MXPA97009585A

MXPA97009585A - Intercalados y exfoliados formados con compuestosintercalantes monomericos, oligomericos o polimericos (c6+) de cadena larga o compatibles con polimero de matriz aromatica; y materiales compuestos que los contienen.

Intercalados y exfoliados formados con compuestosintercalantes monomericos, oligomericos o polimericos (c6+) de cadena larga o compatibles con polimero de matriz aromatica; y materiales compuestos que los contienen.

Info

Publication number: MXPA97009585A
Authority: MX; Mexico
Prior art keywords: percent; weight; composition; interleaving; surface modifier
Prior art date: 1996-12-06

Application number

MXPA97009585A

Other languages

English (en)

Spanish (es)

Inventor

Liang Ying

Original Assignee

Amcol International Corp

Priority date

1996-12-06

Filing date

1997-12-05

Publication date

2005-07-25

1996-12-06 Priority claimed from US08/758,740 external-priority patent/US5952095A/en

1997-12-05 Application filed by Amcol International Corp filed Critical Amcol International Corp

2005-07-25 Publication of MXPA97009585A publication Critical patent/MXPA97009585A/es

Links

239000011159 matrix material Substances 0.000 title claims abstract description 84
150000001875 compounds Chemical class 0.000 title claims abstract description 79
125000003118 aryl group Chemical group 0.000 title claims abstract description 53
239000002131 composite material Substances 0.000 title claims description 12
239000000203 mixture Substances 0.000 claims abstract description 155
239000000463 material Substances 0.000 claims abstract description 133
229920000642 polymer Polymers 0.000 claims abstract description 114
229910052615 phyllosilicate Inorganic materials 0.000 claims abstract description 65
239000003607 modifier Substances 0.000 claims abstract description 33
125000004432 carbon atom Chemical group C* 0.000 claims abstract description 26
239000007788 liquid Substances 0.000 claims abstract description 22
125000000524 functional group Chemical group 0.000 claims abstract description 10
239000010410 layer Substances 0.000 claims description 105
238000009830 intercalation Methods 0.000 claims description 97
239000011229 interlayer Substances 0.000 claims description 81
XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 61
125000000217 alkyl group Chemical group 0.000 claims description 44
150000001768 cations Chemical class 0.000 claims description 38
238000000034 method Methods 0.000 claims description 37
238000000926 separation method Methods 0.000 claims description 32
239000000178 monomer Substances 0.000 claims description 27
238000001179 sorption measurement Methods 0.000 claims description 26
230000002687 intercalation Effects 0.000 claims description 23
239000000138 intercalating agent Substances 0.000 claims description 15
229920001169 thermoplastic Polymers 0.000 claims description 14
230000009918 complex formation Effects 0.000 claims description 12
239000003960 organic solvent Substances 0.000 claims description 11
230000000536 complexating effect Effects 0.000 claims description 5
239000001257 hydrogen Substances 0.000 claims description 5
229910052739 hydrogen Inorganic materials 0.000 claims description 5
229920001187 thermosetting polymer Polymers 0.000 claims description 5
230000009920 chelation Effects 0.000 claims description 3
238000010668 complexation reaction Methods 0.000 claims description 3
150000002500 ions Chemical class 0.000 claims description 3
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238000005411 Van der Waals force Methods 0.000 claims description 2
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239000012876 carrier material Substances 0.000 abstract description 4
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238000004299 exfoliation Methods 0.000 description 22
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RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 description 16
239000002114 nanocomposite Substances 0.000 description 16
239000011734 sodium Substances 0.000 description 16
BPQQTUXANYXVAA-UHFFFAOYSA-N Orthosilicate Chemical compound [O-][Si]([O-])([O-])[O-] BPQQTUXANYXVAA-UHFFFAOYSA-N 0.000 description 15
JUJWROOIHBZHMG-UHFFFAOYSA-N Pyridine Chemical compound C1=CC=NC=C1 JUJWROOIHBZHMG-UHFFFAOYSA-N 0.000 description 15
150000001408 amides Chemical class 0.000 description 15
150000001299 aldehydes Chemical class 0.000 description 14
229920001577 copolymer Polymers 0.000 description 14
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239000005977 Ethylene Substances 0.000 description 13
229910052751 metal Inorganic materials 0.000 description 13
239000002184 metal Substances 0.000 description 13
AWDGGAOYFMTHKT-UHFFFAOYSA-N 1-(12-aminododecyl)pyrrolidin-2-one Chemical compound NCCCCCCCCCCCCN1CCCC1=O AWDGGAOYFMTHKT-UHFFFAOYSA-N 0.000 description 12
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239000004677 Nylon Substances 0.000 description 11
150000001298 alcohols Chemical class 0.000 description 11
QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 11
VGGSQFUCUMXWEO-UHFFFAOYSA-N Ethene Chemical compound C=C VGGSQFUCUMXWEO-UHFFFAOYSA-N 0.000 description 10
125000004429 atom Chemical group 0.000 description 10
150000001732 carboxylic acid derivatives Chemical class 0.000 description 10
125000002887 hydroxy group Chemical group [H]O* 0.000 description 10
150000002576 ketones Chemical class 0.000 description 10
230000008569 process Effects 0.000 description 10
HNJBEVLQSNELDL-UHFFFAOYSA-N pyrrolidin-2-one Chemical compound O=C1CCCN1 HNJBEVLQSNELDL-UHFFFAOYSA-N 0.000 description 10
KAKZBPTYRLMSJV-UHFFFAOYSA-N Butadiene Chemical compound C=CC=C KAKZBPTYRLMSJV-UHFFFAOYSA-N 0.000 description 9
238000002441 X-ray diffraction Methods 0.000 description 9
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IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 8
KKEYFWRCBNTPAC-UHFFFAOYSA-N Terephthalic acid Chemical compound OC(=O)C1=CC=C(C(O)=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-N 0.000 description 8
150000001350 alkyl halides Chemical class 0.000 description 8
230000015572 biosynthetic process Effects 0.000 description 8
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150000004985 diamines Chemical class 0.000 description 8
239000003814 drug Substances 0.000 description 8
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OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 7
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150000008064 anhydrides Chemical class 0.000 description 7
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125000002496 methyl group Chemical group [H]C([H])([H])* 0.000 description 7
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235000019422 polyvinyl alcohol Nutrition 0.000 description 7
UMJSCPRVCHMLSP-UHFFFAOYSA-N pyridine Natural products COC1=CC=CN=C1 UMJSCPRVCHMLSP-UHFFFAOYSA-N 0.000 description 7
239000003760 tallow Substances 0.000 description 7
KKEYFWRCBNTPAC-UHFFFAOYSA-L terephthalate(2-) Chemical compound [O-]C(=O)C1=CC=C(C([O-])=O)C=C1 KKEYFWRCBNTPAC-UHFFFAOYSA-L 0.000 description 7
UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 description 6
OYPRJOBELJOOCE-UHFFFAOYSA-N Calcium Chemical compound [Ca] OYPRJOBELJOOCE-UHFFFAOYSA-N 0.000 description 6
OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 description 6
239000002537 cosmetic Substances 0.000 description 6
238000002156 mixing Methods 0.000 description 6
239000004014 plasticizer Substances 0.000 description 6
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239000004372 Polyvinyl alcohol Substances 0.000 description 5
239000006087 Silane Coupling Agent Substances 0.000 description 5
PPBRXRYQALVLMV-UHFFFAOYSA-N Styrene Chemical compound C=CC1=CC=CC=C1 PPBRXRYQALVLMV-UHFFFAOYSA-N 0.000 description 5
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239000003921 oil Substances 0.000 description 5
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229910001415 sodium ion Inorganic materials 0.000 description 5
238000003786 synthesis reaction Methods 0.000 description 5
VBICKXHEKHSIBG-UHFFFAOYSA-N 1-monostearoylglycerol Chemical compound CCCCCCCCCCCCCCCCCC(=O)OCC(O)CO VBICKXHEKHSIBG-UHFFFAOYSA-N 0.000 description 4
PBLZLIFKVPJDCO-UHFFFAOYSA-N 12-aminododecanoic acid Chemical compound NCCCCCCCCCCCC(O)=O PBLZLIFKVPJDCO-UHFFFAOYSA-N 0.000 description 4
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238000006243 chemical reaction Methods 0.000 description 4
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238000009833 condensation Methods 0.000 description 4
230000005494 condensation Effects 0.000 description 4
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239000003995 emulsifying agent Substances 0.000 description 4
BTCSSZJGUNDROE-UHFFFAOYSA-N gamma-aminobutyric acid Chemical compound NCCCC(O)=O BTCSSZJGUNDROE-UHFFFAOYSA-N 0.000 description 4
235000011187 glycerol Nutrition 0.000 description 4
238000010438 heat treatment Methods 0.000 description 4
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239000000314 lubricant Substances 0.000 description 4
229910052749 magnesium Inorganic materials 0.000 description 4
238000001819 mass spectrum Methods 0.000 description 4
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ARKHFOXARSJRGJ-UHFFFAOYSA-N 1-(6-aminohexyl)pyrrolidin-2-one Chemical compound NCCCCCCN1CCCC1=O ARKHFOXARSJRGJ-UHFFFAOYSA-N 0.000 description 3
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QWZLBLDNRUUYQI-UHFFFAOYSA-M Methylbenzethonium chloride Chemical compound [Cl-].CC1=CC(C(C)(C)CC(C)(C)C)=CC=C1OCCOCC[N+](C)(C)CC1=CC=CC=C1 QWZLBLDNRUUYQI-UHFFFAOYSA-M 0.000 description 3
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VGIBGUSAECPPNB-UHFFFAOYSA-L nonaaluminum;magnesium;tripotassium;1,3-dioxido-2,4,5-trioxa-1,3-disilabicyclo[1.1.1]pentane;iron(2+);oxygen(2-);fluoride;hydroxide Chemical compound [OH-].[O-2].[O-2].[O-2].[O-2].[O-2].[F-].[Mg+2].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[Al+3].[K+].[K+].[K+].[Fe+2].O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2.O1[Si]2([O-])O[Si]1([O-])O2 VGIBGUSAECPPNB-UHFFFAOYSA-L 0.000 description 3
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XNGIFLGASWRNHJ-UHFFFAOYSA-N phthalic acid Chemical compound OC(=O)C1=CC=CC=C1C(O)=O XNGIFLGASWRNHJ-UHFFFAOYSA-N 0.000 description 3
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WSWCOQWTEOXDQX-MQQKCMAXSA-M (E,E)-sorbate Chemical compound C\C=C\C=C\C([O-])=O WSWCOQWTEOXDQX-MQQKCMAXSA-M 0.000 description 2
XFRVVPUIAFSTFO-UHFFFAOYSA-N 1-Tridecanol Chemical compound CCCCCCCCCCCCCO XFRVVPUIAFSTFO-UHFFFAOYSA-N 0.000 description 2
FUJGBKOREIZSDD-KTKRTIGZSA-N 1-[(z)-octadec-9-enyl]pyrrolidin-2-one Chemical compound CCCCCCCC\C=C/CCCCCCCCN1CCCC1=O FUJGBKOREIZSDD-KTKRTIGZSA-N 0.000 description 2
BMVXCPBXGZKUPN-UHFFFAOYSA-N 1-hexanamine Chemical compound CCCCCCN BMVXCPBXGZKUPN-UHFFFAOYSA-N 0.000 description 2
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DJIHQRBJGCGSIR-UHFFFAOYSA-N 2-methylidene-1,3-dioxepane-4,7-dione Chemical compound C1(CCC(=O)OC(=C)O1)=O DJIHQRBJGCGSIR-UHFFFAOYSA-N 0.000 description 2
ULKFLOVGORAZDI-UHFFFAOYSA-N 3,3-dimethyloxetan-2-one Chemical compound CC1(C)COC1=O ULKFLOVGORAZDI-UHFFFAOYSA-N 0.000 description 2
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XYJZYZMKUIMAMT-UHFFFAOYSA-N 3-methyl-4-(2-oxopyrrolidin-1-yl)benzoic acid Chemical compound CC1=CC(C(O)=O)=CC=C1N1C(=O)CCC1 XYJZYZMKUIMAMT-UHFFFAOYSA-N 0.000 description 2
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ULGZDMOVFRHVEP-RWJQBGPGSA-N Erythromycin Chemical compound O([C@@H]1[C@@H](C)C(=O)O[C@@H]([C@@]([C@H](O)[C@@H](C)C(=O)[C@H](C)C[C@@](C)(O)[C@H](O[C@H]2[C@@H]([C@H](C[C@@H](C)O2)N(C)C)O)[C@H]1C)(C)O)CC)[C@H]1C[C@@](C)(OC)[C@@H](O)[C@H](C)O1 ULGZDMOVFRHVEP-RWJQBGPGSA-N 0.000 description 2
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HPEUJPJOZXNMSJ-UHFFFAOYSA-N Methyl stearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC HPEUJPJOZXNMSJ-UHFFFAOYSA-N 0.000 description 2
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VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
NWGKJDSIEKMTRX-AAZCQSIUSA-N Sorbitan monooleate Chemical compound CCCCCCCC\C=C/CCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O NWGKJDSIEKMTRX-AAZCQSIUSA-N 0.000 description 2
HVUMOYIDDBPOLL-XWVZOOPGSA-N Sorbitan monostearate Chemical compound CCCCCCCCCCCCCCCCCC(=O)OC[C@@H](O)[C@H]1OC[C@H](O)[C@H]1O HVUMOYIDDBPOLL-XWVZOOPGSA-N 0.000 description 2
NINIDFKCEFEMDL-UHFFFAOYSA-N Sulfur Chemical compound [S] NINIDFKCEFEMDL-UHFFFAOYSA-N 0.000 description 2
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