KR950032358A - 친수성 폴리우레탄-폴리우레아 및 합성 수지용 분산제로서의 이의 용도 - Google Patents

친수성 폴리우레탄-폴리우레아 및 합성 수지용 분산제로서의 이의 용도 Download PDF

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KR950032358A
KR950032358A KR1019950011105A KR19950011105A KR950032358A KR 950032358 A KR950032358 A KR 950032358A KR 1019950011105 A KR1019950011105 A KR 1019950011105A KR 19950011105 A KR19950011105 A KR 19950011105A KR 950032358 A KR950032358 A KR 950032358A
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polyurea
hydrophilic polyurethane
mol
isocyanate
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메르텐 게르하르트
조엘러 요아힘
우르바노 에드문트
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카를-헤르만 마이어-돌호이어, 베른하르트 엠. 백크
훽스트 아크티엔게젤샤프트
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Publication of KR950032358A publication Critical patent/KR950032358A/ko

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    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
    • C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
    • C08G18/6666—Compounds of group C08G18/48 or C08G18/52
    • C08G18/6692—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/34
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/0804—Manufacture of polymers containing ionic or ionogenic groups
    • C08G18/0819—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups
    • C08G18/0823—Manufacture of polymers containing ionic or ionogenic groups containing anionic or anionogenic groups containing carboxylate salt groups or groups forming them
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/08—Processes
    • C08G18/10—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step
    • C08G18/12—Prepolymer processes involving reaction of isocyanates or isothiocyanates with compounds having active hydrogen in a first reaction step using two or more compounds having active hydrogen in the first polymerisation step
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/2815—Monohydroxy compounds
    • C08G18/282—Alkanols, cycloalkanols or arylalkanols including terpenealcohols
    • C08G18/2825—Alkanols, cycloalkanols or arylalkanols including terpenealcohols having at least 6 carbon atoms
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/2805—Compounds having only one group containing active hydrogen
    • C08G18/285—Nitrogen containing compounds
    • C08G18/2865—Compounds having only one primary or secondary amino group; Ammonia
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3225—Polyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/32—Polyhydroxy compounds; Polyamines; Hydroxyamines
    • C08G18/3271—Hydroxyamines
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3819—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
    • C08G18/3821—Carboxylic acids; Esters thereof with monohydroxyl compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/30—Low-molecular-weight compounds
    • C08G18/38—Low-molecular-weight compounds having heteroatoms other than oxygen
    • C08G18/3819—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen
    • C08G18/3823—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing -N-C=O groups
    • C08G18/3834—Low-molecular-weight compounds having heteroatoms other than oxygen having nitrogen containing -N-C=O groups containing hydrazide or semi-carbazide groups
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G18/00—Polymeric products of isocyanates or isothiocyanates
    • C08G18/06—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen
    • C08G18/28—Polymeric products of isocyanates or isothiocyanates with compounds having active hydrogen characterised by the compounds used containing active hydrogen
    • C08G18/65—Low-molecular-weight compounds having active hydrogen with high-molecular-weight compounds having active hydrogen
    • C08G18/66—Compounds of groups C08G18/42, C08G18/48, or C08G18/52
    • C08G18/6666—Compounds of group C08G18/48 or C08G18/52
    • C08G18/6696—Compounds of group C08G18/48 or C08G18/52 with compounds of group C08G18/36 or hydroxylated esters of higher fatty acids of C08G18/38
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08J—WORKING-UP; GENERAL PROCESSES OF COMPOUNDING; AFTER-TREATMENT NOT COVERED BY SUBCLASSES C08B, C08C, C08F, C08G or C08H
    • C08J3/00—Processes of treating or compounding macromolecular substances
    • C08J3/02—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques
    • C08J3/03—Making solutions, dispersions, lattices or gels by other methods than by solution, emulsion or suspension polymerisation techniques in aqueous media

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Dispersion Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Manufacturing & Machinery (AREA)
  • Polyurethanes Or Polyureas (AREA)
  • Emulsifying, Dispersing, Foam-Producing Or Wetting Agents (AREA)

Abstract

본 발명은 (A) 하나 이상의 유기 폴리이소아네이트를 포함하는 폴리이소시네이트 성분, (B) 하나 이상의 이소시아네이트-반응성 지방산 유도체. (C)필요에 따라, 하이드록실 및 카복실 그롭에서 선택된 두개 이상의 작용성 그룹을 함유하는 화합물, (D) 500 내지 10,000g/mol의 분자량 범위를 갖는 폴리알킬렌 글리콜 성분, 및 (E) 물보다 NCO 그룹과 더 빨리 반응하는 하나 이상의 활성 수소 원자를 갖는 화합물을, 이들 출발 성분(A) 내지 (E)모두를 기준으로 하여 이소시아네이트 그룹 대 이소시아네이트-반응성 그룹의 수소 원자 총합의 몰비를 0.5:1 내지 2:1 로 유지하면서 반응시킴으로써 의해 수득가능한 친수성 폴리우페탄-폴리우레아를 제공한다.

Description

친수성 폴리우레탄-폴리우레아 및 합성 수지용 분산제로서의 이의 용도
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (11)

  1. (A)하나 이상의 유기 폴리이소시아네이트를 포함하는 폴리이소시아네이트 성분, (B) 하나 이상의 이소시아네이트-반응성 지방산 유도체. (C)필요에 따라, 하이드록실 및 카복실 그룹에서 선택된 두개 이상의 작용성 그룹을 함유하는 화합물, (D)500 내지 10,000/mol의 분자량 범위를 갖는 폴리알킬렌 글리콜 성분, 및 (E)몰보다 NCO 그룹과 더 빨리 반응하는 하나 이상의 활성 수소 원자를 갖는 화합물을, 이들 출발성분(A) 내지 (E)모두를 기준으로 하여 이소시아네이트 그룹 디이소시아네이트-반응성 그룹의 수소 원자 총합의 몰비를 0.5:1 내지 2:1로 유지하면서 반응킴으로써 수득가능한 친수성 폴리우레탄-폴리우레아.
  2. 제1항에 있어서, 모든 출발성분(A) 내지 (E)를 기준으로하여, 이소시아네이트 그룹 대 하이드록실 및 아미노 그룹의 총수소 원자의 몰비가 0.7:1 내지 1.5:1인 친수성 폴리우레탄-폴리우레아.
  3. 제1항에 있어서, 성분(A)1mol당 0.1 내지 1mol의 성분(B), 0 내지 0.8mol의 성분(C), 0.1 내지 0.8mol의 성분(D) 및 0.01 내지 0.3mol의 성분(E)를 사용하는 친수성 폴리우레탄-폴리우레아.
  4. 제1항에 있어서, 성분(B)가 불포화된 친수성 폴리우레탄-폴리우레아.
  5. 제1항에 있어서, 성분(B)가 지방 알콜, 지방 아민 및 1 내지 30개의 에틸렌 옥사이드 단위를 갖는 에톡시화된 지방 알콜 및 지방 아민에서 선택되는 친수성 폴리우레탄-폴리우레아.
  6. 제1항에, 성분(B)가 1 내지 20개의 에틸렌 옥사이드 단위를 갖는 에톡시화된 지방 알콜인 친수성 폴리우레탄-폴리우레아.
  7. 제1하에 있어서, 성분(B)가 폴리올을 갖는 지방산의 반응 생성물이면서도 아미노 그룹을 함유할 수 있는 친수성 폴리우레탄-폴리우레아.
  8. 제1항에 있어서, 성분(B)가 지방산과 모노에폭사이드의 반응 생성물인 친수성 폴리우레탄-폴리우레아.
  9. 제1항에있어서, 성분(C)가 비스하이드록시알칸 카복실산인 친수성 폴리우레탄-폴리우레아.
  10. 제1항에 있어서,성분(C)가 디메틸올프로피온산인 친수성 폴리우레탄-폴리우레아.
  11. 추가의 유화제를 사용하거나 사용하지 않고, 수성 합성-수지 분산액의 제조시 물에 분산될 수 없는 합성 수지용 유화제로서 제1항에 따른 친수성 폴리우레탄-폴리우레아를 사용하는 방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019950011105A 1994-05-09 1995-05-08 친수성 폴리우레탄-폴리우레아 및 합성 수지용 분산제로서의 이의 용도 KR950032358A (ko)

Applications Claiming Priority (2)

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DE4416336A DE4416336A1 (de) 1994-05-09 1994-05-09 Hydrophile Polyurethan-Polyharnstoffe und deren Verwendung als Dispergiermittel für Kunstharze
DEP4416336.3 1994-05-09

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KR950032358A true KR950032358A (ko) 1995-12-20

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EP (1) EP0682049A1 (ko)
JP (1) JPH0848743A (ko)
KR (1) KR950032358A (ko)
AU (1) AU1792295A (ko)
BR (1) BR9501946A (ko)
CA (1) CA2148550A1 (ko)
CZ (1) CZ118595A3 (ko)
DE (1) DE4416336A1 (ko)
ZA (1) ZA953669B (ko)

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BR9608714A (pt) * 1995-06-07 1999-06-29 Sherwin Williams Co Tintas penetrantes e selantes de dispersões de poliuretano
US6191213B1 (en) 1996-06-06 2001-02-20 The Sherwin-Williams Company Penetrating stains and sealants from polyurethane dispersions
US6087444A (en) * 1996-09-20 2000-07-11 Ppg Industries Ohio, Inc. Humidity resistant aqueous urethane resins based on hydrophobic polyhydroxy compounds and coatings
DE19822603A1 (de) 1998-05-20 1999-11-25 Goldschmidt Ag Th Pigmentpasten enthaltend hydrophob modifizierte Polyasparaginsäurederivate
DE19852621A1 (de) * 1998-11-14 2000-05-18 Hansa Textilchemie Gmbh Permanentes Mittel zum Ausrüsten von Fasern oder aus Faser bestehenden Produkten
DE19930961A1 (de) 1999-07-05 2001-01-11 Bayer Ag Polyurethan-Dispersionen
DE10215053A1 (de) 2002-04-05 2003-10-23 Bayer Ag Polyurethan-Dispersionen auf Basis von Fettsäuredialkanolamiden
DE10232908A1 (de) 2002-07-19 2004-01-29 Goldschmidt Ag Verwendung organfunktionell modifizierter, Phenylderivate enthaltender Polysiloxane als Dispergier- und Netzmittel für Füllstoffe und Pigmente in wässrigen Pigmentpasten und Farb- oder Lackformulierungen
DE10334753A1 (de) * 2003-07-30 2005-03-10 Constr Res & Tech Gmbh Selbstvernetzende hochmolekulare Polyurethan-Dispersion
EP1566413B1 (de) 2004-02-20 2006-04-19 Goldschmidt GmbH Verfahren zur Herstellung von homogenen, lagerstabilen Pasten, Farben, Lacken unter Mitverwendung ionischer Flüssigkeiten als Dispergierhilfsmittel
US7968197B2 (en) * 2005-08-25 2011-06-28 Ppg Industries Ohio, Inc. Polyurea coating comprising an amine/(meth)acrylate oligomeric reaction product
EP2765147A1 (en) * 2013-02-06 2014-08-13 Momentive Specialty Chemicals Research Belgium S.A. Aqueous polyurethane dispersion derived from tertiary alkyl glycidyl esters
PL2895522T3 (pl) * 2012-09-13 2021-08-16 Hexion Research Belgium Sa Wodna dyspersja poliuretanowa pochodząca z estrów tert-alkilo-glicydylowych
ES2706826T3 (es) 2015-12-10 2019-04-01 Covestro Deutschland Ag Dispersiones de poliuretano de secado oxidativo con una resistencia a productos químicos especialmente alta
CN107602782B (zh) * 2017-08-22 2022-08-09 山西省建筑科学研究院 含聚脲结构的聚羧酸减水剂的制备方法
CN112778498B (zh) * 2019-11-05 2023-05-26 万华化学集团股份有限公司 一种水性改性聚氨酯分散体及其用途与其制备的头发调理剂

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CA1131376A (en) * 1976-10-04 1982-09-07 David G. Hangauer, Jr. Aqueous urea-urethane dispersions
DE4022539A1 (de) * 1990-07-16 1992-01-23 Henkel Kgaa Polyurethane fuer die ledergrundierug
US5198508A (en) * 1990-09-18 1993-03-30 Mitsui Toatsu Chemicals, Inc. Resin compositions and molded articles
DE4306946A1 (de) * 1993-03-05 1994-09-08 Hoechst Ag Ungesättigte Polyurethane und deren Verwendung als Dispergiermittel für Alkydharze

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BR9501946A (pt) 1995-12-12
CZ118595A3 (en) 1995-11-15
EP0682049A1 (de) 1995-11-15
AU1792295A (en) 1995-11-16
DE4416336A1 (de) 1995-11-16
CA2148550A1 (en) 1995-11-10
ZA953669B (en) 1996-11-08

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