MX9300333A - Proceso continuo para la fabricacion de polimeros de lactida con metodos de purificacion mejorados. - Google Patents
Proceso continuo para la fabricacion de polimeros de lactida con metodos de purificacion mejorados.Info
- Publication number
- MX9300333A MX9300333A MX9300333A MX9300333A MX9300333A MX 9300333 A MX9300333 A MX 9300333A MX 9300333 A MX9300333 A MX 9300333A MX 9300333 A MX9300333 A MX 9300333A MX 9300333 A MX9300333 A MX 9300333A
- Authority
- MX
- Mexico
- Prior art keywords
- lactide
- manufacture
- continuous process
- purification methods
- mixture
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/78—Preparation processes
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/06—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from hydroxycarboxylic acids
-
- C—CHEMISTRY; METALLURGY
- C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
- C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
- C08G63/00—Macromolecular compounds obtained by reactions forming a carboxylic ester link in the main chain of the macromolecule
- C08G63/02—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds
- C08G63/06—Polyesters derived from hydroxycarboxylic acids or from polycarboxylic acids and polyhydroxy compounds derived from hydroxycarboxylic acids
- C08G63/08—Lactones or lactides
Landscapes
- Chemical & Material Sciences (AREA)
- Health & Medical Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Medicinal Chemistry (AREA)
- Polymers & Plastics (AREA)
- Organic Chemistry (AREA)
- Polyesters Or Polycarbonates (AREA)
- Heterocyclic Compounds That Contain Two Or More Ring Oxygen Atoms (AREA)
Abstract
Esta invención se refiere a un proceso para la producción de lactida y de polímeros de lactida, sustancialmente purificados, a partir del ácido de lactida o de un éster de ácido láctico, el proceso incluye los pasos de formar un ácido poliláctico crudo, preferiblemente en la presencia de un medio de catalizador en el caso del éster el ácido láctico, para formar un subproducto de la reacción de condensación y ácido poliláctico, y despolimerizar el ácido láctico para formar la lactida cruda, seguido por la purificación subsiguiente de la lactida cruda en un sistema de destilación. Una lactida purificada luego es polimerizada para formar los polímeros de lactida.
Applications Claiming Priority (5)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US07/825,059 US5142023A (en) | 1992-01-24 | 1992-01-24 | Continuous process for manufacture of lactide polymers with controlled optical purity |
US07/926,901 US5258488A (en) | 1992-01-24 | 1992-08-07 | Continuous process for manufacture of lactide polymers with controlled optical purity |
US07/927,149 US5247058A (en) | 1992-01-24 | 1992-08-07 | Continuous process for manufacture of lactide polymers with controlled optical purity |
US07/935,566 US5247059A (en) | 1992-01-24 | 1992-08-24 | Continuous process for the manufacture of a purified lactide from esters of lactic acid |
US07/935,059 US5274073A (en) | 1992-01-24 | 1992-08-24 | Continuous process for manufacture of a purified lactide |
Publications (1)
Publication Number | Publication Date |
---|---|
MX9300333A true MX9300333A (es) | 1993-07-01 |
Family
ID=27542241
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX9300333A MX9300333A (es) | 1992-01-24 | 1993-01-22 | Proceso continuo para la fabricacion de polimeros de lactida con metodos de purificacion mejorados. |
Country Status (14)
Country | Link |
---|---|
EP (2) | EP0623153A1 (es) |
JP (1) | JP3258324B2 (es) |
KR (1) | KR100261850B1 (es) |
AT (1) | ATE466897T1 (es) |
AU (1) | AU677174B2 (es) |
BR (1) | BR9305788A (es) |
CA (1) | CA2128509C (es) |
DE (1) | DE69334330D1 (es) |
ES (1) | ES2345307T3 (es) |
FI (1) | FI113661B (es) |
MX (1) | MX9300333A (es) |
NO (1) | NO309530B1 (es) |
NZ (1) | NZ249033A (es) |
WO (1) | WO1993015127A1 (es) |
Families Citing this family (50)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US6326458B1 (en) * | 1992-01-24 | 2001-12-04 | Cargill, Inc. | Continuous process for the manufacture of lactide and lactide polymers |
US5521278A (en) * | 1994-08-18 | 1996-05-28 | Ecological Chemical Products | Integrated process for the manufacture of lactide |
JP3301311B2 (ja) * | 1996-05-24 | 2002-07-15 | 株式会社神戸製鋼所 | 2−ヒドロキシカルボン酸オリゴマーの連続製造方法 |
JPH10109983A (ja) * | 1996-10-04 | 1998-04-28 | Mitsubishi Gas Chem Co Inc | 環状エステルの製造方法および精製方法 |
JP4284709B2 (ja) * | 1996-12-25 | 2009-06-24 | トヨタ自動車株式会社 | 乳酸系副産物の再生利用法 |
DE60031897T2 (de) | 1999-06-18 | 2007-09-06 | Toray Industries, Inc. | Polymilchsäureharz, damit erhaltene Textilerzeugnisse und Verfahren zur Herstellung derselben |
FR2802923B1 (fr) | 1999-12-28 | 2002-03-08 | Roquette Freres | Procede de preparation d'une composition d'ester d'acide lactique et son utilisation en tant que solvant |
EP1357119B1 (en) * | 2001-01-31 | 2011-05-11 | Toyota Jidosha Kabushiki Kaisha | Process for producing lactide and process for producing polylactic acid starting with fermented lactic acid |
BE1015060A3 (fr) * | 2002-08-06 | 2004-09-07 | Brussels Biotech Nv Sa | Procede de production de polylactide au depart d'une solution d'acide lactique ou d'un de ses derives. |
DE60320282T2 (de) * | 2002-10-08 | 2009-07-16 | Kureha Corp. | Verfahren zur herstellung von aliphatischem polyester |
US7829507B2 (en) | 2003-09-17 | 2010-11-09 | Halliburton Energy Services Inc. | Subterranean treatment fluids comprising a degradable bridging agent and methods of treating subterranean formations |
US7674753B2 (en) | 2003-09-17 | 2010-03-09 | Halliburton Energy Services, Inc. | Treatment fluids and methods of forming degradable filter cakes comprising aliphatic polyester and their use in subterranean formations |
US7833944B2 (en) | 2003-09-17 | 2010-11-16 | Halliburton Energy Services, Inc. | Methods and compositions using crosslinked aliphatic polyesters in well bore applications |
US8030249B2 (en) | 2005-01-28 | 2011-10-04 | Halliburton Energy Services, Inc. | Methods and compositions relating to the hydrolysis of water-hydrolysable materials |
US20060169182A1 (en) | 2005-01-28 | 2006-08-03 | Halliburton Energy Services, Inc. | Methods and compositions relating to the hydrolysis of water-hydrolysable materials |
US7662753B2 (en) | 2005-05-12 | 2010-02-16 | Halliburton Energy Services, Inc. | Degradable surfactants and methods for use |
US7318474B2 (en) | 2005-07-11 | 2008-01-15 | Halliburton Energy Services, Inc. | Methods and compositions for controlling formation fines and reducing proppant flow-back |
US8329621B2 (en) | 2006-07-25 | 2012-12-11 | Halliburton Energy Services, Inc. | Degradable particulates and associated methods |
US7686080B2 (en) | 2006-11-09 | 2010-03-30 | Halliburton Energy Services, Inc. | Acid-generating fluid loss control additives and associated methods |
NL2000454C1 (nl) | 2006-11-28 | 2008-01-02 | Purac Biochem Bv | Stabiele lactidedeeltjes. |
US20080146822A1 (en) | 2006-11-28 | 2008-06-19 | Purac Biochem B.V. | Stable lactide particles |
EP2031009A1 (de) * | 2007-09-03 | 2009-03-04 | Uhde Inventa-Fischer GmbH | Reinigungsvorrichtung zur Abtrennung von Dilactid aus Stoffgemischen, Polymerisationsvorrichtung, Verfahren zur Abtrennung von Dilactid aus Stoffgemischen sowie Verwendung |
JP4427571B2 (ja) | 2007-11-07 | 2010-03-10 | 株式会社日立プラントテクノロジー | ポリマー合成に関する装置および方法 |
AT506038B1 (de) | 2007-11-14 | 2015-02-15 | Jungbunzlauer Austria Ag | Verfahren zur herstellung zyklischer diester von l-, d- und d,l-milchsäure |
US8006760B2 (en) * | 2008-04-10 | 2011-08-30 | Halliburton Energy Services, Inc. | Clean fluid systems for partial monolayer fracturing |
AT506768B1 (de) | 2008-04-16 | 2013-10-15 | Jungbunzlauer Austria Ag | Verfahren zur reinigung zyklischer diester der l- bzw. d-milchsäure |
US7906464B2 (en) | 2008-05-13 | 2011-03-15 | Halliburton Energy Services, Inc. | Compositions and methods for the removal of oil-based filtercakes |
KR101012483B1 (ko) * | 2008-07-08 | 2011-02-09 | 김용환 | 효소 전환반응을 이용한 광학순수형 락티드 제조방법 및광학순수형 유산 또는 알킬 락테이트의 분리방법 |
JP5077170B2 (ja) | 2008-09-22 | 2012-11-21 | 株式会社日立プラントテクノロジー | ポリヒドロキシカルボン酸の製造方法 |
US7833943B2 (en) | 2008-09-26 | 2010-11-16 | Halliburton Energy Services Inc. | Microemulsifiers and methods of making and using same |
CN102439001B (zh) * | 2009-03-13 | 2014-09-17 | 自然工作有限责任公司 | 由内消旋-丙交酯流回收乳酸值 |
US8082992B2 (en) | 2009-07-13 | 2011-12-27 | Halliburton Energy Services, Inc. | Methods of fluid-controlled geometry stimulation |
AU2009352300B2 (en) * | 2009-09-14 | 2014-01-23 | Joseph Daniel Cook | Method for wet flue gas desulfurization |
CN101696203B (zh) * | 2009-10-26 | 2013-02-06 | 江苏科技大学 | 从粗l-丙交酯连续精制l-丙交酯的方法 |
BRPI1004962A2 (pt) * | 2010-08-20 | 2012-05-29 | Companhia Refinadora Da Amazonia | processo de produção de poli (ácido lático ) e reatores para utilização no referido processo |
JP2012097224A (ja) * | 2010-11-04 | 2012-05-24 | Hitachi Plant Technologies Ltd | ポリヒドロキシカルボン酸の製造装置および製造方法 |
EP2559725B1 (de) | 2011-08-19 | 2024-05-08 | Uhde Inventa-Fischer GmbH | Verfahren und Vorrichtung zur Rückgewinnung von Lactid aus Polylactid bzw. Glycolid aus Polyglycolid |
ES2536294T3 (es) | 2012-10-26 | 2015-05-22 | Uhde Inventa-Fischer Gmbh | Procedimiento para preparar diésteres cíclicos, especialmente dilactida |
KR101434462B1 (ko) * | 2012-12-26 | 2014-08-26 | 한국화학연구원 | 락타이드의 회분식 증류정제장치 및 이를 이용한 락타이드의 증류정제방법 |
EP2876124B1 (de) * | 2013-11-20 | 2019-01-09 | Uhde Inventa-Fischer GmbH | Verfahren sowie vorrichtung zur herstellung einer kristallisierbaren polymilchsäuremischung sowie polymilchsäuremischung |
WO2015086613A1 (en) * | 2013-12-10 | 2015-06-18 | Futerro S.A. | Improved process for producing polylactide |
EP3056490A1 (en) * | 2015-02-13 | 2016-08-17 | PURAC Biochem BV | Method for manufacturing lactide |
EP3288930B1 (en) * | 2015-04-30 | 2021-04-21 | PURAC Biochem BV | Method and device for manufacturing lactide |
KR101780779B1 (ko) | 2015-09-24 | 2017-09-21 | 롯데케미칼 주식회사 | 고순도 락타이드의 제조 방법 |
KR101704563B1 (ko) | 2015-10-12 | 2017-02-08 | 한국화학연구원 | 락타이드 정제공정을 이용한 락타이드 제조방법 및 제조장치 |
US10562877B2 (en) * | 2016-06-20 | 2020-02-18 | Total Research & Technology Feluy | Single step lactide production process with hydrolysis of oligomers and catalyst by recovered water |
EP3406605B1 (en) * | 2017-05-22 | 2022-04-20 | NatureWorks LLC | Methods for producing lactide with recrystallization and recycle of meso-lactide |
CN110652946B (zh) * | 2019-09-24 | 2021-11-09 | 安徽神剑新材料股份有限公司 | 一种聚酯树脂生产过程中顶温控制系统及方法 |
CN116635376A (zh) * | 2020-12-24 | 2023-08-22 | 聚晟(新加坡)私人有限公司 | 丙交酯的生产工艺 |
JP2024518184A (ja) * | 2021-02-22 | 2024-04-25 | 聚晟(新加坡)私人有限公司 | ラクチドを製造する方法及び装置 |
Family Cites Families (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US1995970A (en) * | 1931-04-04 | 1935-03-26 | Du Pont | Polymeric lactide resin |
DE3708915C2 (de) * | 1987-03-19 | 1996-04-04 | Boehringer Ingelheim Kg | Verfahren zur Herstellung von Lactid |
EP0261572A1 (de) * | 1986-09-20 | 1988-03-30 | Boehringer Ingelheim Kg | Verfahren zur Herstellung von Lactid |
ES2052551T3 (es) * | 1986-12-19 | 1994-07-16 | Akzo Nv | Metodo para preparar poli(acido lactico) o copolimeros de poli(acido lactico) por polimeracion de la lactida. |
DE3869343D1 (de) * | 1987-06-16 | 1992-04-23 | Boehringer Ingelheim Kg | Meso-lactid und verfahren zu seiner herstellung. |
NL8702563A (nl) | 1987-10-28 | 1989-05-16 | Cca Biochem B V | Polymeer lactide, werkwijze voor het bereiden van een dergelijk polymeer lactide, alsmede een samenstelling, die een dergelijk polymeer lactide bevat. |
-
1993
- 1993-01-22 EP EP93903632A patent/EP0623153A1/en not_active Ceased
- 1993-01-22 KR KR1019940702555A patent/KR100261850B1/ko not_active IP Right Cessation
- 1993-01-22 MX MX9300333A patent/MX9300333A/es unknown
- 1993-01-22 AU AU34821/93A patent/AU677174B2/en not_active Ceased
- 1993-01-22 AT AT98203427T patent/ATE466897T1/de not_active IP Right Cessation
- 1993-01-22 CA CA002128509A patent/CA2128509C/en not_active Expired - Fee Related
- 1993-01-22 ES ES98203427T patent/ES2345307T3/es not_active Expired - Lifetime
- 1993-01-22 EP EP98203427A patent/EP0893462B1/en not_active Expired - Lifetime
- 1993-01-22 WO PCT/US1993/000568 patent/WO1993015127A1/en active IP Right Grant
- 1993-01-22 DE DE69334330T patent/DE69334330D1/de not_active Expired - Lifetime
- 1993-01-22 NZ NZ249033A patent/NZ249033A/en not_active IP Right Cessation
- 1993-01-22 JP JP51333593A patent/JP3258324B2/ja not_active Expired - Fee Related
- 1993-01-22 BR BR9305788A patent/BR9305788A/pt not_active IP Right Cessation
-
1994
- 1994-07-21 NO NO942728A patent/NO309530B1/no not_active IP Right Cessation
- 1994-07-22 FI FI943487A patent/FI113661B/fi not_active Application Discontinuation
Also Published As
Publication number | Publication date |
---|---|
FI113661B (fi) | 2004-05-31 |
FI943487A (fi) | 1994-09-21 |
CA2128509A1 (en) | 1993-08-05 |
NO309530B1 (no) | 2001-02-12 |
BR9305788A (pt) | 1997-02-18 |
EP0623153A1 (en) | 1994-11-09 |
AU677174B2 (en) | 1997-04-17 |
CA2128509C (en) | 2006-09-19 |
NO942728D0 (no) | 1994-07-21 |
KR100261850B1 (ko) | 2000-08-01 |
FI943487A0 (fi) | 1994-07-22 |
NO942728L (no) | 1994-09-23 |
AU3482193A (en) | 1993-09-01 |
ATE466897T1 (de) | 2010-05-15 |
EP0893462A3 (en) | 1999-10-20 |
EP0893462A2 (en) | 1999-01-27 |
DE69334330D1 (de) | 2010-06-17 |
WO1993015127A1 (en) | 1993-08-05 |
ES2345307T3 (es) | 2010-09-20 |
EP0893462B1 (en) | 2010-05-05 |
JPH07503490A (ja) | 1995-04-13 |
NZ249033A (en) | 1996-05-28 |
JP3258324B2 (ja) | 2002-02-18 |
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