MX368456B - Proceso para preparar fluoxastrobina. - Google Patents
Proceso para preparar fluoxastrobina.Info
- Publication number
- MX368456B MX368456B MX2019000836A MX2019000836A MX368456B MX 368456 B MX368456 B MX 368456B MX 2019000836 A MX2019000836 A MX 2019000836A MX 2019000836 A MX2019000836 A MX 2019000836A MX 368456 B MX368456 B MX 368456B
- Authority
- MX
- Mexico
- Prior art keywords
- methyl
- benzofuran
- reacting
- dioxazin
- dione
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D273/00—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00
- C07D273/01—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00 having one nitrogen atom
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
- C07C251/32—Oximes
- C07C251/34—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals
- C07C251/42—Oximes with oxygen atoms of oxyimino groups bound to hydrogen atoms or to carbon atoms of unsubstituted hydrocarbon radicals with the carbon atom of at least one of the oxyimino groups bound to a carbon atom of a ring other than a six-membered aromatic ring
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D273/00—Heterocyclic compounds containing rings having nitrogen and oxygen atoms as the only ring hetero atoms, not provided for by groups C07D261/00 - C07D271/00
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D413/00—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms
- C07D413/02—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings
- C07D413/12—Heterocyclic compounds containing two or more hetero rings, at least one ring having nitrogen and oxygen atoms as the only ring hetero atoms containing two hetero rings linked by a chain containing hetero atoms as chain links
Landscapes
- Organic Chemistry (AREA)
- Chemical & Material Sciences (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Plural Heterocyclic Compounds (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Life Sciences & Earth Sciences (AREA)
- Heterocyclic Carbon Compounds Containing A Hetero Ring Having Oxygen Or Sulfur (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Agronomy & Crop Science (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Pest Control & Pesticides (AREA)
Abstract
Un proceso para preparar fluoxastrobina, incluyendo: (i) reaccionar benzofuran-3(2H)-ona O-metil oxima (10) con un nitrito de alquilo en presencia de un ácido para formar (3E)-2,3-benzofuran-diona O3-metil dioxima (11A) como un isómero predominante; (ii) reaccionar (3E)-2,3-benzofuran-diona O3-metil dioxima (11A) con 2-haloetanol para formar (3E)-benzofuran-2,3-dio na O2-(2-hidroxietil) O3-metil dioxima (12A); y (iii) reaccionar (3E)-benzofuran-2,3-diona O2-(2-hidroetil) O3-metil dioxima (12A) con una base para formar (E)-(5,6-dihidro-1,4,2-dioxazin-3-il)(2-h idroxifenil)metanona O-metil oxima (13) (iv) reaccionar una 4,6-di-halo-5-fluoro-pirimidina (5), en donde X1 es halógeno, con (E)-(5,6-dihidro-1,4,2-dioxazi n-3-il)(2-hidroxifenil)metanona O-metil oxima (13) en presencia de un solvente y opcionalmente en presencia de una base para formar una (E)-(2-((6-halo-5-fluoropiri midina-4-il)oxi)fenil)5,6-dihidro-1,4,2-dioxazin-3-il)metanona O-metil oxima (14): (v) reaccionar la (E)-2-((6-halo-5-fluoropirim idina-4-il)oxi)fenil)(5,6-dihidro-1,4,2-dioxazin-3-il)metanona O-metil oxima (14) con 2-clorofenol en presencia de un solvente y opcionalmente en presencia de una base para formar fluoxastrobina.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201361843656P | 2013-07-08 | 2013-07-08 | |
PCT/US2014/045556 WO2015006203A1 (en) | 2013-07-08 | 2014-07-07 | Process for preparing fluoxastrobin |
Publications (1)
Publication Number | Publication Date |
---|---|
MX368456B true MX368456B (es) | 2019-10-03 |
Family
ID=52133244
Family Applications (2)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2016000315A MX364158B (es) | 2013-07-08 | 2014-07-07 | Proceso para preparar fluoxastrobina. |
MX2019000836A MX368456B (es) | 2013-07-08 | 2014-07-07 | Proceso para preparar fluoxastrobina. |
Family Applications Before (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2016000315A MX364158B (es) | 2013-07-08 | 2014-07-07 | Proceso para preparar fluoxastrobina. |
Country Status (14)
Country | Link |
---|---|
US (2) | US9193698B2 (es) |
EP (2) | EP3699178A1 (es) |
CN (1) | CN105518003B (es) |
AR (1) | AR100015A1 (es) |
AU (1) | AU2014287480B2 (es) |
BR (5) | BR122021013388B1 (es) |
CA (1) | CA2917707C (es) |
HU (1) | HUE051610T2 (es) |
IL (1) | IL243455B (es) |
MX (2) | MX364158B (es) |
PL (1) | PL3019495T3 (es) |
RU (1) | RU2653542C2 (es) |
UA (1) | UA115093C2 (es) |
WO (1) | WO2015006203A1 (es) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR112017025678B1 (pt) * | 2015-05-29 | 2021-12-28 | Arysta Lifescience Corporation | Processo aprimorado para preparação de (e)-(5,6-di-hidro1,4,2-dioxazina-3-il)(2-hidroxifenil) metanona o-metil oxima |
CN107235920A (zh) * | 2017-07-29 | 2017-10-10 | 江苏绿叶农化有限公司 | 一种嘧菌酯的合成方法 |
CA3136883A1 (en) * | 2019-04-18 | 2020-10-22 | Upl Limited | Process for the preparation of fungicidally active strobilurin compounds and intermediates thereof |
JP2023528526A (ja) * | 2020-06-08 | 2023-07-04 | ユーピーエル リミテッド | フルオキサストロビン及びその中間体を調製するためのプロセス |
Family Cites Families (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4136694C2 (de) | 1991-11-07 | 1996-10-10 | Inventa Ag | Stärkefaser oder Stärke-modifizierte Faser, Verfahren zu ihrer Herstellung sowie ihre Verwendung |
DE4237882A1 (de) | 1992-11-10 | 1994-05-11 | Bayer Ag | Verfahren zur Herstellung von alpha-Fluor-beta-dicarbonylverbindungen |
DE4408005A1 (de) | 1993-08-11 | 1995-02-16 | Bayer Ag | Substituierte Azadioxacycloalkene |
ZW8594A1 (en) | 1993-08-11 | 1994-10-12 | Bayer Ag | Substituted azadioxacycbalkenes |
DE19602095A1 (de) | 1996-01-22 | 1997-07-24 | Bayer Ag | Halogenpyrimidine |
TW492962B (en) | 1996-05-30 | 2002-07-01 | Bayer Ag | Process for preparing 3-(1-hydroxyphenyl-1-alkoximinomethyl)dioxazines |
DE19706396A1 (de) | 1996-12-09 | 1998-06-10 | Bayer Ag | Verfahren zur Herstellung von 3-(l-Hydroxiphenyl-l-alkoximinomethyl)dioxazinen |
DE19739982A1 (de) | 1996-12-10 | 1998-06-18 | Bayer Ag | Fungizide Wirkstoffkombinationen |
DE19710609A1 (de) | 1997-03-14 | 1998-09-17 | Bayer Ag | Substituierte Aminosalicylsäureamide |
EP1003742A1 (de) | 1997-08-14 | 2000-05-31 | Bayer Aktiengesellschaft | Methoximinomethyloxadiazine als pestizide |
DE19744705A1 (de) | 1997-10-10 | 1999-04-15 | Bayer Ag | Verfahren zur Herstellung gegebenenfalls substituierter Benzofuranone |
KR100676222B1 (ko) | 1999-08-18 | 2007-01-30 | 바이엘 악티엔게젤샤프트 | 4,6-디클로로-5-플루오로피리미딘의 제조방법 |
DE19954936A1 (de) | 1999-11-16 | 2001-05-17 | Bayer Ag | Verfahren zur Herstellung von Benzofuranonoximen |
DE10014607A1 (de) | 2000-03-24 | 2001-09-27 | Bayer Ag | Verfahren zur Herstellung von unsymmetrischen 4,6-Bis(aryloxy pyrimidin-Derivaten |
TWI312274B (en) * | 2001-08-13 | 2009-07-21 | Du Pont | Method for controlling particular insect pests by applying anthranilamide compounds |
DE10226220A1 (de) | 2002-06-13 | 2003-12-24 | Bayer Cropscience Ag | Verfahren zur Herstellung von 4,6-Dichlor-5-fluorpyrimidin |
DE10337885A1 (de) | 2003-08-18 | 2005-03-24 | Bayer Cropscience Ag | Verfahren zur Herstellung von α-Fluormalonsäuredialkylestern |
DE102004040702B4 (de) | 2004-08-23 | 2019-03-28 | Bayer Cropscience Aktiengesellschaft | Verfahren zur Herstellung eines Dioxazin-Derivats |
DE102004049761A1 (de) | 2004-10-12 | 2006-04-13 | Bayer Cropscience Ag | Fungizide Wirkstoffkombinationen |
-
2014
- 2014-07-03 US US14/323,413 patent/US9193698B2/en active Active
- 2014-07-03 AR ARP140102483A patent/AR100015A1/es unknown
- 2014-07-07 PL PL14822781T patent/PL3019495T3/pl unknown
- 2014-07-07 AU AU2014287480A patent/AU2014287480B2/en active Active
- 2014-07-07 EP EP20170142.2A patent/EP3699178A1/en not_active Withdrawn
- 2014-07-07 WO PCT/US2014/045556 patent/WO2015006203A1/en active Application Filing
- 2014-07-07 EP EP14822781.2A patent/EP3019495B1/en active Active
- 2014-07-07 BR BR122021013388-3A patent/BR122021013388B1/pt active IP Right Grant
- 2014-07-07 BR BR112016000445-0A patent/BR112016000445B1/pt active IP Right Grant
- 2014-07-07 MX MX2016000315A patent/MX364158B/es active IP Right Grant
- 2014-07-07 BR BR122021013386-7A patent/BR122021013386B1/pt active IP Right Grant
- 2014-07-07 RU RU2016102192A patent/RU2653542C2/ru active
- 2014-07-07 UA UAA201600290A patent/UA115093C2/uk unknown
- 2014-07-07 CA CA2917707A patent/CA2917707C/en active Active
- 2014-07-07 BR BR122021013389-1A patent/BR122021013389B1/pt active IP Right Grant
- 2014-07-07 MX MX2019000836A patent/MX368456B/es unknown
- 2014-07-07 CN CN201480047316.4A patent/CN105518003B/zh active Active
- 2014-07-07 BR BR122021013387-5A patent/BR122021013387B1/pt active IP Right Grant
- 2014-07-07 HU HUE14822781A patent/HUE051610T2/hu unknown
-
2015
- 2015-10-23 US US14/921,657 patent/US9670171B2/en active Active
-
2016
- 2016-01-04 IL IL243455A patent/IL243455B/en active IP Right Grant
Also Published As
Publication number | Publication date |
---|---|
MX364158B (es) | 2019-04-15 |
EP3019495A4 (en) | 2017-03-15 |
BR122021013386B1 (pt) | 2023-05-16 |
AU2014287480B2 (en) | 2016-11-03 |
EP3699178A1 (en) | 2020-08-26 |
MX2016000315A (es) | 2016-11-14 |
BR122021013389B1 (pt) | 2021-08-31 |
EP3019495B1 (en) | 2020-06-03 |
AU2014287480A1 (en) | 2016-02-04 |
PL3019495T3 (pl) | 2021-01-25 |
IL243455B (en) | 2018-08-30 |
BR122021013388B1 (pt) | 2021-09-28 |
CN105518003B (zh) | 2018-02-13 |
US9670171B2 (en) | 2017-06-06 |
UA115093C2 (uk) | 2017-09-11 |
US9193698B2 (en) | 2015-11-24 |
WO2015006203A1 (en) | 2015-01-15 |
RU2016102192A (ru) | 2017-08-11 |
US20160237047A1 (en) | 2016-08-18 |
EP3019495A1 (en) | 2016-05-18 |
US20150011753A1 (en) | 2015-01-08 |
CN105518003A (zh) | 2016-04-20 |
HUE051610T2 (hu) | 2021-03-01 |
AR100015A1 (es) | 2016-09-07 |
CA2917707A1 (en) | 2015-01-15 |
CA2917707C (en) | 2018-04-10 |
BR122021013387B1 (pt) | 2022-12-27 |
BR112016000445A2 (pt) | 2017-07-25 |
RU2653542C2 (ru) | 2018-05-11 |
BR112016000445B1 (pt) | 2021-08-17 |
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