MX377665B - Metodo para preparar oxisulfuro y derivados fluorados mediante sulfinacion. - Google Patents

Metodo para preparar oxisulfuro y derivados fluorados mediante sulfinacion.

Info

Publication number
MX377665B
MX377665B MX2016003205A MX2016003205A MX377665B MX 377665 B MX377665 B MX 377665B MX 2016003205 A MX2016003205 A MX 2016003205A MX 2016003205 A MX2016003205 A MX 2016003205A MX 377665 B MX377665 B MX 377665B
Authority
MX
Mexico
Prior art keywords
sulphur oxide
oxysulphide
preparing
sulfination
compound
Prior art date
Application number
MX2016003205A
Other languages
English (en)
Other versions
MX2016003205A (es
Inventor
Denis Revelant
François Metz
Marie Chauve
Valery Dambrin
Original Assignee
Rhodia Operations
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Rhodia Operations filed Critical Rhodia Operations
Publication of MX2016003205A publication Critical patent/MX2016003205A/es
Publication of MX377665B publication Critical patent/MX377665B/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C313/00—Sulfinic acids; Sulfenic acids; Halides, esters or anhydrides thereof; Amides of sulfinic or sulfenic acids, i.e. compounds having singly-bound oxygen atoms of sulfinic or sulfenic groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C313/02—Sulfinic acids; Derivatives thereof
    • C07C313/04—Sulfinic acids; Esters thereof
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
    • B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
    • B01J31/0215—Sulfur-containing compounds
    • B01J31/0225—Sulfur-containing compounds comprising sulfonic acid groups or the corresponding salts
    • B01J31/0227—Sulfur-containing compounds comprising sulfonic acid groups or the corresponding salts being perfluorinated, i.e. comprising at least one perfluorinated moiety as substructure in case of polyfunctional compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/02—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of sulfonic acids or halides thereof
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C303/00—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides
    • C07C303/32—Preparation of esters or amides of sulfuric acids; Preparation of sulfonic acids or of their esters, halides, anhydrides or amides of salts of sulfonic acids
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C313/00—Sulfinic acids; Sulfenic acids; Halides, esters or anhydrides thereof; Amides of sulfinic or sulfenic acids, i.e. compounds having singly-bound oxygen atoms of sulfinic or sulfenic groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C313/02—Sulfinic acids; Derivatives thereof
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Catalysts (AREA)

Abstract

Se describe un procedimiento de preparación de un derivado oxisulfurado y fluorado que comprende hacer reaccionar, en presencia de un disolvente orgánico: i) Al menos un compuesto de fórmula Ea-COOR (I), donde Ea representa al átomo de flúor o un grupo que tiene de 1 a 10 átomos de carbono seleccionado de los fluoroalquilos, los perfluoroalquilos y los fluoroalquenilos y R representa hidrógeno, un catión monovalente o un grupo alquilo, y ii) Un óxido de azufre, siendo dicho procedimiento tal que la razón molar inicial (óxido de azufre/compuesto de fórmula (I) es inferior a 0.4 y la concentración de óxido de azufre disuelto en el medio de reacción se mantiene constante durante toda la duración de la reacción a un valor comprendido entre el 00.2% y el 3% en peso mediante una adición continua de dicho óxido de azufre al medio de reacción.
MX2016003205A 2013-09-12 2014-09-11 Metodo para preparar oxisulfuro y derivados fluorados mediante sulfinacion. MX377665B (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
FR1302126A FR3010407B1 (fr) 2013-09-12 2013-09-12 Procede de preparation de derives oxysulfures et fluores par sulfination
PCT/EP2014/069436 WO2015036504A1 (fr) 2013-09-12 2014-09-11 Procede de preparation de derives oxysulfures et fluores par sulfination

Publications (2)

Publication Number Publication Date
MX2016003205A MX2016003205A (es) 2016-08-11
MX377665B true MX377665B (es) 2025-03-11

Family

ID=49578348

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2016003205A MX377665B (es) 2013-09-12 2014-09-11 Metodo para preparar oxisulfuro y derivados fluorados mediante sulfinacion.

Country Status (10)

Country Link
US (1) US9873666B2 (es)
EP (1) EP3044205B1 (es)
JP (1) JP6463364B2 (es)
KR (1) KR102181926B1 (es)
CN (1) CN105722821B (es)
BR (1) BR112016005473B1 (es)
CA (1) CA2923347C (es)
FR (1) FR3010407B1 (es)
MX (1) MX377665B (es)
WO (1) WO2015036504A1 (es)

Families Citing this family (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
EP3412659A1 (en) 2017-06-09 2018-12-12 Solvay Sa Processes for the manufacture of sulfur-substituted pyrazole derivatives
CN117326989A (zh) * 2023-09-26 2024-01-02 衢州市九洲化工有限公司 一种利用微通道反应装置将含氟羧酸钾盐直接硫化制备含氟亚磺酸盐的工艺技术

Family Cites Families (13)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
SK286140B6 (sk) * 1995-03-24 2008-04-07 Rhone-Poulenc Agrochimie Reakčné činidlo na použitie pri príprave derivátov organických zlúčenín s oxidovanou sírnou skupinou a fluorovaných a spôsob ich prípravy
AU728097B2 (en) * 1996-08-01 2001-01-04 Rhodia Chimie Process for grafting a substituted difluoromethyle group
JP3169171B2 (ja) * 1996-10-15 2001-05-21 セントラル硝子株式会社 高純度フルオロアルキルスルホン酸無水物の製造方法
GB0026012D0 (en) * 2000-10-24 2000-12-13 Air Prod & Chem Electrophilic fluorination
FR2900403B1 (fr) * 2006-04-26 2008-07-11 Rhodia Recherches & Tech Procede de preparation de derives organiques oxysulfures et fluores
FR2904313A1 (fr) 2006-07-27 2008-02-01 Rhodia Recherches & Tech Procede de preparation d'un anhydride d'acide sulfonique
US20090137840A1 (en) * 2007-11-28 2009-05-28 E. I. Du Pont De Nemours And Company Fluorinated Alkanesulfonic Acid Anhydrides and Processes for Making the Same
CN102786450A (zh) * 2008-12-05 2012-11-21 华中科技大学 一种碱金属盐的制备方法
JP2010159242A (ja) * 2008-12-12 2010-07-22 Mitsubishi Materials Corp 含フッ素ｎ−アルキルスルホニルイミド化合物及びその製造方法、並びにイオン性化合物の製造方法
JP5169880B2 (ja) * 2009-01-29 2013-03-27 セントラル硝子株式会社 トリフルオロメタンスルホニルフルオリドの精製方法
CN102365266B (zh) * 2009-03-31 2013-11-06 三菱综合材料株式会社 含氟n-烷基磺酰亚胺化合物及其制造方法、以及离子性化合物的制造方法
JP5460190B2 (ja) * 2009-09-07 2014-04-02 住化スタイロンポリカーボネート株式会社 帯電防止性ポリカーボネート樹脂組成物
CN102153493A (zh) * 2011-03-04 2011-08-17 孙乐群 一种新型的制备二(三氟甲基磺酰)亚胺锂的方法

Also Published As

Publication number Publication date
JP6463364B2 (ja) 2019-01-30
CA2923347C (fr) 2022-10-18
FR3010407B1 (fr) 2015-09-04
CN105722821A (zh) 2016-06-29
JP2016535067A (ja) 2016-11-10
EP3044205A1 (fr) 2016-07-20
US20160221939A1 (en) 2016-08-04
MX2016003205A (es) 2016-08-11
BR112016005473B1 (pt) 2020-10-20
EP3044205B1 (fr) 2017-12-27
WO2015036504A1 (fr) 2015-03-19
FR3010407A1 (fr) 2015-03-13
CN105722821B (zh) 2018-09-18
US9873666B2 (en) 2018-01-23
KR102181926B1 (ko) 2020-11-23
CA2923347A1 (fr) 2015-03-19
KR20160058127A (ko) 2016-05-24

Similar Documents

Publication Publication Date Title
CY1120188T1 (el) ΠΑΡΑΓΩΓΑ ΝΑΦΘΥΡΙΔΙΝΗΣ ΧΡΗΣΙΜΑ ΩΣ ΑΝΤΑΓΩΝΙΣΤΕΣ ΙΝΤΕΓΚΡΙΝΗΣ αvβ6
BR112016002083A2 (pt) composto tetrazolinona e uso para o mesmo
MX2020005077A (es) Compuestos con acción estabilizadora, procedimiento para su preparación, composición que contiene estos compuestos estabilizadores, procedimiento para la estabilización de un componente orgánico así como uso de compuestos estabilizadores.
MX353957B (es) Carboxamidas heterociclicas fungicidas.
MX2018016267A (es) Metodo para producir derivado de piridona policiclica sustituida y cristal del mismo.
MX2018001734A (es) Derivados de 3-fenil-benzofuran-2-ona que contienen fosforo como estabilizantes.
MX380421B (es) Compuestos herbicidas de pirimidiniloxi benceno sustituido.
MX347476B (es) Compuestos de ácido dimetil-benzoico.
BR112012031314A2 (pt) "processo de preparo de compostos esteramidas"
MX390748B (es) Composiciones y metodos para tratar accidente cerebrovascular isquemico.
CY1121626T1 (el) Νεο παραγωγο υδροξαμικου οξεος ή αλας αυτου
EA201391214A1 (ru) Композиции, содержащие алкилалкоксисульфонаты, для производства термостабильных пен
MX377665B (es) Metodo para preparar oxisulfuro y derivados fluorados mediante sulfinacion.
BR112015007467A2 (pt) composto de imida, método para a fabricação do mesmo e uso como inseticida
BR112019001015A2 (pt) composto de benzilamida, método para produção do mesmo, e miticida
BR112016026310A8 (pt) processo para a reação de compostos químicos
MY170131A (en) Tracers and method of marking hydrocarbon liquids
CO2018007668A2 (es) Composición para el control de plagas y método para el control de plagas
BR112017003121A2 (pt) método para a síntese de um óxido de fosfina de hidrogênio heterocíclico
PL410423A1 (pl) 4-chloro-2-metylofenoksyoctany alkoksymetylobis(2-hydroksyetylo)metyloamoniowe,  sposób otrzymywania i zastosowanie jako środków  ochrony roślin
AR096373A1 (es) Método para producir compuesto de piridazina
MX382813B (es) Agente retardante de flama para resinas, composicion de resina retardante a la flama que contiene el mismo, y metodo para producir compuesto organofosforado.
BR112018067299A2 (pt) método para produção de derivado de sulfóxido
FR2970880B1 (fr) Agents moussants phosphores stables a haute temperature
AR104428A1 (es) Derivados de piridona policíclica sustituida y profármaco de los mismos

Legal Events

Date Code Title Description
FG Grant or registration