KR960000961A - 폴리에테르아민과 α, β-불포화 디카복실산의 중합체와의 반응 생성물 - Google Patents

폴리에테르아민과 α, β-불포화 디카복실산의 중합체와의 반응 생성물 Download PDF

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KR960000961A
KR960000961A KR1019950017001A KR19950017001A KR960000961A KR 960000961 A KR960000961 A KR 960000961A KR 1019950017001 A KR1019950017001 A KR 1019950017001A KR 19950017001 A KR19950017001 A KR 19950017001A KR 960000961 A KR960000961 A KR 960000961A
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크룰 마티아스
포이슈텔 미카엘
밀케 에르트만
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아울미히, 귀틀라인
훽스트 아크티엔게젤샤프트
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Abstract

본 발명은 20 내지 80mol%, 바람직하게는 40 내지 60mol%의 2가 구조 단위 (A) 및/또는 (C)및, 경우에 따라, (B)및 80 내지 20mol%, 바람직하게는 60 내지 40mol%의 2가 구조 단위(D)를 포함하는 디하이드록실산 무수술을 포함하는 중합체와 폴리에테르아민과의 반응 생성물에 관한 것이다.
상기식에서, R1및 R2는 서로 독립적으로 수소 또는 메틸이고, a및 b는 0 또는 1이고 a+b는 1이고, Y는 X 또는 NRR3이고, X는 -OH, -0-C1-30-알킬, NR3R4또는이고, R3및 R4는 서로 독립적으로 수소, C6-C40-알킬 또는 R이고, R은이고, Z는 C2-C4-알킬이고, n은 1내지 1000의 수이고, R5는 수소, C1-C30-알킬, C5-C12-사이클로알킬 또는 C6-C30-아릴이고, R6은 수소 또는 C1-C4-알킬, 바람직하게는 메틸이고, R7은 수소 또는 C1-C4-알킬이고, R8은 C1-C60-알킬 또는 C6-C18-아릴이고, 단, 중합체에 결합된 무수물 그룹의 1mol% 이상은 폴리에테르아민과 반응한다.

Description

폴리에테르아민과 α,β-불포화 디카복실산의 중합체와의 반응 생성물
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (14)

  1. 20 내지 80mol%, 바람직하게는 40 내지 60mol%의 2가 구조 단위 (A) 및/또는 (C)및, 경우에 따라, (B)및 80 내지 20mol%, 바람직하게는 60 내지 40mol%의 2가 구조 단위(D)를 포함하는 디카복실산 무수술그룹을 포함하는 중합체와 폴리에테르아민과의 반응 생성물.
    상기식에서, R1및 R2는 서로 독립적으로 수소 또는 메틸이고, a및 b는 0 또는 1이고 a+b는 1이고, Y는 X 또는 NRR3이고, X는 -OH, -0-C1-30-알킬, NR3R4또는이고, R3및 R4는 서로 독립적으로 수소, C6-C40-알킬 또는 R이고, R은이고, Z는 C2-C4-알킬이고, n은 1내지 1000의 수이고, R5는 수소, C1-C30-알킬, C5-C12-사이클로알킬 또는 C6-C30-아릴이고, R6은 수소 또는 C1-C4-알킬, 바람직하게는 메틸이고, R7은 수소 또는 C1-C4-알킬이고, R8은 C1-C60-알킬 또는 C6-C18-아릴이고, 단, 중합체에 결합된 무수물 그룹의 1mol% 이상은 폴리에테르아민과 반응한다.
  2. 일반식(E) 및/또는 (F)의 단량체 및 일반식(G)의 단량체를 서로 중합시킨 다음, 생성물을 일반식(H)의 폴리에테르아민 및/또는 일반식(I)의 알칼올아민과 반응시킴을 포함하여, 제1항에 따르는 반응 생성물을 제조하는 방법.
    상기식에서, R1및 R2는 서로 독립적으로 수소 또는 메틸이고, R7은 수소 또는 C1-C4-알킬이고, R8은 수소 또는 C1-C60-알킬 또는 C6-C18-아릴이고, R3은 수소, C6-C40-알킬 또는 R이고, R은 일반식 의 그룹이고, Z는 C2-C4알킬이고, n은 1 내지 1000의 수이고, R5는 수소, C1-C30-알킬, C5-C12-사이클로알킬 또는 C8-C30-아릴이고, R6은 수소 또는 C1-C4-알킬이고, R9및 R10은 서로 독립적으로 수소, C2-C22-알켄일, C1-C22-알킬 또는 Z-OH이고, 단, 라디칼 R9또는 R10중의 하나 이상은 Z-OH이고, 중합체에 결합된 무수물 그룹의 1mol% 이상은 폴리에테르아민과 반응한다.
  3. 제2항에 있어서, 일반식(H)의 폴리에테르아민 및/또는 일반식(I)의 알칼올아민과 중합체와의 반응이 50 내지 250℃의 온도에서 수행되는 방법.
  4. 제2항에 있어서, 중합이, 일반식 (E), (F), (G), (H)및/또는 (I)의 단량체 및 제1항에 따르는 반응생성물이 가용성인 용매 중에서 수행되는 방법.
  5. 제1항에 따르는 반응 생성물 하나 이상과 에틸렌/비닐 에스테르 공중합체 하나 이상을 포함하는 혼합물.
  6. 제5항에 있어서, 단량체로서 C1-C20-알킬 비닐 에스테르, 포화된 C10-C24-지방산의 비닐 에스테르, 불포화 카복실산의 에스테르, 디이소부틸렌, 디메틸비닐카비놀 및 비닐 메톡시아세테이트를 포함하는 공중합체로부터 유도된 에틸렌/비닐 에스테르 공중합체를 포함하는 혼합물.
  7. 제5항 또는 제6항에 있어서, 에틸린/비닐 에스테르 공중합체가 에틸렌 80 내지 51중량% 및 비닐 아세테이트 또는 비닐 프로피오네이트 20 내지 49중량%를 포함하는 혼합물.
  8. 제5항 또는 제7항중 어느 한 항에 있어서, 에틸렌/비닐 에스테르 공중합체가 에틸렌 79 내지 40중량%, 비닐아세테이트 또는 비닐 프로피오네이트 20 내지 35중량%, 바람직하게는 1 내지 15중량% 및 디이소부틸렌, 비닐 네오노나노에이트 도는 비닐 네오데카노에이트 1 내지 25중량%, 바람직하게는 1 내지 15중량%를 포함하는 혼합물.
  9. 제5항 내지 제8항 중의 어느 한 항에 따르는 혼합물과 하기 일반식의 4급 암모늄 염 하나 이상을 포함하는 혼합물.
    상기식에서, R11은 C1-C30-알킬, 바람직하게는 C1-C22-알킬, C2-C30-알켄일, 바람직하게는 C2-C22-알켄일, 벤질 또는 일반식 -(CH2CH2-O)n-R12의 라디칼이고, 여기서, R12는 수소 또는 일반식 C(O)-R13의 지방산 라디칼(여기서, R13은 C6-C40-알킬 도는 C6-C40-알켄일이다)이고, n은 1 내지 30의 수이고, X는 할로겐, 바람직하게는 염소, 또는 메토설페이트이다.
  10. 제5항 내지 제9항 중의 어느 한 항에 따르는 혼합물의 광유 중간 증류물에서의 파라핀 분산제로서의 용도.
  11. 제5항 내지 제9항 중의 어느 한 항에 따르는 혼합물의 광유 중간 증류물에서 운점을 감소시키기 위하 용도.
  12. 제10항 또는 제11항에 있어서, 10 내지 1000ppm, 바람직하게는 50 내지 500ppm의 반응 생성물 및 100 내지 10,000ppm, 바람직하게는 50 내지 1000ppm의 에틸렌/비닐 에스테르 공중합체를 포함하는 혼합물이 파라핀 함유 광유 중간 증류물에 가해지는 용도.
  13. 제5항 내지 제9항 중의 어느 한 항에 따르는 혼합물을 포함하는 파라핀 함유 광유 중간 증류물.
  14. 제10항 또는 제11항에 있어서, 10 내지 1000ppm, 바람직하게는 50 내지 500ppm의 제1항에 따르는 반응 생성물, 10 내지 10,000ppm, 바람직하게는 50 내지 1000ppm의 에틸렌/비닐 에스테르 공중합체 및 10 내지 1000ppm, 바람직하게는 50 내지 500ppm의 일반식의 4급 암모늄 염을 포함하는 혼합물이 파라핀 함유 광유 중간 증류물에 가해지는 용도.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019950017001A 1994-06-24 1995-06-23 폴리에테르아민과 α, β-불포화 디카복실산의 중합체와의 반응 생성물 KR960000961A (ko)

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DE4422159A DE4422159A1 (de) 1994-06-24 1994-06-24 Umsetzungsprodukte von Polyetheraminen mit Polymeren alpha,beta-ungesättigter Dicarbonsäuren

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FI953135A (fi) 1995-12-25
DE59503500D1 (de) 1998-10-15
NO952539L (no) 1995-12-27
NO952539D0 (no) 1995-06-23
ATE170879T1 (de) 1998-09-15
EP0688796B1 (de) 1998-09-09
DE4422159A1 (de) 1996-01-04
US5705603A (en) 1998-01-06
JPH0881563A (ja) 1996-03-26
FI953135A0 (fi) 1995-06-22
EP0688796A1 (de) 1995-12-27

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