MX338962B - Proceso para la preparacion de 4-amio-5-fluor-3-halo-6-picolinatos (substituido). - Google Patents
Proceso para la preparacion de 4-amio-5-fluor-3-halo-6-picolinatos (substituido).Info
- Publication number
- MX338962B MX338962B MX2013008602A MX2013008602A MX338962B MX 338962 B MX338962 B MX 338962B MX 2013008602 A MX2013008602 A MX 2013008602A MX 2013008602 A MX2013008602 A MX 2013008602A MX 338962 B MX338962 B MX 338962B
- Authority
- MX
- Mexico
- Prior art keywords
- picolinates
- halo
- fluoro
- amino
- preparation
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/81—Amides; Imides
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/79—Acids; Esters
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
- C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
- C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
- C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
- C07D213/79—Acids; Esters
- C07D213/803—Processes of preparation
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Pyridine Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
Abstract
Los 4-amino-5-flúor-3-halo-6-(substituido) picolinatos son convenientemente preparados desde 4,5,6-tricloropicolinonitrilo mediante una serie de pasos que involucran al intercambio de flúor, la aminación, el intercambio de halógeno, la halogenación, la hidrólisis de nitrilo, la esterificación, y el acoplamiento de un metal de transición asistido.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US201161435936P | 2011-01-25 | 2011-01-25 | |
PCT/US2012/022289 WO2012103045A1 (en) | 2011-01-25 | 2012-01-24 | Process for the preparation of 4-amino-5-fluoro-3-halo-6-(substituted)picolinates |
Publications (2)
Publication Number | Publication Date |
---|---|
MX2013008602A MX2013008602A (es) | 2013-12-09 |
MX338962B true MX338962B (es) | 2016-05-06 |
Family
ID=46544650
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
MX2013008602A MX338962B (es) | 2011-01-25 | 2012-01-24 | Proceso para la preparacion de 4-amio-5-fluor-3-halo-6-picolinatos (substituido). |
Country Status (20)
Country | Link |
---|---|
US (2) | US8754231B2 (es) |
EP (1) | EP2667712B1 (es) |
JP (1) | JP5781171B2 (es) |
KR (2) | KR20150013334A (es) |
CN (1) | CN103458689B (es) |
AR (1) | AR085020A1 (es) |
AU (1) | AU2012209281B2 (es) |
BR (2) | BR102012001643A2 (es) |
CA (1) | CA2825468C (es) |
CO (1) | CO6731129A2 (es) |
HK (1) | HK1188684A1 (es) |
IL (1) | IL227647B (es) |
MX (1) | MX338962B (es) |
PL (1) | PL2667712T3 (es) |
RU (1) | RU2542985C1 (es) |
SG (1) | SG192101A1 (es) |
TW (1) | TWI537252B (es) |
UA (1) | UA109806C2 (es) |
WO (1) | WO2012103045A1 (es) |
ZA (1) | ZA201305582B (es) |
Families Citing this family (13)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CA2839627C (en) * | 2011-06-30 | 2021-01-19 | Dow Agrosciences Llc | 3-alkoxy, thioalkyl and amino-4-amino-6-(substituted)picolinates and their use as herbicides |
AR091856A1 (es) | 2012-07-24 | 2015-03-04 | Dow Agrosciences Llc | Proceso para la preparacion de 4-amino-5-fluor-3-halo-6-(substituido) picolinatos |
AR092355A1 (es) | 2012-07-24 | 2015-04-15 | Dow Agrosciences Llc | Fluoruros de fluoropicolinoilo y procesos para su preparacion |
CN106977453A (zh) * | 2012-12-13 | 2017-07-25 | 美国陶氏益农公司 | 制备4‑氨基‑5‑氟‑3‑氯‑6‑(取代的)吡啶甲酸酯的方法 |
BR102014028164A2 (pt) * | 2013-11-12 | 2015-09-08 | Dow Agrosciences Llc | processo para fluoração de compostos |
TW201609652A (zh) | 2013-11-12 | 2016-03-16 | 陶氏農業科學公司 | 用於氟化化合物之過程(三) |
TW201609651A (zh) | 2013-11-12 | 2016-03-16 | 陶氏農業科學公司 | 用於氟化化合物之過程(一) |
TWI726900B (zh) | 2015-08-04 | 2021-05-11 | 美商陶氏農業科學公司 | 用於氟化化合物之過程 |
ES2837035T3 (es) * | 2016-07-07 | 2021-06-29 | Dow Agrosciences Llc | Procedimientos para la preparación de 4-alcoxi-3-(acil o alquil)oxipicolinamidas |
CN111655659B (zh) * | 2018-02-02 | 2023-03-28 | 关东电化工业株式会社 | 具有包含氢且包含氟和/或氯的丁二烯骨架的化合物的制造方法 |
BR112021005140A8 (pt) * | 2018-09-19 | 2021-06-29 | Corteva Agriscience Llc | preparação de análogos de halogênio de picloram |
BR112022018513A2 (pt) | 2020-03-18 | 2022-11-01 | Corteva Agriscience Llc | Síntese melhorada de 6-aril-4-aminopicolinatos |
BR112022018508A2 (pt) | 2020-03-18 | 2022-10-25 | Corteva Agriscience Llc | Síntese melhorada de 4-amino-6-(heterocíclico)picolinatos |
Family Cites Families (15)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US3285925A (en) * | 1962-03-06 | 1966-11-15 | Dow Chemical Co | Amino-trichloropicolinic acid compounds |
US3325272A (en) * | 1965-06-23 | 1967-06-13 | Dow Chemical Co | Plant growth control methods and compositions |
US3629424A (en) * | 1967-12-26 | 1971-12-21 | Dow Chemical Co | Cyanofluoropyridines and fungicidal compositions and methods for using the same |
US3803159A (en) | 1967-12-26 | 1974-04-09 | Dow Chemical Co | Fluorine containing cyanopyridines |
CN1042333C (zh) * | 1992-10-14 | 1999-03-03 | 美国氰胺公司 | 5,6-二取代-3-吡啶甲基卤化铵类化合物及其制备方法 |
FR2803592A1 (fr) * | 2000-01-06 | 2001-07-13 | Aventis Cropscience Sa | Nouveaux derives de l'acide 3-hydroxypicolinique, leur procede de preparation et compositions fongicides les contenant. |
AU760286B2 (en) * | 2000-01-14 | 2003-05-08 | Dow Agrosciences Llc | 4-aminopicolinates and their use as herbicides |
US6297197B1 (en) | 2000-01-14 | 2001-10-02 | Dow Agrosciences Llc | 4-aminopicolinates and their use as herbicides |
AR037228A1 (es) * | 2001-07-30 | 2004-11-03 | Dow Agrosciences Llc | Compuestos del acido 6-(aril o heteroaril)-4-aminopicolinico, composicion herbicida que los comprende y metodo para controlar vegetacion no deseada |
UA82358C2 (uk) | 2003-04-02 | 2008-04-10 | Дау Агросайенсиз Ллс | 6-алкіл або алкеніл-4-амінопіколінати гербіцидна композиція, спосіб боротьби з небажаною рослинністю |
WO2006062979A1 (en) * | 2004-12-06 | 2006-06-15 | E.I. Dupont De Nemours And Company | Herbicidal 6-cyclopropyl-substitute 4-aminopicolinic acid derivatives |
KR101350071B1 (ko) * | 2006-01-13 | 2014-01-14 | 다우 아그로사이언시즈 엘엘씨 | 6-(다-치환 아릴)-4-아미노피콜리네이트 및 그의제초제로서의 용도 |
DK2332914T3 (da) | 2007-10-02 | 2013-06-17 | Dow Agrosciences Llc | Substituerede 4-aminopicolinsyrer og deres anvendelse som herbicider |
US8252938B2 (en) * | 2009-06-08 | 2012-08-28 | Dow Agrosciences, Llc. | Process for the preparation of 6-(aryl)-4-aminopicolinates |
GB0910766D0 (en) * | 2009-06-22 | 2009-08-05 | Syngenta Ltd | Chemical compounds |
-
2012
- 2012-01-20 TW TW101102533A patent/TWI537252B/zh not_active IP Right Cessation
- 2012-01-24 SG SG2013056171A patent/SG192101A1/en unknown
- 2012-01-24 CN CN201280014129.7A patent/CN103458689B/zh not_active Expired - Fee Related
- 2012-01-24 KR KR1020147036124A patent/KR20150013334A/ko not_active Application Discontinuation
- 2012-01-24 PL PL12739149T patent/PL2667712T3/pl unknown
- 2012-01-24 KR KR1020137021997A patent/KR101537880B1/ko active IP Right Grant
- 2012-01-24 RU RU2013139379/04A patent/RU2542985C1/ru not_active IP Right Cessation
- 2012-01-24 US US13/356,686 patent/US8754231B2/en not_active Expired - Fee Related
- 2012-01-24 BR BR102012001643-5A patent/BR102012001643A2/pt not_active Application Discontinuation
- 2012-01-24 UA UAA201310368A patent/UA109806C2/ru unknown
- 2012-01-24 WO PCT/US2012/022289 patent/WO2012103045A1/en active Application Filing
- 2012-01-24 EP EP12739149.8A patent/EP2667712B1/en not_active Not-in-force
- 2012-01-24 CA CA2825468A patent/CA2825468C/en not_active Expired - Fee Related
- 2012-01-24 MX MX2013008602A patent/MX338962B/es active IP Right Grant
- 2012-01-24 BR BR112013018945A patent/BR112013018945A2/pt not_active Application Discontinuation
- 2012-01-24 JP JP2013551279A patent/JP5781171B2/ja not_active Expired - Fee Related
- 2012-01-24 AR ARP120100232A patent/AR085020A1/es unknown
- 2012-01-24 AU AU2012209281A patent/AU2012209281B2/en not_active Ceased
-
2013
- 2013-07-23 ZA ZA2013/05582A patent/ZA201305582B/en unknown
- 2013-07-24 IL IL227647A patent/IL227647B/en active IP Right Grant
- 2013-07-25 CO CO13175761A patent/CO6731129A2/es unknown
-
2014
- 2014-02-26 HK HK14101836.0A patent/HK1188684A1/zh not_active IP Right Cessation
- 2014-03-24 US US14/222,912 patent/US8993772B2/en not_active Expired - Fee Related
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