MXPA04004920A - Metodo para el aislamiento de trimetilolpropano a partir de una mezcla de reaccion. - Google Patents

Metodo para el aislamiento de trimetilolpropano a partir de una mezcla de reaccion.

Info

Publication number
MXPA04004920A
MXPA04004920A MXPA04004920A MXPA04004920A MXPA04004920A MX PA04004920 A MXPA04004920 A MX PA04004920A MX PA04004920 A MXPA04004920 A MX PA04004920A MX PA04004920 A MXPA04004920 A MX PA04004920A MX PA04004920 A MXPA04004920 A MX PA04004920A
Authority
MX
Mexico
Prior art keywords
trimethylol propane
reaction mixture
column
isolation
mixture
Prior art date
Application number
MXPA04004920A
Other languages
English (en)
Inventor
Sirch Tilman
Original Assignee
Basf Ag
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Family has litigation
First worldwide family litigation filed litigation Critical https://patents.darts-ip.com/?family=7708393&utm_source=google_patent&utm_medium=platform_link&utm_campaign=public_patent_search&patent=MXPA04004920(A) "Global patent litigation dataset” by Darts-ip is licensed under a Creative Commons Attribution 4.0 International License.
Application filed by Basf Ag filed Critical Basf Ag
Publication of MXPA04004920A publication Critical patent/MXPA04004920A/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
    • C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
    • C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
    • C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
    • C07C31/18—Polyhydroxylic acyclic alcohols
    • C07C31/22—Trihydroxylic alcohols, e.g. glycerol

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Steroid Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)

Abstract

Se aisla trimetilolpropano a partir de una mezcla de reaccion, obtenida mediante la reaccion de n-butiraldehido con formaldehido en presencia de una base e hidrogenacion opcional de la mezcla obtenida. La mezcla es destilada utilizando una columna de separacion o una columna de destilacion con una columna anterior o una columna de destilacion posterior. El metodo esta caracterizado por una baja inversion y costo de energia y la formacion reducida de subproductos de alto punto de ebullicion.
MXPA04004920A 2001-12-07 2004-05-24 Metodo para el aislamiento de trimetilolpropano a partir de una mezcla de reaccion. MXPA04004920A (es)

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
DE10160180A DE10160180A1 (de) 2001-12-07 2001-12-07 Verfahren zur Isolierung von Trimethylolpropan aus einem Reaktionsgemisch

Publications (1)

Publication Number Publication Date
MXPA04004920A true MXPA04004920A (es) 2004-08-11

Family

ID=7708393

Family Applications (1)

Application Number Title Priority Date Filing Date
MXPA04004920A MXPA04004920A (es) 2001-12-07 2004-05-24 Metodo para el aislamiento de trimetilolpropano a partir de una mezcla de reaccion.

Country Status (12)

Country Link
US (1) US7112707B2 (es)
EP (1) EP1456159B1 (es)
JP (1) JP3923472B2 (es)
KR (1) KR100884121B1 (es)
CN (1) CN1257141C (es)
AT (1) ATE334957T1 (es)
AU (1) AU2002358636A1 (es)
BR (1) BR0214543B1 (es)
DE (2) DE10160180A1 (es)
MX (1) MXPA04004920A (es)
MY (1) MY128842A (es)
WO (1) WO2003048093A2 (es)

Families Citing this family (15)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8575401B2 (en) * 2008-12-09 2013-11-05 Basf Se Method for purifying crude polymethylols
JP5783905B2 (ja) * 2008-12-09 2015-09-24 ビーエーエスエフ ソシエタス・ヨーロピアＢａｓｆ Ｓｅ ポリメチロールの製造方法
MY155607A (en) * 2009-01-12 2015-11-13 Basf Se Method for producing polymethylols
DE102010033844B4 (de) 2010-08-11 2013-01-03 Oxea Gmbh Verfahren zur Gewinnung von Di-Trimethylolpropan und mit Trimethylolpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung
DE102010042936A1 (de) * 2010-10-26 2012-04-26 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat
DE102010042934A1 (de) * 2010-10-26 2012-04-26 Bayer Materialscience Aktiengesellschaft Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat
KR101530102B1 (ko) * 2010-12-29 2015-06-18 주식회사 엘지화학 네오펜틸글리콜 정제를 위한 분리벽형 증류탑 및 이를 이용한 정제방법
JP2015530416A (ja) * 2012-09-28 2015-10-15 ダウ グローバル テクノロジーズ エルエルシー 高純度グリコールエステル類の生成のための方法
US10150720B2 (en) * 2013-01-16 2018-12-11 Lg Chem, Ltd. Device for preparing n-butanol
CN106861353A (zh) * 2015-12-14 2017-06-20 财团法人工业技术研究院 分离装置
KR102224268B1 (ko) * 2016-10-31 2021-03-08 주식회사 엘지화학 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
KR102224243B1 (ko) * 2016-10-31 2021-03-08 주식회사 엘지화학 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
KR102224267B1 (ko) * 2016-10-31 2021-03-08 주식회사 엘지화학 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법
US10913700B2 (en) 2018-02-01 2021-02-09 Lg Chem, Ltd. Method for producing dimethylolbutanal and distillation apparatus for producing same
WO2023140986A1 (en) 2022-01-19 2023-07-27 Exxonmobil Chemical Patents Inc. Compositions containing tri-cyclopentadiene and processes for making same

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2471134A (en) * 1946-07-17 1949-05-24 Standard Oil Dev Co Fractionation apparatus
DE3302525A1 (de) * 1983-01-26 1984-07-26 Basf Ag, 6700 Ludwigshafen Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes
DE3340791A1 (de) * 1983-11-11 1985-05-23 Basf Ag, 6700 Ludwigshafen Verfahren zur herstellung von trimethylolalkanen aus alkanalen und formaldehyd
GB2303511A (en) * 1995-07-19 1997-02-19 Univ Manchester Compensating for backscattered light
US5767922A (en) * 1996-04-05 1998-06-16 Cornell Research Foundation, Inc. Apparatus and process for detecting scene breaks in a sequence of video frames
DE19653093A1 (de) * 1996-12-20 1998-06-25 Basf Ag Verfahren zur Herstellung von Polyalkoholen
JP4284477B2 (ja) 1998-12-25 2009-06-24 三菱瓦斯化学株式会社 高純度トリメチロールプロパンの製造法
US6778697B1 (en) * 1999-02-05 2004-08-17 Samsung Electronics Co., Ltd. Color image processing method and apparatus thereof
US6389417B1 (en) * 1999-06-29 2002-05-14 Samsung Electronics Co., Ltd. Method and apparatus for searching a digital image
DE19963435A1 (de) * 1999-12-28 2001-07-05 Basf Ag Verfahren zur Reinigung von durch Hydrierung hergestelltem Trimethylolpropan durch kontinuierliche Destillation

Also Published As

Publication number Publication date
AU2002358636A1 (en) 2003-06-17
WO2003048093A3 (de) 2004-01-15
JP3923472B2 (ja) 2007-05-30
US7112707B2 (en) 2006-09-26
DE10160180A1 (de) 2003-06-18
EP1456159B1 (de) 2006-08-02
US20040267055A1 (en) 2004-12-30
CN1257141C (zh) 2006-05-24
CN1599707A (zh) 2005-03-23
JP2005511674A (ja) 2005-04-28
ATE334957T1 (de) 2006-08-15
WO2003048093A2 (de) 2003-06-12
EP1456159A2 (de) 2004-09-15
BR0214543A (pt) 2004-11-03
BR0214543B1 (pt) 2013-04-16
MY128842A (en) 2007-02-28
DE50207749D1 (de) 2006-09-14
KR100884121B1 (ko) 2009-02-17
KR20050044718A (ko) 2005-05-12

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