MX2014008732A - Proceso para preparar hidróxido de colina a partir de trimetilamina y óxido de etileno. - Google Patents

Proceso para preparar hidróxido de colina a partir de trimetilamina y óxido de etileno.

Info

Publication number
MX2014008732A
MX2014008732A MX2014008732A MX2014008732A MX2014008732A MX 2014008732 A MX2014008732 A MX 2014008732A MX 2014008732 A MX2014008732 A MX 2014008732A MX 2014008732 A MX2014008732 A MX 2014008732A MX 2014008732 A MX2014008732 A MX 2014008732A
Authority
MX
Mexico
Prior art keywords
reactor
trimethylamine
choline hydroxide
product
ethylene oxide
Prior art date
Application number
MX2014008732A
Other languages
English (en)
Other versions
MX357544B (es
Inventor
Ruokang Li
Ravindra S Dixit
Avani M Patel
Xiaoyun Chen
Randy J Pell
John G Pendergast
Original Assignee
Dow Agrosciences Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Agrosciences Llc filed Critical Dow Agrosciences Llc
Publication of MX2014008732A publication Critical patent/MX2014008732A/es
Publication of MX357544B publication Critical patent/MX357544B/es

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/04—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reaction of ammonia or amines with olefin oxides or halohydrins
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/12—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/10—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic with one amino group and at least two hydroxy groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/02—Formation of carboxyl groups in compounds containing amino groups, e.g. by oxidation of amino alcohols
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)

Abstract

Se describen procesos para preparar hidróxido de N, N,N-trimetiletanolamonio (hidróxido de colina) y el hidróxido de colina producido. Estos procesos minimizan la producción del subproducto colina monoetoxilada y dietoxilada en el producto hidróxido de colina. Los procesos generalmente incluyen alimentar óxido de etileno, trimetilamina y agua en un primer reactor para crear un primer producto bajo condiciones controladas de temperatura. El producto del primer reactor se alimenta en un segundo reactor para formar un segundo producto de reactor bajo condiciones no controladas, adiabáticas. Finalmente, toda trimetilamina no reaccionada en el segundo producto de reactor se retira para formar un producto final que comprende hidróxido de colina. Es posible utilizar reactores adicionales para la reacción de óxido de etileno y trimetilamina.
MX2014008732A 2012-01-19 2013-01-17 Proceso para preparar hidróxido de colina a partir de trimetilamina y óxido de etileno. MX357544B (es)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201261588234P 2012-01-19 2012-01-19
US201261720711P 2012-10-31 2012-10-31
PCT/US2013/021864 WO2013109705A1 (en) 2012-01-19 2013-01-17 Process for preparing choline hydroxide from trimethylamine and ethylene oxide

Publications (2)

Publication Number Publication Date
MX2014008732A true MX2014008732A (es) 2015-02-04
MX357544B MX357544B (es) 2018-07-13

Family

ID=48797749

Family Applications (1)

Application Number Title Priority Date Filing Date
MX2014008732A MX357544B (es) 2012-01-19 2013-01-17 Proceso para preparar hidróxido de colina a partir de trimetilamina y óxido de etileno.

Country Status (18)

Country Link
US (1) US9353045B2 (es)
EP (1) EP2804477B1 (es)
JP (1) JP6109853B2 (es)
KR (2) KR20200032242A (es)
CN (2) CN106928072A (es)
AR (1) AR089756A1 (es)
AU (2) AU2013209783B2 (es)
BR (1) BR112014017781B1 (es)
CA (1) CA2863057C (es)
CO (1) CO7010820A2 (es)
DK (1) DK2804477T3 (es)
IL (1) IL233601B (es)
IN (1) IN2014DN05702A (es)
MX (1) MX357544B (es)
NZ (1) NZ627045A (es)
PL (1) PL2804477T3 (es)
RU (1) RU2641815C2 (es)
WO (1) WO2013109705A1 (es)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
AU2014253067C1 (en) * 2013-04-11 2018-10-04 Taminco Improved process for preparing choline hydroxide
CN113214093B (zh) * 2021-05-21 2022-11-29 济南亚西亚药业有限公司 酒石酸氢胆碱废母液中回收氯化胆碱和酒石酸盐的方法
WO2023102167A1 (en) * 2021-12-03 2023-06-08 Huntsman Petrochemical Llc Production of anhydrous quaternary ammonium hydroxides

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2774759A (en) * 1955-01-06 1956-12-18 American Cyanamid Co Preparation of choline base and choline salts
DE2115094B2 (de) * 1971-03-29 1981-07-23 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung einer wäßrigen Cholinchloridlösung
DD241594A1 (de) * 1985-10-04 1986-12-17 Chemisch Pharmazeutisches Werk Verfahren und vorrichtung zur herstellung von cholin und cholinsalzen
DD241596A1 (de) * 1985-10-04 1986-12-17 Chemisch Pharmazeutisches Werk Verfahren und vorrichtung zur herstellung von cholin
CN1078231A (zh) * 1992-05-02 1993-11-10 中国石油化工总公司上海石油化工总厂 氯化胆碱的制造方法
JP3478893B2 (ja) * 1995-02-10 2003-12-15 日本ヒドラジン工業株式会社 高純度コリンの製造方法
US5895823A (en) * 1998-01-30 1999-04-20 Air Products And Chemicals, Inc. Process for the preparation of aqueous solutions of betaine
JP4184672B2 (ja) * 2001-02-19 2008-11-19 日本乳化剤株式会社 第４級アンモニウム水酸化物含有組成物及びその製造法
CN1502602A (zh) * 2002-11-22 2004-06-09 张国强 采用列管式反应和薄膜蒸发浓缩连续生产胆碱的方法
WO2006005692A1 (en) * 2004-07-09 2006-01-19 Akzo Nobel N.V. Composition comprising choline hydroxide and process for preparing the same

Also Published As

Publication number Publication date
CO7010820A2 (es) 2014-07-31
AU2013209783A1 (en) 2014-07-24
EP2804477B1 (en) 2018-06-27
RU2014133861A (ru) 2016-03-20
EP2804477A1 (en) 2014-11-26
IN2014DN05702A (es) 2015-04-10
CA2863057C (en) 2020-03-31
CN104039143B (zh) 2017-07-04
AR089756A1 (es) 2014-09-17
WO2013109705A1 (en) 2013-07-25
DK2804477T3 (en) 2018-10-01
JP6109853B2 (ja) 2017-04-05
BR112014017781B1 (pt) 2019-12-03
CN104039143A (zh) 2014-09-10
JP2015504090A (ja) 2015-02-05
PL2804477T3 (pl) 2018-12-31
NZ627045A (en) 2015-06-26
US9353045B2 (en) 2016-05-31
KR20140114867A (ko) 2014-09-29
CA2863057A1 (en) 2013-07-25
RU2641815C2 (ru) 2018-01-22
BR112014017781A2 (es) 2017-06-20
AU2013209783B2 (en) 2016-11-17
IL233601B (en) 2020-08-31
MX357544B (es) 2018-07-13
AU2017200997A1 (en) 2017-03-09
CN106928072A (zh) 2017-07-07
IL233601A0 (en) 2014-08-31
KR102091495B1 (ko) 2020-03-20
KR20200032242A (ko) 2020-03-25
EP2804477A4 (en) 2015-09-23
BR112014017781A8 (pt) 2017-07-11
US20130190534A1 (en) 2013-07-25

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