KR920021478A - 퍼플루오로 알킬 브로마이드의 합성 - Google Patents
퍼플루오로 알킬 브로마이드의 합성 Download PDFInfo
- Publication number
- KR920021478A KR920021478A KR1019920008640A KR920008640A KR920021478A KR 920021478 A KR920021478 A KR 920021478A KR 1019920008640 A KR1019920008640 A KR 1019920008640A KR 920008640 A KR920008640 A KR 920008640A KR 920021478 A KR920021478 A KR 920021478A
- Authority
- KR
- South Korea
- Prior art keywords
- process according
- synthesis
- carried out
- perfluoroalkyl
- bromide
- Prior art date
Links
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
- C07C17/202—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction
- C07C17/204—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms two or more compounds being involved in the reaction the other compound being a halogen
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C19/00—Acyclic saturated compounds containing halogen atoms
- C07C19/08—Acyclic saturated compounds containing halogen atoms containing fluorine
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C17/00—Preparation of halogenated hydrocarbons
- C07C17/093—Preparation of halogenated hydrocarbons by replacement by halogens
- C07C17/20—Preparation of halogenated hydrocarbons by replacement by halogens of halogen atoms by other halogen atoms
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Acyclic And Carbocyclic Compounds In Medicinal Compositions (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (12)
- 반응이 기체상에서 수행됨을 특징으로 하는, 상응하는 퍼플루오로 알킬 요오다이드 RF-I과 브롬의 반응에 의한 퍼플루오로알킬 브로마이드 AF-Br(RF는 2 내지 12개의 탄소원자를 포함하는 선형 또는 측쇄 퍼플루오로알킬 라디칼)의 연속적인 제조방법.
- 제1항에 있어서, 200℃와 600℃사이의 온도에서, 바람직하게는 350℃와 500℃사이의 온도에서 수행되는 방법.
- 제1항 또는 제2항에 있어서, Br2/RFI몰비가 0.1 내지 2사이, 바람직하게는 0.3 내지 1사이인 방법.
- 제1항 또는 제2항에 있어서, 불활성 희석제의 존재하에, 바람직하게는 질소의 존재하에서 수행되는 방법.
- 제1항 또는 제2항에 있어서, 접촉시간이 1초 내지 2분 사이인, 바람직하게는 5초 내지 30초 사이인 방법.
- 제1항 또는 제2항에 있어서, 대기압에서 수행되는 방법.
- 제1항 또는 제2항에 있어서, 브롬 및 RFI의 균일 혼합물이 반응기로 도입되는 방법.
- 제1항 또는 제2항에 있어서, Br2/RFI의 몰비를 0.5이하로 수행한 다음, 요오드를 반응 혼합물에서 분리하여, RFBr/RFI 혼합물을 수득하고, 이를 증류시켜 RFI를 재순환시키거나 보충 브롬을 가하여 2차 반응기에서 반응기에서 반응을 종료하는 방법.
- 제1항 내지 제8항의 어느 한 항에 있어서, 따르는 방법의 퍼플루오로옥틸 브로마이드 합성에의 응용.
- 제1항 내지 제8항의 어느 한 항에 있어서, 따르는 방법의 퍼플루오로헥실 브로마이드 합성에의 응용.
- 제1항 내지 제8항의 어느 한 항에 있어서, 따르는 방법의 퍼플루오로데실 브로마이드 합성에의 응용.
- 제1항 내지 제8항의 어느 한 항에 있어서, 따르는 방법의 퍼플루오로알킬 브로마이드 혼합물의 합성에의 응용.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
FR9106114 | 1991-05-21 | ||
FR9106114A FR2676731A1 (fr) | 1991-05-21 | 1991-05-21 | Synthese de bromures de perfluoroalkyle. |
FR91-9106114 | 1991-05-21 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR920021478A true KR920021478A (ko) | 1992-12-18 |
KR950012995B1 KR950012995B1 (ko) | 1995-10-24 |
Family
ID=9412960
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019920008640A KR950012995B1 (ko) | 1991-05-21 | 1992-05-21 | 퍼플루오로 알킬 브로마이드의 합성 |
Country Status (15)
Country | Link |
---|---|
EP (1) | EP0515258B1 (ko) |
KR (1) | KR950012995B1 (ko) |
CN (1) | CN1032306C (ko) |
AT (1) | ATE110705T1 (ko) |
AU (1) | AU642350B2 (ko) |
CA (1) | CA2069018C (ko) |
DK (1) | DK0515258T3 (ko) |
ES (1) | ES2057968T3 (ko) |
FI (1) | FI922293A (ko) |
FR (1) | FR2676731A1 (ko) |
HU (1) | HU207506B (ko) |
IE (1) | IE64724B1 (ko) |
IL (2) | IL101772A0 (ko) |
NO (1) | NO177636C (ko) |
ZA (1) | ZA923664B (ko) |
Families Citing this family (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
DE4027766A1 (de) * | 1990-09-01 | 1992-03-05 | Riedel De Haen Ag | Verfahren zur herstellung von weitgehend fluorierten alkylbromiden |
FR2710053B1 (fr) * | 1993-09-16 | 1995-11-03 | Atochem Elf Sa | Fabrication des bromures de perfluoroalkyle solides. |
CN116903433A (zh) * | 2023-07-12 | 2023-10-20 | 安徽科芯微流化工科技有限公司 | 一种微通道反应制备全氟溴辛烷的方法 |
Family Cites Families (7)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US4588719A (en) * | 1984-04-27 | 1986-05-13 | William H. Rorer, Inc. | Bicyclic benzenoid aminoalkylene ethers and thioethers, pharmaceutical compositions and use |
JPS60184033A (ja) * | 1984-03-02 | 1985-09-19 | Daikin Ind Ltd | パ−フルオロアルキルブロマイドの製造方法 |
IT1200594B (it) * | 1985-02-26 | 1989-01-27 | Montefluos Spa | Procedimento per la preparazione di alfa-omega-aloperfluorocarburi |
FR2617836B1 (fr) * | 1987-07-10 | 1989-12-01 | Atochem | Synthese des bromures de perfluoroalkyle |
FR2655039B1 (fr) * | 1989-11-24 | 1992-02-21 | Atochem | Synthese des bromures de perfluoroalkyle. |
JP2797626B2 (ja) * | 1990-04-03 | 1998-09-17 | 旭硝子株式会社 | パーフルオロアルキルブロマイドの製造方法 |
DE4116361A1 (de) * | 1990-06-23 | 1992-01-02 | Hoechst Ag | Verfahren zur herstellung von perfluoralkylmonobromiden |
-
1991
- 1991-05-21 FR FR9106114A patent/FR2676731A1/fr active Pending
-
1992
- 1992-05-04 IL IL101772A patent/IL101772A0/xx unknown
- 1992-05-04 IL IL19177292A patent/IL101772A/en not_active IP Right Cessation
- 1992-05-18 ES ES92401350T patent/ES2057968T3/es not_active Expired - Lifetime
- 1992-05-18 DK DK92401350.1T patent/DK0515258T3/da active
- 1992-05-18 AT AT92401350T patent/ATE110705T1/de not_active IP Right Cessation
- 1992-05-18 EP EP92401350A patent/EP0515258B1/fr not_active Expired - Lifetime
- 1992-05-20 ZA ZA923664A patent/ZA923664B/xx unknown
- 1992-05-20 HU HU9201683A patent/HU207506B/hu not_active IP Right Cessation
- 1992-05-20 AU AU17038/92A patent/AU642350B2/en not_active Ceased
- 1992-05-20 FI FI922293A patent/FI922293A/fi not_active Application Discontinuation
- 1992-05-20 NO NO921992A patent/NO177636C/no unknown
- 1992-05-20 CA CA002069018A patent/CA2069018C/fr not_active Expired - Fee Related
- 1992-05-21 KR KR1019920008640A patent/KR950012995B1/ko not_active IP Right Cessation
- 1992-05-21 CN CN92103936A patent/CN1032306C/zh not_active Expired - Fee Related
- 1992-07-01 IE IE921621A patent/IE64724B1/en not_active IP Right Cessation
Also Published As
Publication number | Publication date |
---|---|
EP0515258B1 (fr) | 1994-08-31 |
IE64724B1 (en) | 1995-08-23 |
EP0515258A1 (fr) | 1992-11-25 |
ZA923664B (en) | 1993-02-24 |
IE921621A1 (en) | 1992-12-02 |
KR950012995B1 (ko) | 1995-10-24 |
NO177636C (no) | 1995-10-25 |
FR2676731A1 (fr) | 1992-11-27 |
ES2057968T3 (es) | 1994-10-16 |
DK0515258T3 (da) | 1995-02-13 |
HU9201683D0 (en) | 1992-08-28 |
ATE110705T1 (de) | 1994-09-15 |
AU642350B2 (en) | 1993-10-14 |
AU1703892A (en) | 1992-11-26 |
FI922293A (fi) | 1992-11-22 |
NO177636B (no) | 1995-07-17 |
CN1032306C (zh) | 1996-07-17 |
HU207506B (en) | 1993-04-28 |
FI922293A0 (fi) | 1992-05-20 |
NO921992L (no) | 1992-11-23 |
CA2069018C (fr) | 1997-05-13 |
HUT60987A (en) | 1992-11-30 |
IL101772A0 (en) | 1992-12-30 |
IL101772A (en) | 1996-01-19 |
CN1067239A (zh) | 1992-12-23 |
CA2069018A1 (fr) | 1992-11-22 |
NO921992D0 (no) | 1992-05-20 |
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