steel Inorganic materials 0.000 description 1
- 239000005864 Sulphur Substances 0.000 description 1
- 238000004847 absorption spectroscopy Methods 0.000 description 1
- 238000000862 absorption spectrum Methods 0.000 description 1
- 125000004054 acenaphthylenyl group Chemical group C1(=CC2=CC=CC3=CC=CC1=C23)* 0.000 description 1
- HXGDTGSAIMULJN-UHFFFAOYSA-N acetnaphthylene Natural products C1=CC(C=C2)=C3C2=CC=CC3=C1 HXGDTGSAIMULJN-UHFFFAOYSA-N 0.000 description 1
- 230000002378 acidificating effect Effects 0.000 description 1
- 230000002411 adverse Effects 0.000 description 1
- 230000002776 aggregation Effects 0.000 description 1
- 238000004220 aggregation Methods 0.000 description 1
- 150000001298 alcohols Chemical class 0.000 description 1
- 150000001336 alkenes Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 239000012491 analyte Substances 0.000 description 1
- 235000019568 aromas Nutrition 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical group [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 238000011001 backwashing Methods 0.000 description 1
- 235000013405 beer Nutrition 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 235000010290 biphenyl Nutrition 0.000 description 1
- 239000004305 biphenyl Substances 0.000 description 1
- 239000006227 byproduct Substances 0.000 description 1
- 238000004364 calculation method Methods 0.000 description 1
- 150000001716 carbazoles Chemical class 0.000 description 1
- 150000001721 carbon Chemical class 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- XIIAYQZJNBULGD-LDHZKLTISA-N cholestane Chemical compound C1CC2CCCC[C@]2(C)[C@@H]2[C@@H]1[C@@H]1CC[C@H]([C@H](C)CCCC(C)C)[C@@]1(C)CC2 XIIAYQZJNBULGD-LDHZKLTISA-N 0.000 description 1
- 238000013375 chromatographic separation Methods 0.000 description 1
- 238000003776 cleavage reaction Methods 0.000 description 1
- 238000002485 combustion reaction Methods 0.000 description 1
- 230000021615 conjugation Effects 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 230000002596 correlated effect Effects 0.000 description 1
- 239000010779 crude oil Substances 0.000 description 1
- 125000004122 cyclic group Chemical group 0.000 description 1
- 125000000113 cyclohexyl group Chemical group [H]C1([H])C([H])([H])C([H])([H])C([H])(*)C([H])([H])C1([H])[H] 0.000 description 1
- 238000013523 data management Methods 0.000 description 1
- 238000009795 derivation Methods 0.000 description 1
- 239000002283 diesel fuel Substances 0.000 description 1
- 238000010790 dilution Methods 0.000 description 1
- 239000012895 dilution Substances 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 238000011067 equilibration Methods 0.000 description 1
- 238000001914 filtration Methods 0.000 description 1
- 238000004508 fractional distillation Methods 0.000 description 1
- 239000000446 fuel Substances 0.000 description 1
- 125000000524 functional group Chemical group 0.000 description 1
- 125000001072 heteroaryl group Chemical group 0.000 description 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 description 1
- 230000000977 initiatory effect Effects 0.000 description 1
- 229910052809 inorganic oxide Inorganic materials 0.000 description 1
- 230000010354 integration Effects 0.000 description 1
- 238000011005 laboratory method Methods 0.000 description 1
- 230000000670 limiting effect Effects 0.000 description 1
- 238000012886 linear function Methods 0.000 description 1
- 238000012417 linear regression Methods 0.000 description 1
- 238000011068 loading method Methods 0.000 description 1
- 230000001050 lubricating effect Effects 0.000 description 1
- 238000007726 management method Methods 0.000 description 1
- 238000004949 mass spectrometry Methods 0.000 description 1
- 238000000691 measurement method Methods 0.000 description 1
- 229910052751 metal Inorganic materials 0.000 description 1
- 239000002184 metal Substances 0.000 description 1
- 150000002739 metals Chemical class 0.000 description 1
- 125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 1
- GYNNXHKOJHMOHS-UHFFFAOYSA-N methyl-cycloheptane Natural products CC1CCCCCC1 GYNNXHKOJHMOHS-UHFFFAOYSA-N 0.000 description 1
- ZGEGCLOFRBLKSE-UHFFFAOYSA-N methylene hexane Natural products CCCCCC=C ZGEGCLOFRBLKSE-UHFFFAOYSA-N 0.000 description 1
- 239000003607 modifier Substances 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- SHWJJBRTHGGZBE-UHFFFAOYSA-N nonadecylbenzene Chemical compound CCCCCCCCCCCCCCCCCCCC1=CC=CC=C1 SHWJJBRTHGGZBE-UHFFFAOYSA-N 0.000 description 1
- 239000010742 number 1 fuel oil Substances 0.000 description 1
- TVMXDCGIABBOFY-UHFFFAOYSA-N octane Chemical compound CCCCCCCC TVMXDCGIABBOFY-UHFFFAOYSA-N 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 238000005457 optimization Methods 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 239000001301 oxygen Chemical group 0.000 description 1
- 229910052760 oxygen Chemical group 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 125000002080 perylenyl group Chemical group C1(=CC=C2C=CC=C3C4=CC=CC5=CC=CC(C1=C23)=C45)* 0.000 description 1
- CSHWQDPOILHKBI-UHFFFAOYSA-N peryrene Natural products C1=CC(C2=CC=CC=3C2=C2C=CC=3)=C3C2=CC=CC3=C1 CSHWQDPOILHKBI-UHFFFAOYSA-N 0.000 description 1
- 238000005504 petroleum refining Methods 0.000 description 1
- 238000005375 photometry Methods 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 238000002360 preparation method Methods 0.000 description 1
- 230000007425 progressive decline Effects 0.000 description 1
- 239000001294 propane Substances 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 238000010992 reflux Methods 0.000 description 1
- 230000008929 regeneration Effects 0.000 description 1
- 238000011069 regeneration method Methods 0.000 description 1
- 230000007017 scission Effects 0.000 description 1
- 125000005372 silanol group Chemical group 0.000 description 1
- 238000004088 simulation Methods 0.000 description 1
- 238000007613 slurry method Methods 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000004071 soot Substances 0.000 description 1
- 238000001179 sorption measurement Methods 0.000 description 1
- 230000003595 spectral effect Effects 0.000 description 1
- 239000010959 steel Substances 0.000 description 1
- 125000000446 sulfanediyl group Chemical group *S* 0.000 description 1
- 239000013589 supplement Substances 0.000 description 1
- CXWXQJXEFPUFDZ-UHFFFAOYSA-N tetralin Chemical compound C1=CC=C2CCCCC2=C1 CXWXQJXEFPUFDZ-UHFFFAOYSA-N 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 229930192474 thiophene Natural products 0.000 description 1
- 238000012384 transportation and delivery Methods 0.000 description 1
- 238000000825 ultraviolet detection Methods 0.000 description 1
- 238000009834 vaporization Methods 0.000 description 1
- 230000008016 vaporization Effects 0.000 description 1
- 238000005303 weighing Methods 0.000 description 1
- 239000008096 xylene Substances 0.000 description 1
Classifications
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/38—Flow patterns
- G01N30/46—Flow patterns using more than one column
- G01N30/461—Flow patterns using more than one column with serial coupling of separation columns
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G11/00—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils
- C10G11/14—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts
- C10G11/18—Catalytic cracking, in the absence of hydrogen, of hydrocarbon oils with preheated moving solid catalysts according to the "fluidised-bed" technique
- C10G11/187—Controlling or regulating
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G21/00—Refining of hydrocarbon oils, in the absence of hydrogen, by extraction with selective solvents
- C10G21/30—Controlling or regulating
-
- C—CHEMISTRY; METALLURGY
- C10—PETROLEUM, GAS OR COKE INDUSTRIES; TECHNICAL GASES CONTAINING CARBON MONOXIDE; FUELS; LUBRICANTS; PEAT
- C10G—CRACKING HYDROCARBON OILS; PRODUCTION OF LIQUID HYDROCARBON MIXTURES, e.g. BY DESTRUCTIVE HYDROGENATION, OLIGOMERISATION, POLYMERISATION; RECOVERY OF HYDROCARBON OILS FROM OIL-SHALE, OIL-SAND, OR GASES; REFINING MIXTURES MAINLY CONSISTING OF HYDROCARBONS; REFORMING OF NAPHTHA; MINERAL WAXES
- C10G69/00—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one other conversion process
- C10G69/02—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one other conversion process plural serial stages only
- C10G69/04—Treatment of hydrocarbon oils by at least one hydrotreatment process and at least one other conversion process plural serial stages only including at least one step of catalytic cracking in the absence of hydrogen
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/62—Detectors specially adapted therefor
- G01N30/74—Optical detectors
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/86—Signal analysis
- G01N30/8675—Evaluation, i.e. decoding of the signal into analytical information
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N33/00—Investigating or analysing materials by specific methods not covered by groups G01N1/00 - G01N31/00
- G01N33/26—Oils; Viscous liquids; Paints; Inks
- G01N33/28—Oils, i.e. hydrocarbon liquids
- G01N33/2829—Mixtures of fuels
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/88—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86
- G01N2030/8809—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample
- G01N2030/884—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds
- G01N2030/8854—Integrated analysis systems specially adapted therefor, not covered by a single one of the groups G01N30/04 - G01N30/86 analysis specially adapted for the sample organic compounds involving hydrocarbons
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N21/00—Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
- G01N21/17—Systems in which incident light is modified in accordance with the properties of the material investigated
- G01N21/25—Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
- G01N21/31—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry
- G01N21/33—Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry using ultraviolet light
-
- G—PHYSICS
- G01—MEASURING; TESTING
- G01N—INVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
- G01N30/00—Investigating or analysing materials by separation into components using adsorption, absorption or similar phenomena or using ion-exchange, e.g. chromatography or field flow fractionation
- G01N30/02—Column chromatography
- G01N30/26—Conditioning of the fluid carrier; Flow patterns
- G01N30/28—Control of physical parameters of the fluid carrier
- G01N30/34—Control of physical parameters of the fluid carrier of fluid composition, e.g. gradient
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/21—Hydrocarbon
- Y10T436/212—Aromatic
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10T—TECHNICAL SUBJECTS COVERED BY FORMER US CLASSIFICATION
- Y10T436/00—Chemistry: analytical and immunological testing
- Y10T436/21—Hydrocarbon
- Y10T436/218—Total hydrocarbon, flammability, combustibility [e.g., air-fuel mixture, etc.]
Landscapes
- Chemical & Material Sciences (AREA)
- Oil, Petroleum & Natural Gas (AREA)
- Engineering & Computer Science (AREA)
- Physics & Mathematics (AREA)
- Health & Medical Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Pathology (AREA)
- General Chemical & Material Sciences (AREA)
- General Physics & Mathematics (AREA)
- Immunology (AREA)
- Biochemistry (AREA)
- Analytical Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Spectroscopy & Molecular Physics (AREA)
- Library & Information Science (AREA)
- Food Science & Technology (AREA)
- Medicinal Chemistry (AREA)
- Investigating Or Analysing Materials By Optical Means (AREA)
- Production Of Liquid Hydrocarbon Mixture For Refining Petroleum (AREA)
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US07/358,779 US4988446A (en) | 1988-05-14 | 1989-05-30 | Method for spectroscopic analysis of hydrocarbons |
Publications (3)
| Publication Number | Publication Date |
|---|---|
| NO902324D0 NO902324D0 (no) | 1990-05-25 |
| NO902324L NO902324L (no) | 1990-12-03 |
| NO311594B1 true NO311594B1 (no) | 2001-12-10 |
Family
ID=23411010
Family Applications (2)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO19902324A NO311594B1 (no) | 1989-05-30 | 1990-05-25 | Fremgangsmåte for kromatografisk analyse av hydrokarboner, og fremgangsmåte for raffinering av en petroleumhydrokarbontilförsel |
| NO973894A NO305921B1 (no) | 1989-05-30 | 1997-08-25 | Fremgangsmåte for kromatografisk analyse av hydrokarbonolje |
Family Applications After (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| NO973894A NO305921B1 (no) | 1989-05-30 | 1997-08-25 | Fremgangsmåte for kromatografisk analyse av hydrokarbonolje |
Country Status (10)
| Country | Link |
|---|---|
| US (1) | US4988446A (ja) |
| EP (1) | EP0400989B1 (ja) |
| JP (2) | JP3073757B2 (ja) |
| AU (1) | AU622082B2 (ja) |
| CA (1) | CA2016222C (ja) |
| DE (1) | DE69030341T2 (ja) |
| ES (1) | ES2100870T3 (ja) |
| GR (1) | GR3023326T3 (ja) |
| MY (1) | MY105829A (ja) |
| NO (2) | NO311594B1 (ja) |
Families Citing this family (52)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US5190882A (en) * | 1990-03-02 | 1993-03-02 | Exxon Research And Engineering Company | Method for quantitatively determining the amount of saturates, olefins, and aromatics in a mixture thereof |
| IL98729A (en) * | 1991-07-04 | 1996-08-04 | Spectronix Ltd | Method and apparatus for detecting hydrocarbon vapours in a monitored area |
| FR2746921B1 (fr) * | 1996-03-29 | 1998-06-26 | Gen Rehabilitation Des Sites | Procede pour l'estimation de la pollution d'un solvant par des hydrocarbures aromatiques polycycliques |
| FR2773219B1 (fr) | 1997-12-30 | 2000-02-18 | Elf Exploration Prod | Procede de detection et de caracterisation d'hydrocarbures de formation |
| US6307201B1 (en) | 1998-11-30 | 2001-10-23 | Envirotest Systems Corp. | Method and apparatus for selecting a filter for a remote sensing device |
| KR100326588B1 (ko) * | 1998-12-28 | 2002-10-12 | 에스케이 주식회사 | 근적외선분광분석기술을활용한자동원유분석방법 |
| US6717021B2 (en) * | 2000-06-13 | 2004-04-06 | Conocophillips Company | Solvating component and solvent system for mesophase pitch |
| EP2322919A1 (en) * | 2000-11-21 | 2011-05-18 | Waters Technologies Corporation | Mobile phase dilution scheme for enhanced chromatography |
| US20030139907A1 (en) * | 2002-01-24 | 2003-07-24 | Mccarthy Robert J | System, Method, and Product for Nanoscale Modeling, Analysis, Simulation, and Synthesis (NMASS) |
| JP4403853B2 (ja) | 2004-03-26 | 2010-01-27 | いすゞ自動車株式会社 | 多環芳香族炭化水素分析のための分析前処理方法及び装置 |
| KR20070029731A (ko) * | 2004-06-01 | 2007-03-14 | 이 아이 듀폰 디 네모아 앤드 캄파니 | 자외선-투명성 알칸 및 진공 및 원자외선 응용에서 그의사용 방법 |
| FR2883602B1 (fr) * | 2005-03-22 | 2010-04-16 | Alain Lunati | Procede d'optimisation des parametres de fonctionnement d'un moteur a combustion |
| US7447597B2 (en) * | 2005-05-06 | 2008-11-04 | Exxonmobil Research And Engineering Company | Data processing/visualization method for two (multi) dimensional separation gas chromatography xmass spectrometry (GCxMS) technique with a two (multiply) dimensional separation concept as an example |
| US10449502B2 (en) | 2005-08-25 | 2019-10-22 | The University of Wyoming Research Corporateion | Methods for analyzing hydrocarbons and hydrocarbon blends for chemical compositions |
| US7875464B2 (en) | 2005-08-25 | 2011-01-25 | The University Of Wyoming Research Corporation | Processing and analysis techniques involving in-vessel material generation |
| US9353317B2 (en) | 2011-09-20 | 2016-05-31 | The University Of Wyoming Research Corporation | Hydrocarbon separation and analysis apparatus and methods |
| US20130104772A1 (en) * | 2005-08-25 | 2013-05-02 | The University Of Wyoming Research Corporation D/B/A Western Research Institute | Methods for Changing Stability of Water and Oil Emulsions |
| RU2333476C1 (ru) * | 2006-12-28 | 2008-09-10 | Шлюмберже Текнолоджи Б.В. | Способ определения содержания парафинов и асфальтенов в нефти |
| WO2008107477A1 (en) * | 2007-03-07 | 2008-09-12 | Shell Internationale Research Maatschappij B.V. | Method of analysing the hydrocarbon compounds in a bituminous material |
| EP2009423A1 (en) * | 2007-06-28 | 2008-12-31 | Bp Oil International Limited | Sample plate |
| JP2010133392A (ja) * | 2008-12-08 | 2010-06-17 | Mitsubishi Heavy Ind Ltd | ディーゼルエンジン燃料健全性制御システム及びディーゼルエンジン燃料健全性評価方法 |
| US20110062058A1 (en) * | 2009-09-14 | 2011-03-17 | Chevron U.S.A. Inc. | Method for determining asphaltene stability of a hydrocarbon-containing material |
| JP5508837B2 (ja) * | 2009-12-24 | 2014-06-04 | 出光興産株式会社 | 重質油の成分分析方法 |
| US9778240B2 (en) | 2011-02-22 | 2017-10-03 | Saudi Arabian Oil Company | Characterization of crude oil by ultraviolet visible spectroscopy |
| US20120153139A1 (en) * | 2010-12-16 | 2012-06-21 | Exxonmobil Research And Engineering Company | Generation of model-of-composition of petroleum by high resolution mass spectrometry and associated analytics |
| US10684239B2 (en) | 2011-02-22 | 2020-06-16 | Saudi Arabian Oil Company | Characterization of crude oil by NMR spectroscopy |
| US11022588B2 (en) | 2011-02-22 | 2021-06-01 | Saudi Arabian Oil Company | Characterization of crude oil by simulated distillation |
| US10677718B2 (en) | 2011-02-22 | 2020-06-09 | Saudi Arabian Oil Company | Characterization of crude oil by near infrared spectroscopy |
| US10031121B2 (en) * | 2011-02-22 | 2018-07-24 | Saudi Arabian Oil Company | Characterization of an API gravity value of crude oil by ultraviolet visible spectroscopy |
| US10571452B2 (en) * | 2011-06-28 | 2020-02-25 | Saudi Arabian Oil Company | Characterization of crude oil by high pressure liquid chromatography |
| US10725013B2 (en) | 2011-06-29 | 2020-07-28 | Saudi Arabian Oil Company | Characterization of crude oil by Fourier transform ion cyclotron resonance mass spectrometry |
| US10662384B2 (en) | 2011-09-20 | 2020-05-26 | The University Of Wyoming Research Corporation | Methods for analyzing hydrocarbons and hydrocarbon blends for chemical compositions |
| US9127213B2 (en) | 2011-11-11 | 2015-09-08 | Chevron U.S.A. Inc. | Method for predicting catalyst performance |
| US9921203B2 (en) | 2011-11-11 | 2018-03-20 | Chevron U.S.A. Inc. | Method for predicting sediment content of a hydroprocessed hydrocarbon product |
| CA2889424A1 (en) | 2012-09-12 | 2014-03-20 | The University Of Wyoming Research Corporation D/B/A Western Research Institute | Continuous destabilization of emulsions |
| WO2016112002A1 (en) * | 2015-01-05 | 2016-07-14 | Saudi Arabian Oil Company | Characterizatin of crude oil by ultraviolet visible spectroscopy |
| JP6783771B2 (ja) | 2015-01-05 | 2020-11-11 | サウジ アラビアン オイル カンパニー | 近赤外分光法による原油のキャラクタリゼーション |
| SG11201705473XA (en) * | 2015-01-05 | 2017-08-30 | Saudi Arabian Oil Co | Relative valuation method for naphtha streams |
| KR20170121166A (ko) | 2015-01-05 | 2017-11-01 | 사우디 아라비안 오일 컴퍼니 | 열중량 분석에 의한 원유 및 이의 분획의 특성화 |
| JP6552647B2 (ja) * | 2015-06-10 | 2019-07-31 | サウジ アラビアン オイル カンパニー | レーザー誘起紫外線蛍光分光法を使用した原油のキャラクタリゼーション |
| JP6619583B2 (ja) * | 2015-08-20 | 2019-12-11 | 新コスモス電機株式会社 | ガスまたは液体の検出方法、および、ガスまたは液体の検出装置 |
| US10451593B2 (en) * | 2016-08-04 | 2019-10-22 | Aa Holdings, Ltd. | Detection system and method with nanostructure flow cell |
| WO2018025813A1 (ja) * | 2016-08-04 | 2018-02-08 | アクトファイブ株式会社 | 油分濃度計測装置及び油分濃度計測方法 |
| CN112005112A (zh) * | 2018-06-06 | 2020-11-27 | 瓦克化学股份公司 | 基于锯齿形梯度的高分辨液相色谱 |
| US11401471B2 (en) * | 2018-12-19 | 2022-08-02 | ExxonMobil Technology and Engineering Company | Simulated distillation using gas chromatography with vacuum ultraviolet detection |
| KR102608272B1 (ko) * | 2019-03-08 | 2023-11-29 | 주식회사 엘지화학 | 탄화수소유 내 원소분석방법 |
| WO2021011759A1 (en) * | 2019-07-17 | 2021-01-21 | Exxonmobil Research And Engineering Company | Methods for analysis of crude oil components using evaporative light scattering detection |
| US20230001327A1 (en) * | 2019-10-28 | 2023-01-05 | Petrochina Company Limited | Automatic separation apparatus for four fractions of heavy oil and separation method thereof |
| WO2022224697A1 (ja) * | 2021-04-19 | 2022-10-27 | 国立大学法人大阪大学 | 分子送達用粒子を特徴づけるための方法 |
| CN114062537B (zh) * | 2021-11-01 | 2024-03-19 | 河南中烟工业有限责任公司 | 一种准确检测加热卷烟中施加料液扩散速率的方法 |
| US11781988B2 (en) | 2022-02-28 | 2023-10-10 | Saudi Arabian Oil Company | Method to prepare virtual assay using fluorescence spectroscopy |
| US11913332B2 (en) | 2022-02-28 | 2024-02-27 | Saudi Arabian Oil Company | Method to prepare virtual assay using fourier transform infrared spectroscopy |
Family Cites Families (20)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US2974226A (en) * | 1957-11-01 | 1961-03-07 | Phillips Petroleum Co | Ultraviolet analyzer |
| US3676649A (en) * | 1970-05-08 | 1972-07-11 | Phillips Petroleum Co | Signal analysis and recording |
| US3897213A (en) * | 1973-08-06 | 1975-07-29 | Dow Chemical Co | Automated quantitative analysis of ionic species |
| US3975727A (en) * | 1974-06-28 | 1976-08-17 | Technicon Instruments Corporation | Automated calibration and standardization apparatus |
| US4199323A (en) * | 1978-06-08 | 1980-04-22 | The Dow Chemical Company | Analytical technique for quantitating acid/salt and base/salt samples for species concentration |
| US4264814A (en) * | 1979-07-31 | 1981-04-28 | The United States Of America As Represented By The United States Department Of Energy | Method for detecting trace impurities in gases |
| US4254656A (en) * | 1979-09-12 | 1981-03-10 | Philips Petroleum Company | Chromatographic analysis without calibration using dual detectors |
| JPS5689058A (en) * | 1979-12-21 | 1981-07-20 | Toyo Soda Mfg Co Ltd | Method for analyzing hydrocarbon compound |
| US4265634A (en) * | 1980-03-10 | 1981-05-05 | Dionex Corporation | Chromatographic separation and quantitative analysis of ionic species |
| US4476713A (en) * | 1982-08-31 | 1984-10-16 | Varian Associates, Inc. | Liquid chromatographic separation of hydrocarbons |
| US4563585A (en) * | 1982-09-23 | 1986-01-07 | Moniteg Ltd. | Monitoring gas and vapor concentrations |
| US4446105A (en) * | 1982-10-29 | 1984-05-01 | The United States Of America As Represented By The United States Department Of Energy | System for analyzing coal liquefaction products |
| US4631687A (en) * | 1983-11-03 | 1986-12-23 | Rohrback Technology Corporation | Method and apparatus for analysis employing multiple separation processes |
| SU1187032A1 (ru) * | 1984-01-04 | 1985-10-23 | Предприятие П/Я Р-6711 | Способ определени содержани бензольных углеводородов в нефтепродуктах |
| US4614871A (en) * | 1984-10-31 | 1986-09-30 | Driscoll John N | Photodiode |
| US4567753A (en) * | 1984-12-12 | 1986-02-04 | The Dow Chemical Company | Independent analysis of anions and cations using indirect photometric chromatography |
| US4733084A (en) * | 1985-01-09 | 1988-03-22 | Sumitomo Electric Industries, Ltd. | Method of detection and quantitative determination of sulfur and sulfur monitor using the method |
| US4671103A (en) * | 1985-04-08 | 1987-06-09 | Exxon Chemical Patents Inc. | Method for determining crude oil fouling by high performance liquid chromatography |
| US4802986A (en) * | 1986-09-09 | 1989-02-07 | The United States Of America As Represented By The Secretary Of The Air Force | Hydrocarbon group-type analyzer system |
| US4783416A (en) * | 1987-05-08 | 1988-11-08 | Shell Oil Company | Analytical method to determine the unwashed gum content in a gasoline boiling hydrocarbon |
-
1989
- 1989-05-30 US US07/358,779 patent/US4988446A/en not_active Expired - Lifetime
-
1990
- 1990-05-07 CA CA002016222A patent/CA2016222C/en not_active Expired - Fee Related
- 1990-05-25 NO NO19902324A patent/NO311594B1/no unknown
- 1990-05-28 AU AU55984/90A patent/AU622082B2/en not_active Ceased
- 1990-05-30 ES ES90305881T patent/ES2100870T3/es not_active Expired - Lifetime
- 1990-05-30 JP JP02141190A patent/JP3073757B2/ja not_active Expired - Fee Related
- 1990-05-30 MY MYPI90000891A patent/MY105829A/en unknown
- 1990-05-30 DE DE69030341T patent/DE69030341T2/de not_active Expired - Fee Related
- 1990-05-30 EP EP90305881A patent/EP0400989B1/en not_active Expired - Lifetime
-
1997
- 1997-05-02 GR GR970400985T patent/GR3023326T3/el unknown
- 1997-05-30 JP JP09142038A patent/JP3084382B2/ja not_active Expired - Fee Related
- 1997-08-25 NO NO973894A patent/NO305921B1/no unknown
Also Published As
| Publication number | Publication date |
|---|---|
| JP3084382B2 (ja) | 2000-09-04 |
| AU622082B2 (en) | 1992-03-26 |
| DE69030341D1 (de) | 1997-05-07 |
| JPH03115837A (ja) | 1991-05-16 |
| NO973894L (no) | 1997-08-25 |
| ES2100870T3 (es) | 1997-07-01 |
| AU5598490A (en) | 1990-12-06 |
| US4988446A (en) | 1991-01-29 |
| NO902324D0 (no) | 1990-05-25 |
| JP3073757B2 (ja) | 2000-08-07 |
| NO973894D0 (no) | 1997-08-25 |
| NO305921B1 (no) | 1999-08-16 |
| CA2016222A1 (en) | 1990-11-30 |
| EP0400989A2 (en) | 1990-12-05 |
| MY105829A (en) | 1995-01-30 |
| EP0400989A3 (en) | 1992-04-29 |
| EP0400989B1 (en) | 1997-04-02 |
| DE69030341T2 (de) | 1997-08-21 |
| NO902324L (no) | 1990-12-03 |
| GR3023326T3 (en) | 1997-08-29 |
| JPH1082774A (ja) | 1998-03-31 |
| CA2016222C (en) | 2001-02-20 |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| NO311594B1 (no) | Fremgangsmåte for kromatografisk analyse av hydrokarboner, og fremgangsmåte for raffinering av en petroleumhydrokarbontilförsel | |
| US5076909A (en) | Method for refining or upgrading hydrocarbons with analysis | |
| US4865746A (en) | Chromatographic analysis of hydrocarbons | |
| US10662384B2 (en) | Methods for analyzing hydrocarbons and hydrocarbon blends for chemical compositions | |
| US20190170725A1 (en) | Method for estimating sediment content of a hydroprocessed hydrocarbon-containing feedstock | |
| US20150106029A1 (en) | Method of characterizing crude oil by high pressure liquid chromatography | |
| US20150106032A1 (en) | Characterization of crude oil by simulated distillation | |
| WO2011032125A2 (en) | Method for predicting reactivity of a hydrocarbon-containing feedstock for hydroprocessing | |
| US20130124105A1 (en) | Method for predicting sediment content of a hydroprocessed hydrocarbon product | |
| Robbins | Quantitative measurement of mass and aromaticity distributions for heavy distillates 1. Capabilities of the HPLC-2 system | |
| US9127213B2 (en) | Method for predicting catalyst performance | |
| US4762797A (en) | Method for determining the fouling tendency of hydrocarbons | |
| Miranda et al. | SimDis-HT analysis of crude oils as a tool to define operating conditions for primary treatment processes | |
| Drushel | Sulfur compound type distributions in petroleum using an in-line reactor or pyrolysis combined with gas chromatography and a microcoulometric sulfur detector | |
| US20230273176A1 (en) | Method to prepare virtual assay using high pressure liquid chromatography | |
| Sánchez et al. | Size exclusion chromatographic approach for the evaluation of processes for upgrading heavy petroleum | |
| JP3090930B2 (ja) | 炭化水素のクロマトグラフ分析のための方法および装置、並びにこれを用いた炭化水素精製操作 | |
| CA1324897C (en) | Method and equipment for chromatographic analysis of hydrocarbons, and hydrocarbon refining operations using same | |
| CA2313990C (en) | Method for spectroscopic analysis of hydrocarbons, and hydrocarbon refining operations using same | |
| Gautam et al. | Review of spectrometric techniques for the characterization of crude oil and petroleum products | |
| DE68927133T2 (de) | Chromatographische Analyse von Kohlenwasserstoffölen | |
| Colin et al. | Characterisation of heavy crude oils and petroleum residues-review of the results obtained by the ASVAHL analytical group | |
| Voelkel et al. | Inverse gas chromatography for the examination of fractions separated from oil vacuum distillation residues | |
| Oschmann et al. | Separation of paraffin from crude oil by supercritical fluid extraction | |
| Terrell | Petroleum |