BR0214543A - Processo para isolar trimetilolpropano a partir de uma mistura de reação - Google Patents
Processo para isolar trimetilolpropano a partir de uma mistura de reaçãoInfo
- Publication number
- BR0214543A BR0214543A BR0214543-0A BR0214543A BR0214543A BR 0214543 A BR0214543 A BR 0214543A BR 0214543 A BR0214543 A BR 0214543A BR 0214543 A BR0214543 A BR 0214543A
- Authority
- BR
- Brazil
- Prior art keywords
- trimethylolpropane
- reaction mixture
- isolating
- column
- mixture
- Prior art date
Links
Classifications
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
- B01D3/14—Fractional distillation or use of a fractionation or rectification column
- B01D3/141—Fractional distillation or use of a fractionation or rectification column where at least one distillation column contains at least one dividing wall
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C29/00—Preparation of compounds having hydroxy or O-metal groups bound to a carbon atom not belonging to a six-membered aromatic ring
- C07C29/74—Separation; Purification; Use of additives, e.g. for stabilisation
- C07C29/76—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment
- C07C29/80—Separation; Purification; Use of additives, e.g. for stabilisation by physical treatment by distillation
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C31/00—Saturated compounds having hydroxy or O-metal groups bound to acyclic carbon atoms
- C07C31/18—Polyhydroxylic acyclic alcohols
- C07C31/22—Trihydroxylic alcohols, e.g. glycerol
Abstract
"PROCESSO PARA ISOLAR TRIMETILOLPROPANO A PARTIR DE UMA MISTURA DE REAçãO". O trimetilolpropano é isolado a partir de uma mistura de reação, obtida pela reação de n-butiraldeído com formaldeído na presença de uma base e hidrogenação opcional da mistura obtida. A mistura é destilada usando uma coluna de separação ou uma coluna de destilação com uma pré coluna ou uma coluna de destilação com uma pós coluna. O método é caracterizado por um custo de investimento e energia baixos e a formação reduzida de subprodutos de alta ebulição.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DE10160180A DE10160180A1 (de) | 2001-12-07 | 2001-12-07 | Verfahren zur Isolierung von Trimethylolpropan aus einem Reaktionsgemisch |
PCT/EP2002/013882 WO2003048093A2 (de) | 2001-12-07 | 2002-12-06 | Verfahren zur isolierung von trimethylolpropan aus einem reaktionsgemisch |
Publications (2)
Publication Number | Publication Date |
---|---|
BR0214543A true BR0214543A (pt) | 2004-11-03 |
BR0214543B1 BR0214543B1 (pt) | 2013-04-16 |
Family
ID=7708393
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
BRPI0214543-0A BR0214543B1 (pt) | 2001-12-07 | 2002-12-06 | processo para isolar trimetilolpropano a partir de uma mistura de reaÇço. |
Country Status (12)
Country | Link |
---|---|
US (1) | US7112707B2 (pt) |
EP (1) | EP1456159B1 (pt) |
JP (1) | JP3923472B2 (pt) |
KR (1) | KR100884121B1 (pt) |
CN (1) | CN1257141C (pt) |
AT (1) | ATE334957T1 (pt) |
AU (1) | AU2002358636A1 (pt) |
BR (1) | BR0214543B1 (pt) |
DE (2) | DE10160180A1 (pt) |
MX (1) | MXPA04004920A (pt) |
MY (1) | MY128842A (pt) |
WO (1) | WO2003048093A2 (pt) |
Families Citing this family (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
WO2010066674A2 (de) * | 2008-12-09 | 2010-06-17 | Basf Se | Verfahren zur herstellung von polymethylolen |
MY153850A (en) * | 2008-12-09 | 2015-03-31 | Basf Se | Method for purifying crude polymethylols |
US8933277B2 (en) * | 2009-01-12 | 2015-01-13 | Basf Se | Process for preparing polymethylols |
DE102010033844B4 (de) | 2010-08-11 | 2013-01-03 | Oxea Gmbh | Verfahren zur Gewinnung von Di-Trimethylolpropan und mit Trimethylolpropan angereicherten Produktströmen aus den Nebenströmen der Trimethylolpropanherstellung |
DE102010042936A1 (de) * | 2010-10-26 | 2012-04-26 | Bayer Materialscience Aktiengesellschaft | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat |
DE102010042934A1 (de) * | 2010-10-26 | 2012-04-26 | Bayer Materialscience Aktiengesellschaft | Verfahren zur kontinuierlichen Herstellung von Dialkylcarbonat |
KR101530102B1 (ko) * | 2010-12-29 | 2015-06-18 | 주식회사 엘지화학 | 네오펜틸글리콜 정제를 위한 분리벽형 증류탑 및 이를 이용한 정제방법 |
CA2885432C (en) * | 2012-09-28 | 2017-04-25 | Dow Global Technologies Llc | Process for the production of high purity glycol esters |
JP6329962B2 (ja) * | 2013-01-16 | 2018-05-23 | エルジー・ケム・リミテッド | アルカノールの製造装置 |
CN106861353A (zh) * | 2015-12-14 | 2017-06-20 | 财团法人工业技术研究院 | 分离装置 |
KR102224267B1 (ko) * | 2016-10-31 | 2021-03-08 | 주식회사 엘지화학 | 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법 |
KR102224243B1 (ko) * | 2016-10-31 | 2021-03-08 | 주식회사 엘지화학 | 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법 |
KR102224268B1 (ko) * | 2016-10-31 | 2021-03-08 | 주식회사 엘지화학 | 트리메틸올프로판의 제조장치 및 이를 이용한 제조방법 |
KR102391592B1 (ko) | 2018-02-01 | 2022-04-28 | 주식회사 엘지화학 | 디메틸올부탄알의 제조방법 및 증류 장치 |
WO2023140986A1 (en) | 2022-01-19 | 2023-07-27 | Exxonmobil Chemical Patents Inc. | Compositions containing tri-cyclopentadiene and processes for making same |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2471134A (en) * | 1946-07-17 | 1949-05-24 | Standard Oil Dev Co | Fractionation apparatus |
DE3302525A1 (de) * | 1983-01-26 | 1984-07-26 | Basf Ag, 6700 Ludwigshafen | Destillationskolonne zur destillativen zerlegung eines aus mehreren fraktionen bestehenden zulaufproduktes |
DE3340791A1 (de) * | 1983-11-11 | 1985-05-23 | Basf Ag, 6700 Ludwigshafen | Verfahren zur herstellung von trimethylolalkanen aus alkanalen und formaldehyd |
GB2303511A (en) * | 1995-07-19 | 1997-02-19 | Univ Manchester | Compensating for backscattered light |
US5767922A (en) * | 1996-04-05 | 1998-06-16 | Cornell Research Foundation, Inc. | Apparatus and process for detecting scene breaks in a sequence of video frames |
DE19653093A1 (de) | 1996-12-20 | 1998-06-25 | Basf Ag | Verfahren zur Herstellung von Polyalkoholen |
JP4284477B2 (ja) * | 1998-12-25 | 2009-06-24 | 三菱瓦斯化学株式会社 | 高純度トリメチロールプロパンの製造法 |
US6778697B1 (en) * | 1999-02-05 | 2004-08-17 | Samsung Electronics Co., Ltd. | Color image processing method and apparatus thereof |
US6389417B1 (en) * | 1999-06-29 | 2002-05-14 | Samsung Electronics Co., Ltd. | Method and apparatus for searching a digital image |
DE19963435A1 (de) * | 1999-12-28 | 2001-07-05 | Basf Ag | Verfahren zur Reinigung von durch Hydrierung hergestelltem Trimethylolpropan durch kontinuierliche Destillation |
-
2001
- 2001-12-07 DE DE10160180A patent/DE10160180A1/de not_active Withdrawn
-
2002
- 2002-11-27 MY MYPI20024454A patent/MY128842A/en unknown
- 2002-12-06 AU AU2002358636A patent/AU2002358636A1/en not_active Abandoned
- 2002-12-06 KR KR1020047008681A patent/KR100884121B1/ko not_active IP Right Cessation
- 2002-12-06 EP EP02792927A patent/EP1456159B1/de not_active Expired - Lifetime
- 2002-12-06 DE DE50207749T patent/DE50207749D1/de not_active Expired - Lifetime
- 2002-12-06 US US10/497,522 patent/US7112707B2/en not_active Expired - Fee Related
- 2002-12-06 JP JP2003549288A patent/JP3923472B2/ja not_active Expired - Fee Related
- 2002-12-06 CN CNB028241711A patent/CN1257141C/zh not_active Expired - Fee Related
- 2002-12-06 BR BRPI0214543-0A patent/BR0214543B1/pt not_active IP Right Cessation
- 2002-12-06 WO PCT/EP2002/013882 patent/WO2003048093A2/de active IP Right Grant
- 2002-12-06 AT AT02792927T patent/ATE334957T1/de not_active IP Right Cessation
-
2004
- 2004-05-24 MX MXPA04004920A patent/MXPA04004920A/es active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
AU2002358636A1 (en) | 2003-06-17 |
US20040267055A1 (en) | 2004-12-30 |
US7112707B2 (en) | 2006-09-26 |
JP3923472B2 (ja) | 2007-05-30 |
DE10160180A1 (de) | 2003-06-18 |
BR0214543B1 (pt) | 2013-04-16 |
WO2003048093A3 (de) | 2004-01-15 |
DE50207749D1 (de) | 2006-09-14 |
MXPA04004920A (es) | 2004-08-11 |
ATE334957T1 (de) | 2006-08-15 |
EP1456159B1 (de) | 2006-08-02 |
MY128842A (en) | 2007-02-28 |
JP2005511674A (ja) | 2005-04-28 |
KR20050044718A (ko) | 2005-05-12 |
WO2003048093A2 (de) | 2003-06-12 |
CN1599707A (zh) | 2005-03-23 |
KR100884121B1 (ko) | 2009-02-17 |
EP1456159A2 (de) | 2004-09-15 |
CN1257141C (zh) | 2006-05-24 |
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Legal Events
Date | Code | Title | Description |
---|---|---|---|
B07A | Application suspended after technical examination (opinion) [chapter 7.1 patent gazette] | ||
B09A | Decision: intention to grant [chapter 9.1 patent gazette] | ||
B16A | Patent or certificate of addition of invention granted [chapter 16.1 patent gazette] |
Free format text: PRAZO DE VALIDADE: 10 (DEZ) ANOS CONTADOS A PARTIR DE 16/04/2013, OBSERVADAS AS CONDICOES LEGAIS. |
|
B21F | Lapse acc. art. 78, item iv - on non-payment of the annual fees in time |
Free format text: REFERENTE A 16A ANUIDADE. |
|
B24J | Lapse because of non-payment of annual fees (definitively: art 78 iv lpi, resolution 113/2013 art. 12) |
Free format text: EM VIRTUDE DA EXTINCAO PUBLICADA NA RPI 2494 DE 23-10-2018 E CONSIDERANDO AUSENCIA DE MANIFESTACAO DENTRO DOS PRAZOS LEGAIS, INFORMO QUE CABE SER MANTIDA A EXTINCAO DA PATENTE E SEUS CERTIFICADOS, CONFORME O DISPOSTO NO ARTIGO 12, DA RESOLUCAO 113/2013. |