MX373387B - Materiales polimericos de ciclodextrina porosa y metodos de fabricacion y uso de los mismos. - Google Patents

Materiales polimericos de ciclodextrina porosa y metodos de fabricacion y uso de los mismos.

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Publication number
MX373387B
MX373387B MX2017013406A MX2017013406A MX373387B MX 373387 B MX373387 B MX 373387B MX 2017013406 A MX2017013406 A MX 2017013406A MX 2017013406 A MX2017013406 A MX 2017013406A MX 373387 B MX373387 B MX 373387B
Authority
MX
Mexico
Prior art keywords
cdps
sorbents
manufacturing
methods
same
Prior art date
Application number
MX2017013406A
Other languages
English (en)
Other versions
MX2017013406A (es
Inventor
Alaaeddin Alsbaiee
Brian J Smith
Damian Helbling
Diego Alzate-Sanchez
Juan Hinestroza
Leilei Xiao
William R Dichtel
Yuhan Ling
Original Assignee
Univ Cornell
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Univ Cornell filed Critical Univ Cornell
Publication of MX2017013406A publication Critical patent/MX2017013406A/es
Publication of MX373387B publication Critical patent/MX373387B/es

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/24—Crosslinking, e.g. vulcanising, of macromolecules
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D15/00—Separating processes involving the treatment of liquids with solid sorbents; Apparatus therefor
    • B01D15/08—Selective adsorption, e.g. chromatography
    • B01D15/26—Selective adsorption, e.g. chromatography characterised by the separation mechanism
    • B01D15/40—Selective adsorption, e.g. chromatography characterised by the separation mechanism using supercritical fluid as mobile phase or eluent
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D53/00—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols
    • B01D53/02—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography
    • B01D53/025—Separation of gases or vapours; Recovering vapours of volatile solvents from gases; Chemical or biological purification of waste gases, e.g. engine exhaust gases, smoke, fumes, flue gases, aerosols by adsorption, e.g. preparative gas chromatography with wetted adsorbents; Chromatography
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    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J20/00—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof
    • B01J20/22—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof comprising organic material
    • B01J20/24—Naturally occurring macromolecular compounds, e.g. humic acids or their derivatives
    • B—PERFORMING OPERATIONS; TRANSPORTING
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    • B01J20/28—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties
    • B01J20/28014—Solid sorbent compositions or filter aid compositions; Sorbents for chromatography; Processes for preparing, regenerating or reactivating thereof characterised by their form or physical properties characterised by their form
    • B01J20/28033—Membrane, sheet, cloth, pad, lamellar or mat
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
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    • B01J20/281—Sorbents specially adapted for preparative, analytical or investigative chromatography
    • B01J20/286—Phases chemically bonded to a substrate, e.g. to silica or to polymers
    • B01J20/289—Phases chemically bonded to a substrate, e.g. to silica or to polymers bonded via a spacer
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    • B01J20/3212—Polymeric carriers, supports or substrates consisting of a polymer obtained by reactions otherwise than involving only carbon to carbon unsaturated bonds
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    • C02F—TREATMENT OF WATER, WASTE WATER, SEWAGE, OR SLUDGE
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  • Materials Engineering (AREA)
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  • Molecular Biology (AREA)
  • Hydrology & Water Resources (AREA)
  • Environmental & Geological Engineering (AREA)
  • Water Supply & Treatment (AREA)
  • General Chemical & Material Sciences (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Inorganic Chemistry (AREA)
  • Thermal Sciences (AREA)
  • Solid-Sorbent Or Filter-Aiding Compositions (AREA)
  • Polysaccharides And Polysaccharide Derivatives (AREA)
  • Separation Of Gases By Adsorption (AREA)
  • Water Treatment By Sorption (AREA)
  • Compositions Of Macromolecular Compounds (AREA)

Abstract

Una reacción de sustitución nucleofílica para degradar el polímero de ciclodextrina (CD) con grupos aromáticos rígidos, proporcionando polímeros que contienen CD mesoporoso de gran área superficial (P-CDPs). Los P-CDPs pueden ser usados para remover contaminantes orgánicos del agua. Encapsulando los contaminantes se forman complejos anfitrión-huésped bien definidos con selectividades complementarias para sorbentes de carbono activado (AC). Los P-CDPs pueden secuestrar rápidamente sustancias farmacéuticas, pesticidas, y otros microcontaminantes orgánicos, logrando capacidad de fijación en equilibrio en segundos con constantes de velocidad de adsorción 15 a 200 veces mayores que los ACs y los sorbentes de CD no porosos. El polímero CD puede regenerarse varias veces, a través del procedimiento de lavado a temperatura ambiente, sin pérdida de eficacia.
MX2017013406A 2015-04-20 2016-04-19 Materiales polimericos de ciclodextrina porosa y metodos de fabricacion y uso de los mismos. MX373387B (es)

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US20160304630A1 (en) 2016-10-20
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