MX2018009453A - Proceso de hidrogenacion catalitico para preparar pirazoles. - Google Patents

Proceso de hidrogenacion catalitico para preparar pirazoles.

Info

Publication number
MX2018009453A
MX2018009453A MX2018009453A MX2018009453A MX2018009453A MX 2018009453 A MX2018009453 A MX 2018009453A MX 2018009453 A MX2018009453 A MX 2018009453A MX 2018009453 A MX2018009453 A MX 2018009453A MX 2018009453 A MX2018009453 A MX 2018009453A
Authority
MX
Mexico
Prior art keywords
catalytic hydrogenation
hydrogenation process
preparing pyrazoles
acids
pyrazoles
Prior art date
Application number
MX2018009453A
Other languages
English (en)
Inventor
Rack Michael
Gockel Birgit
George KLAUBER Eric
Soergel Sebastian
Goetz Roland
Original Assignee
Basf Se
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Basf Se filed Critical Basf Se
Publication of MX2018009453A publication Critical patent/MX2018009453A/es

Links

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D231/00—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings
    • C07D231/02—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings
    • C07D231/10—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members
    • C07D231/14—Heterocyclic compounds containing 1,2-diazole or hydrogenated 1,2-diazole rings not condensed with other rings having two or three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J21/00—Catalysts comprising the elements, oxides, or hydroxides of magnesium, boron, aluminium, carbon, silicon, titanium, zirconium, or hafnium
    • B01J21/18—Carbon
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/38—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals
    • B01J23/40—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of noble metals of the platinum group metals
    • B01J23/42—Platinum
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/16—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of hydrazones
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/72—Hydrazones
    • C07C251/74—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms
    • C07C251/76—Hydrazones having doubly-bound carbon atoms of hydrazone groups bound to hydrogen atoms or to acyclic carbon atoms to carbon atoms of a saturated carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D401/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom
    • C07D401/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings
    • C07D401/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, at least one ring being a six-membered ring with only one nitrogen atom containing two hetero rings linked by a chain containing hetero atoms as chain links
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D403/00—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00
    • C07D403/02—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings
    • C07D403/12—Heterocyclic compounds containing two or more hetero rings, having nitrogen atoms as the only ring hetero atoms, not provided for by group C07D401/00 containing two hetero rings linked by a chain containing hetero atoms as chain links

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Plural Heterocyclic Compounds (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Catalysts (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Agricultural Chemicals And Associated Chemicals (AREA)

Abstract

La presente invención se refiere a un proceso catalítico para preparar pirazoles que comprende la etapa de ciclar compuestos de carbonilo a,ß-insaturados sustituidos por hidrazona mediante su reacción con hidrógeno en una mezcla de reacción que comprende como componentes (a) un catalizador de hidrogenación, (b) un ácido seleccionado de ácidos de Brønsted, sales de amonio de ácidos de Brønsted y ácidos de Lewis, (c) un solvente prótico y opcionalmente (d) un solvente aprótico.
MX2018009453A 2016-02-02 2017-01-25 Proceso de hidrogenacion catalitico para preparar pirazoles. MX2018009453A (es)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
EP16153833 2016-02-02
PCT/EP2017/051524 WO2017133942A1 (en) 2016-02-02 2017-01-25 Catalytic hydrogenation process for preparing pyrazoles

Publications (1)

Publication Number Publication Date
MX2018009453A true MX2018009453A (es) 2018-09-21

Family

ID=55304873

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2018009453A MX2018009453A (es) 2016-02-02 2017-01-25 Proceso de hidrogenacion catalitico para preparar pirazoles.

Country Status (20)

Country Link
US (1) US10975036B2 (es)
EP (1) EP3411360B1 (es)
JP (1) JP6900400B2 (es)
KR (1) KR102651666B1 (es)
CN (1) CN108699003B (es)
AU (1) AU2017216082B2 (es)
BR (1) BR112018014357B8 (es)
CA (1) CA3010561C (es)
CL (1) CL2018002075A1 (es)
CO (1) CO2018008428A2 (es)
DK (1) DK3411360T3 (es)
ES (1) ES2795874T3 (es)
IL (1) IL260375B (es)
MX (1) MX2018009453A (es)
PE (1) PE20181539A1 (es)
PL (1) PL3411360T3 (es)
PT (1) PT3411360T (es)
RU (1) RU2733958C2 (es)
WO (1) WO2017133942A1 (es)
ZA (1) ZA201805742B (es)

Families Citing this family (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
MX2017001462A (es) 2014-07-31 2017-05-23 Basf Se Proceso para la preparacion de pirazoles.
KR20180003570A (ko) 2015-05-08 2018-01-09 바스프 아그로 비.브이. 테르피놀렌 에폭시드의 제조 방법
DK3294700T3 (da) 2015-05-08 2020-04-14 Basf Agro Bv Fremgangsmåde til fremstilling af limonen-4-ol
PE20180327A1 (es) 2015-05-11 2018-02-13 Basf Se Proceso para preparar 4-amino-piridazinas
AU2017286055B2 (en) 2016-06-15 2021-07-01 BASF Agro B.V. Process for the epoxidation of a tetrasubstituted alkene
AU2017284971B2 (en) 2016-06-15 2021-01-21 BASF Agro B.V. Process for the epoxidation of a tetrasubstituted alkene
EP3481795A1 (en) 2016-07-07 2019-05-15 Basf Se Oxy-cope rearrangement for the manufacture of insecticidal cyclopentene compounds
CN109843875A (zh) 2016-11-04 2019-06-04 巴斯夫欧洲公司 纯化吡唑哒嗪类的方法
EP3541788B1 (en) 2016-11-17 2020-09-02 Basf Se Process for the purification of 1-(4-chlorophenyl)pyrazol-3-ol
US10961213B2 (en) 2017-01-25 2021-03-30 Basf Se Process for preparation of benzylic amides
CN110431126B (zh) 2017-03-20 2022-12-02 巴斯夫欧洲公司 制备一溴三氯甲烷的方法
WO2019086545A1 (en) 2017-11-02 2019-05-09 Basf Se Process for preparing 4-chlorobenzyl propargyl ether

Family Cites Families (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP2007326784A (ja) * 2006-06-06 2007-12-20 Sagami Chem Res Center １−置換−５−フルオロアルキルピラゾール−４−カルボン酸エステルの製造方法
US8143293B2 (en) * 2007-04-20 2012-03-27 Deciphera Pharmaceuticals, Llc Kinase inhibitors useful for the treatment of myleoprolific diseases and other proliferative diseases
US20110189167A1 (en) 2007-04-20 2011-08-04 Flynn Daniel L Methods and Compositions for the Treatment of Myeloproliferative Diseases and other Proliferative Diseases
EP2197280B1 (en) 2007-08-27 2013-06-19 Basf Se Pyrazole compounds for controlling invertebrate pests
WO2009068652A1 (en) * 2007-11-30 2009-06-04 Smithkline Beecham Corporation 2, 6-disubstituted pyridines and 2, 4-disubstituted pyrimidines as soluble guanylate cyclase activators
CN102015654B (zh) * 2008-05-05 2014-03-12 巴斯夫欧洲公司 制备1，3，4-取代的吡唑化合物的方法
JP2012503623A (ja) 2008-09-24 2012-02-09 ビーエーエスエフ ソシエタス・ヨーロピア 無脊椎動物系害虫防除用ピラゾール化合物
JP5536073B2 (ja) * 2008-09-24 2014-07-02 ビーエーエスエフ ソシエタス・ヨーロピア 無脊椎動物系害虫を防除するためのピラゾール化合物
EP2236505A1 (de) 2009-04-03 2010-10-06 Bayer CropScience AG Acylierte Aminopyridine und - pyridazine als Insektizide
AR076984A1 (es) 2009-06-08 2011-07-20 Merck Serono Sa Derivados de pirazol oxadiazol
CN107334529B (zh) 2011-04-12 2020-06-09 热医学公司 用于对流体增强型消融装置使用除气流体的方法和装置
BR112013024708B1 (pt) * 2011-04-21 2018-10-09 Basf Se compostos de pirazol,composições, métodos para combater ou controlar pragas invertebradas e para proteger plantas em crescimento, processo para proteger sementes e uso dos compostos
JO3407B1 (ar) * 2012-05-31 2019-10-20 Eisai R&D Man Co Ltd مركبات رباعي هيدرو بيرازولو بيريميدين
EP2671873A1 (en) * 2012-06-06 2013-12-11 Solvay Sa Method for the cyclization of hydrazinoacrylic acid derivatives
ES2660132T3 (es) * 2012-06-20 2018-03-20 Basf Se Compuestos de pirazol plaguicidas
WO2014089364A1 (en) 2012-12-06 2014-06-12 Quanticel Pharmaceuticals, Inc Histone demethylase inhibitors
MX2017001462A (es) 2014-07-31 2017-05-23 Basf Se Proceso para la preparacion de pirazoles.
PE20180327A1 (es) 2015-05-11 2018-02-13 Basf Se Proceso para preparar 4-amino-piridazinas

Also Published As

Publication number Publication date
AU2017216082B2 (en) 2020-12-03
CA3010561C (en) 2024-04-16
EP3411360B1 (en) 2020-03-11
EP3411360A1 (en) 2018-12-12
RU2733958C2 (ru) 2020-10-08
DK3411360T3 (da) 2020-06-08
CA3010561A1 (en) 2017-08-10
JP6900400B2 (ja) 2021-07-07
ES2795874T3 (es) 2020-11-25
RU2018130339A3 (es) 2020-03-19
IL260375B (en) 2021-03-25
RU2018130339A (ru) 2020-03-04
KR20180104743A (ko) 2018-09-21
PT3411360T (pt) 2020-06-01
CN108699003A (zh) 2018-10-23
CN108699003B (zh) 2023-02-03
US10975036B2 (en) 2021-04-13
AU2017216082A1 (en) 2018-07-26
CO2018008428A2 (es) 2018-08-21
CL2018002075A1 (es) 2018-09-14
WO2017133942A1 (en) 2017-08-10
BR112018014357B8 (pt) 2022-09-06
PL3411360T3 (pl) 2020-08-24
ZA201805742B (en) 2019-11-27
JP2019504883A (ja) 2019-02-21
BR112018014357A2 (pt) 2018-12-18
US20190055200A1 (en) 2019-02-21
BR112018014357B1 (pt) 2022-08-16
KR102651666B1 (ko) 2024-03-26
PE20181539A1 (es) 2018-09-26

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