BR112014017781A8 - Processo para preparação de hidróxido de colina a partir de trimetilamina e óxido de etileno - Google Patents

Processo para preparação de hidróxido de colina a partir de trimetilamina e óxido de etileno

Info

Publication number
BR112014017781A8
BR112014017781A8 BR112014017781A BR112014017781A BR112014017781A8 BR 112014017781 A8 BR112014017781 A8 BR 112014017781A8 BR 112014017781 A BR112014017781 A BR 112014017781A BR 112014017781 A BR112014017781 A BR 112014017781A BR 112014017781 A8 BR112014017781 A8 BR 112014017781A8
Authority
BR
Brazil
Prior art keywords
trimethylamine
reactor
product
choline hydroxide
ethylene oxide
Prior art date
Application number
BR112014017781A
Other languages
English (en)
Other versions
BR112014017781A2 (pt
BR112014017781B1 (pt
Inventor
Li Ruokang
S Dixit Ravindra
M Patel Avani
Chen Xiaoyun
J Pell Randy
G Pendergast John
Original Assignee
Dow Agrosciences Llc
Corteva Agriscience Llc
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Dow Agrosciences Llc, Corteva Agriscience Llc filed Critical Dow Agrosciences Llc
Publication of BR112014017781A2 publication Critical patent/BR112014017781A2/pt
Publication of BR112014017781A8 publication Critical patent/BR112014017781A8/pt
Publication of BR112014017781B1 publication Critical patent/BR112014017781B1/pt

Links

Classifications

    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • A—HUMAN NECESSITIES
    • A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
    • A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
    • A01N33/00—Biocides, pest repellants or attractants, or plant growth regulators containing organic nitrogen compounds
    • A01N33/02—Amines; Quaternary ammonium compounds
    • A01N33/12—Quaternary ammonium compounds
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C213/00—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton
    • C07C213/04—Preparation of compounds containing amino and hydroxy, amino and etherified hydroxy or amino and esterified hydroxy groups bound to the same carbon skeleton by reaction of ammonia or amines with olefin oxides or halohydrins
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C215/00—Compounds containing amino and hydroxy groups bound to the same carbon skeleton
    • C07C215/02—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton
    • C07C215/04—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated
    • C07C215/06—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic
    • C07C215/10—Compounds containing amino and hydroxy groups bound to the same carbon skeleton having hydroxy groups and amino groups bound to acyclic carbon atoms of the same carbon skeleton the carbon skeleton being saturated and acyclic with one amino group and at least two hydroxy groups bound to the carbon skeleton
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C227/00—Preparation of compounds containing amino and carboxyl groups bound to the same carbon skeleton
    • C07C227/02—Formation of carboxyl groups in compounds containing amino groups, e.g. by oxidation of amino alcohols
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Agronomy & Crop Science (AREA)
  • Pest Control & Pesticides (AREA)
  • Plant Pathology (AREA)
  • Health & Medical Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Dentistry (AREA)
  • General Health & Medical Sciences (AREA)
  • Wood Science & Technology (AREA)
  • Zoology (AREA)
  • Environmental Sciences (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
  • Epoxy Compounds (AREA)

Abstract

PROCESSO PARA PREPARAÇÃO DE HIDRÓXIDO DE COLINA A PARTIR DE TRIMETILAMINA E ÓXIDO DE ETILENO. A presente invenção refere-se a processos para preparação de N,N,N-hidróxido de trimetiletanolamônia (hidróxido de colina) e o hidróxido de colina produzido são descritos. Estes processos minimizam a produção de subproduto de colina monoetoxilatada e dietoxilatada no produto de hidróxido de colina. Os processos geralmente incluem alimentar óxido de etileno, trimetilamina, e água, em um primeiro reator, para criar um primeiro produto de reator sob condições de temperatura controlada. O produto do primeiro reator é alimentado em um segundo reator, para formar um segundo produto de reator sob condições adiabáticas não controladas. Finalmente, qualquer trimetilamina não reagida no segundo produto de reator é removida para formar um produto final compreendendo hidróxido de colina. Reatores adicionais podem ser usados para a reação de óxido de etileno e trimetilamina.
BR112014017781A 2012-01-19 2013-01-17 processo para preparação de hidróxido de colina a partir de trimetilamina e óxido de etileno BR112014017781B1 (pt)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201261588234P 2012-01-19 2012-01-19
US201261720711P 2012-10-31 2012-10-31
PCT/US2013/021864 WO2013109705A1 (en) 2012-01-19 2013-01-17 Process for preparing choline hydroxide from trimethylamine and ethylene oxide

Publications (3)

Publication Number Publication Date
BR112014017781A2 BR112014017781A2 (pt) 2017-06-20
BR112014017781A8 true BR112014017781A8 (pt) 2017-07-11
BR112014017781B1 BR112014017781B1 (pt) 2019-12-03

Family

ID=48797749

Family Applications (1)

Application Number Title Priority Date Filing Date
BR112014017781A BR112014017781B1 (pt) 2012-01-19 2013-01-17 processo para preparação de hidróxido de colina a partir de trimetilamina e óxido de etileno

Country Status (18)

Country Link
US (1) US9353045B2 (pt)
EP (1) EP2804477B1 (pt)
JP (1) JP6109853B2 (pt)
KR (2) KR20200032242A (pt)
CN (2) CN106928072A (pt)
AR (1) AR089756A1 (pt)
AU (2) AU2013209783B2 (pt)
BR (1) BR112014017781B1 (pt)
CA (1) CA2863057C (pt)
CO (1) CO7010820A2 (pt)
DK (1) DK2804477T3 (pt)
IL (1) IL233601B (pt)
IN (1) IN2014DN05702A (pt)
MX (1) MX357544B (pt)
NZ (1) NZ627045A (pt)
PL (1) PL2804477T3 (pt)
RU (1) RU2641815C2 (pt)
WO (1) WO2013109705A1 (pt)

Families Citing this family (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
RU2678972C2 (ru) * 2013-04-11 2019-02-05 Таминко Усовершенствованный способ получения холингидроксида
CN113214093B (zh) * 2021-05-21 2022-11-29 济南亚西亚药业有限公司 酒石酸氢胆碱废母液中回收氯化胆碱和酒石酸盐的方法
WO2023102167A1 (en) * 2021-12-03 2023-06-08 Huntsman Petrochemical Llc Production of anhydrous quaternary ammonium hydroxides

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2774759A (en) * 1955-01-06 1956-12-18 American Cyanamid Co Preparation of choline base and choline salts
DE2115094B2 (de) * 1971-03-29 1981-07-23 Basf Ag, 6700 Ludwigshafen Verfahren zur kontinuierlichen Herstellung einer wäßrigen Cholinchloridlösung
DD241594A1 (de) * 1985-10-04 1986-12-17 Chemisch Pharmazeutisches Werk Verfahren und vorrichtung zur herstellung von cholin und cholinsalzen
DD241596A1 (de) * 1985-10-04 1986-12-17 Chemisch Pharmazeutisches Werk Verfahren und vorrichtung zur herstellung von cholin
CN1078231A (zh) * 1992-05-02 1993-11-10 中国石油化工总公司上海石油化工总厂 氯化胆碱的制造方法
JP3478893B2 (ja) * 1995-02-10 2003-12-15 日本ヒドラジン工業株式会社 高純度コリンの製造方法
US5895823A (en) * 1998-01-30 1999-04-20 Air Products And Chemicals, Inc. Process for the preparation of aqueous solutions of betaine
JP4184672B2 (ja) * 2001-02-19 2008-11-19 日本乳化剤株式会社 第４級アンモニウム水酸化物含有組成物及びその製造法
CN1502602A (zh) * 2002-11-22 2004-06-09 张国强 采用列管式反应和薄膜蒸发浓缩连续生产胆碱的方法
EP1781594A1 (en) 2004-07-09 2007-05-09 Akzo Nobel N.V. Composition comprising choline hydroxide and process for preparing the same

Also Published As

Publication number Publication date
CA2863057C (en) 2020-03-31
MX357544B (es) 2018-07-13
EP2804477A1 (en) 2014-11-26
AU2013209783B2 (en) 2016-11-17
KR20140114867A (ko) 2014-09-29
CO7010820A2 (es) 2014-07-31
RU2014133861A (ru) 2016-03-20
IN2014DN05702A (pt) 2015-04-10
US9353045B2 (en) 2016-05-31
BR112014017781A2 (pt) 2017-06-20
AU2013209783A1 (en) 2014-07-24
JP6109853B2 (ja) 2017-04-05
WO2013109705A1 (en) 2013-07-25
IL233601B (en) 2020-08-31
CN104039143B (zh) 2017-07-04
KR102091495B1 (ko) 2020-03-20
AU2017200997A1 (en) 2017-03-09
NZ627045A (en) 2015-06-26
BR112014017781B1 (pt) 2019-12-03
IL233601A0 (en) 2014-08-31
CA2863057A1 (en) 2013-07-25
DK2804477T3 (en) 2018-10-01
CN106928072A (zh) 2017-07-07
MX2014008732A (es) 2015-02-04
US20130190534A1 (en) 2013-07-25
EP2804477B1 (en) 2018-06-27
PL2804477T3 (pl) 2018-12-31
RU2641815C2 (ru) 2018-01-22
KR20200032242A (ko) 2020-03-25
AR089756A1 (es) 2014-09-17
CN104039143A (zh) 2014-09-10
EP2804477A4 (en) 2015-09-23
JP2015504090A (ja) 2015-02-05

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Legal Events

Date Code Title Description
B06T Formal requirements before examination [chapter 6.20 patent gazette]
B06F Objections, documents and/or translations needed after an examination request according [chapter 6.6 patent gazette]
B07A Application suspended after technical examination (opinion) [chapter 7.1 patent gazette]
B15K Others concerning applications: alteration of classification

Free format text: A CLASSIFICACAO ANTERIOR ERA: A01N 33/12

Ipc: C07C 213/04 (1990.01)

B09A Decision: intention to grant [chapter 9.1 patent gazette]
B16A Patent or certificate of addition of invention granted [chapter 16.1 patent gazette]

Free format text: PRAZO DE VALIDADE: 20 (VINTE) ANOS CONTADOS A PARTIR DE 17/01/2013, OBSERVADAS AS CONDICOES LEGAIS. (CO) 20 (VINTE) ANOS CONTADOS A PARTIR DE 17/01/2013, OBSERVADAS AS CONDICOES LEGAIS

B25D Requested change of name of applicant approved

Owner name: CORTEVA AGRISCIENCE LLC (US)