KR920001740B1 - 멜라민을 제조하는 연속법 및 이를 위한 플랜트 시스템 - Google Patents
멜라민을 제조하는 연속법 및 이를 위한 플랜트 시스템 Download PDFInfo
- Publication number
 - KR920001740B1 KR920001740B1 KR1019840008590A KR840008590A KR920001740B1 KR 920001740 B1 KR920001740 B1 KR 920001740B1 KR 1019840008590 A KR1019840008590 A KR 1019840008590A KR 840008590 A KR840008590 A KR 840008590A KR 920001740 B1 KR920001740 B1 KR 920001740B1
 - Authority
 - KR
 - South Korea
 - Prior art keywords
 - melamine
 - liquid
 - product
 - pressure
 - temperature
 - Prior art date
 - Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
 - Expired
 
Links
- JDSHMPZPIAZGSV-UHFFFAOYSA-N melamine Chemical compound NC1=NC(N)=NC(N)=N1 JDSHMPZPIAZGSV-UHFFFAOYSA-N 0.000 title claims description 164
 - 229920000877 Melamine resin Polymers 0.000 title claims description 160
 - 238000010924 continuous production Methods 0.000 title claims description 4
 - QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 85
 - 239000000047 product Substances 0.000 claims description 75
 - 238000006243 chemical reaction Methods 0.000 claims description 71
 - 239000007789 gas Substances 0.000 claims description 60
 - XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 claims description 57
 - 239000004202 carbamide Substances 0.000 claims description 57
 - 239000007788 liquid Substances 0.000 claims description 53
 - 238000000926 separation method Methods 0.000 claims description 45
 - 238000000034 method Methods 0.000 claims description 38
 - 238000005406 washing Methods 0.000 claims description 37
 - 238000001816 cooling Methods 0.000 claims description 29
 - 238000010791 quenching Methods 0.000 claims description 10
 - YSRVJVDFHZYRPA-UHFFFAOYSA-N melem Chemical compound NC1=NC(N23)=NC(N)=NC2=NC(N)=NC3=N1 YSRVJVDFHZYRPA-UHFFFAOYSA-N 0.000 claims description 8
 - 239000007787 solid Substances 0.000 claims description 8
 - YZEZMSPGIPTEBA-UHFFFAOYSA-N 2-n-(4,6-diamino-1,3,5-triazin-2-yl)-1,3,5-triazine-2,4,6-triamine Chemical compound NC1=NC(N)=NC(NC=2N=C(N)N=C(N)N=2)=N1 YZEZMSPGIPTEBA-UHFFFAOYSA-N 0.000 claims description 7
 - 239000007795 chemical reaction product Substances 0.000 claims description 7
 - 238000002844 melting Methods 0.000 claims description 7
 - 230000008018 melting Effects 0.000 claims description 7
 - 230000000171 quenching effect Effects 0.000 claims description 7
 - 238000000746 purification Methods 0.000 claims description 4
 - 238000000354 decomposition reaction Methods 0.000 claims 1
 - 229910000069 nitrogen hydride Inorganic materials 0.000 claims 1
 - 238000003825 pressing Methods 0.000 claims 1
 - 238000000197 pyrolysis Methods 0.000 claims 1
 - 230000001105 regulatory effect Effects 0.000 claims 1
 - 229910021529 ammonia Inorganic materials 0.000 description 34
 - CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 description 26
 - 239000003054 catalyst Substances 0.000 description 17
 - 229910002092 carbon dioxide Inorganic materials 0.000 description 13
 - 239000001569 carbon dioxide Substances 0.000 description 13
 - 239000002245 particle Substances 0.000 description 10
 - 239000012535 impurity Substances 0.000 description 8
 - 238000001953 recrystallisation Methods 0.000 description 7
 - XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 7
 - 239000013078 crystal Substances 0.000 description 6
 - 239000000843 powder Substances 0.000 description 6
 - 239000000243 solution Substances 0.000 description 6
 - 239000006227 byproduct Substances 0.000 description 5
 - 239000002826 coolant Substances 0.000 description 5
 - KXDHJXZQYSOELW-UHFFFAOYSA-M Carbamate Chemical compound NC([O-])=O KXDHJXZQYSOELW-UHFFFAOYSA-M 0.000 description 4
 - PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 4
 - 230000015572 biosynthetic process Effects 0.000 description 4
 - 238000003786 synthesis reaction Methods 0.000 description 4
 - 238000012546 transfer Methods 0.000 description 4
 - NLXLAEXVIDQMFP-UHFFFAOYSA-N Ammonium chloride Substances [NH4+].[Cl-] NLXLAEXVIDQMFP-UHFFFAOYSA-N 0.000 description 3
 - VHUUQVKOLVNVRT-UHFFFAOYSA-N Ammonium hydroxide Chemical compound [NH4+].[OH-] VHUUQVKOLVNVRT-UHFFFAOYSA-N 0.000 description 3
 - OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 3
 - 235000011114 ammonium hydroxide Nutrition 0.000 description 3
 - 238000009833 condensation Methods 0.000 description 3
 - 230000005494 condensation Effects 0.000 description 3
 - 238000007796 conventional method Methods 0.000 description 3
 - 238000005265 energy consumption Methods 0.000 description 3
 - 239000003337 fertilizer Substances 0.000 description 3
 - 238000001914 filtration Methods 0.000 description 3
 - 238000010438 heat treatment Methods 0.000 description 3
 - 239000002002 slurry Substances 0.000 description 3
 - 239000000126 substance Substances 0.000 description 3
 - 239000004215 Carbon black (E152) Substances 0.000 description 2
 - 238000009835 boiling Methods 0.000 description 2
 - 230000003197 catalytic effect Effects 0.000 description 2
 - 238000005260 corrosion Methods 0.000 description 2
 - 230000007797 corrosion Effects 0.000 description 2
 - 238000013461 design Methods 0.000 description 2
 - 239000012467 final product Substances 0.000 description 2
 - 229930195733 hydrocarbon Natural products 0.000 description 2
 - 150000002430 hydrocarbons Chemical class 0.000 description 2
 - 239000000543 intermediate Substances 0.000 description 2
 - 238000004519 manufacturing process Methods 0.000 description 2
 - 239000000463 material Substances 0.000 description 2
 - VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 description 2
 - 239000000203 mixture Substances 0.000 description 2
 - 238000012986 modification Methods 0.000 description 2
 - 230000004048 modification Effects 0.000 description 2
 - 238000012545 processing Methods 0.000 description 2
 - 238000011084 recovery Methods 0.000 description 2
 - 150000003839 salts Chemical class 0.000 description 2
 - 230000000153 supplemental effect Effects 0.000 description 2
 - 241000283690 Bos taurus Species 0.000 description 1
 - 229910000975 Carbon steel Inorganic materials 0.000 description 1
 - 229910001069 Ti alloy Inorganic materials 0.000 description 1
 - RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
 - 238000010521 absorption reaction Methods 0.000 description 1
 - 150000001298 alcohols Chemical class 0.000 description 1
 - 239000012670 alkaline solution Substances 0.000 description 1
 - 229910045601 alloy Inorganic materials 0.000 description 1
 - 239000000956 alloy Substances 0.000 description 1
 - ZEYWAHILTZGZBH-UHFFFAOYSA-N azane;carbon dioxide Chemical compound N.O=C=O ZEYWAHILTZGZBH-UHFFFAOYSA-N 0.000 description 1
 - 229910052799 carbon Inorganic materials 0.000 description 1
 - 238000004140 cleaning Methods 0.000 description 1
 - 230000006835 compression Effects 0.000 description 1
 - 238000007906 compression Methods 0.000 description 1
 - 239000000470 constituent Substances 0.000 description 1
 - 239000000498 cooling water Substances 0.000 description 1
 - 238000002425 crystallisation Methods 0.000 description 1
 - 230000008025 crystallization Effects 0.000 description 1
 - 230000001627 detrimental effect Effects 0.000 description 1
 - 238000001035 drying Methods 0.000 description 1
 - 230000005611 electricity Effects 0.000 description 1
 - 238000009434 installation Methods 0.000 description 1
 - 239000000155 melt Substances 0.000 description 1
 - 244000005700 microbiome Species 0.000 description 1
 - 239000012452 mother liquor Substances 0.000 description 1
 - 239000003345 natural gas Substances 0.000 description 1
 - QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
 - 230000009972 noncorrosive effect Effects 0.000 description 1
 - 238000002360 preparation method Methods 0.000 description 1
 - 239000002994 raw material Substances 0.000 description 1
 - 239000000376 reactant Substances 0.000 description 1
 - 239000012495 reaction gas Substances 0.000 description 1
 - 238000004064 recycling Methods 0.000 description 1
 - 239000003507 refrigerant Substances 0.000 description 1
 - 239000004576 sand Substances 0.000 description 1
 - 229920006395 saturated elastomer Polymers 0.000 description 1
 - 239000002689 soil Substances 0.000 description 1
 - 239000012265 solid product Substances 0.000 description 1
 - 239000007858 starting material Substances 0.000 description 1
 - 229910052719 titanium Inorganic materials 0.000 description 1
 - 239000010936 titanium Substances 0.000 description 1
 - 238000009834 vaporization Methods 0.000 description 1
 - 230000008016 vaporization Effects 0.000 description 1
 
Images
Classifications
- 
        
- B—PERFORMING OPERATIONS; TRANSPORTING
 - B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
 - B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
 - B01J3/00—Processes of utilising sub-atmospheric or super-atmospheric pressure to effect chemical or physical change of matter; Apparatus therefor
 - B01J3/04—Pressure vessels, e.g. autoclaves
 - B01J3/042—Pressure vessels, e.g. autoclaves in the form of a tube
 
 - 
        
- C—CHEMISTRY; METALLURGY
 - C07—ORGANIC CHEMISTRY
 - C07D—HETEROCYCLIC COMPOUNDS
 - C07D251/00—Heterocyclic compounds containing 1,3,5-triazine rings
 - C07D251/02—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings
 - C07D251/12—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
 - C07D251/26—Heterocyclic compounds containing 1,3,5-triazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with only hetero atoms directly attached to ring carbon atoms
 - C07D251/40—Nitrogen atoms
 - C07D251/54—Three nitrogen atoms
 - C07D251/56—Preparation of melamine
 - C07D251/60—Preparation of melamine from urea or from carbon dioxide and ammonia
 
 
Landscapes
- Chemical & Material Sciences (AREA)
 - Organic Chemistry (AREA)
 - Chemical Kinetics & Catalysis (AREA)
 - Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
 
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title | 
|---|---|---|---|
| US56840884A | 1984-01-05 | 1984-01-05 | |
| US568,408 | 1984-03-05 | 
Publications (2)
| Publication Number | Publication Date | 
|---|---|
| KR850005425A KR850005425A (ko) | 1985-08-26 | 
| KR920001740B1 true KR920001740B1 (ko) | 1992-02-24 | 
Family
ID=24271166
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date | 
|---|---|---|---|
| KR1019840008590A Expired KR920001740B1 (ko) | 1984-01-05 | 1984-12-31 | 멜라민을 제조하는 연속법 및 이를 위한 플랜트 시스템 | 
Country Status (16)
Families Citing this family (8)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| US5514796A (en) * | 1995-06-07 | 1996-05-07 | Melamine Chemicals, Inc. | Melamine of improved purity produced by high-pressure, non-catalytic process | 
| NL1002669C2 (nl) * | 1996-03-21 | 1997-09-23 | Dsm Nv | Werkwijze voor de bereiding van melamine. | 
| NL1003105C2 (nl) * | 1996-05-14 | 1997-11-18 | Dsm Nv | Werkwijze voor de bereiding van melamine. | 
| NL1003328C2 (nl) * | 1996-06-13 | 1997-12-17 | Dsm Nv | Werkwijze voor het bereiden van melamine. | 
| NL1003709C2 (nl) * | 1996-07-30 | 1998-02-05 | Dsm Nv | Werkwijze voor het bereiden van melamine. | 
| NL1004814C2 (nl) * | 1996-12-18 | 1998-06-19 | Dsm Nv | Werkwijze voor het bereiden van melamine. | 
| AU5346298A (en) * | 1996-12-16 | 1998-07-15 | Dsm N.V. | Method for the preparation of melamine | 
| NL1008571C2 (nl) * | 1998-03-12 | 1999-07-28 | Dsm Nv | Kristallijn melamine. | 
Family Cites Families (4)
| Publication number | Priority date | Publication date | Assignee | Title | 
|---|---|---|---|---|
| DE1670286A1 (de) * | 1967-11-11 | 1971-01-28 | Basf Ag | Verfahren zur Aufarbeitung der bei der Melaminsynthese anfallenden Abgase | 
| GB1218522A (en) * | 1969-01-24 | 1971-01-06 | Nissan Chemical Ind Ltd | A process for recovering the purified melamine | 
| NL7903473A (nl) * | 1979-05-03 | 1980-11-05 | Stamicarbon | Werkwijze voor het bereiden van melamine. | 
| NL8201479A (nl) * | 1982-04-07 | 1983-11-01 | Stamicarbon | Werkwijze voor het bereiden van melamine. | 
- 
        1984
        
- 1984-12-18 CA CA000470380A patent/CA1220476A/en not_active Expired
 - 1984-12-18 IE IE3247/84A patent/IE57911B1/en not_active IP Right Cessation
 - 1984-12-19 NL NL8403843A patent/NL193832C/nl not_active IP Right Cessation
 - 1984-12-20 NZ NZ210678A patent/NZ210678A/en unknown
 - 1984-12-26 EG EG817/84A patent/EG16900A/xx active
 - 1984-12-27 ES ES539126A patent/ES8606303A1/es not_active Expired
 - 1984-12-27 NO NO845248A patent/NO176795C/no not_active IP Right Cessation
 - 1984-12-29 JP JP59282026A patent/JPS60208970A/ja active Granted
 - 1984-12-31 KR KR1019840008590A patent/KR920001740B1/ko not_active Expired
 
 - 
        1985
        
- 1985-01-04 GB GB08500197A patent/GB2152505B/en not_active Expired
 - 1985-01-04 BR BR8500032A patent/BR8500032A/pt not_active IP Right Cessation
 - 1985-01-04 FR FR858500073A patent/FR2557876B1/fr not_active Expired - Lifetime
 - 1985-01-04 MX MX203965A patent/MX164901B/es unknown
 - 1985-01-04 AU AU37376/85A patent/AU568469B2/en not_active Expired
 - 1985-01-04 IT IT83302/85A patent/IT1188084B/it active
 - 1985-01-04 AT AT21/85A patent/AT393124B/de not_active IP Right Cessation
 
 - 
        1996
        
- 1996-01-24 JP JP8029814A patent/JP2757163B2/ja not_active Expired - Lifetime
 
 
Also Published As
| Publication number | Publication date | 
|---|---|
| NL193832B (nl) | 2000-08-01 | 
| JP2757163B2 (ja) | 1998-05-25 | 
| JPH0925271A (ja) | 1997-01-28 | 
| FR2557876B1 (fr) | 1991-04-19 | 
| NO845248L (no) | 1985-07-08 | 
| GB2152505A (en) | 1985-08-07 | 
| CA1220476A (en) | 1987-04-14 | 
| NL8403843A (nl) | 1985-08-01 | 
| NO176795C (no) | 1995-05-31 | 
| IT1188084B (it) | 1987-12-30 | 
| NL193832C (nl) | 2000-12-04 | 
| JPS60208970A (ja) | 1985-10-21 | 
| ES539126A0 (es) | 1986-04-16 | 
| IE57911B1 (en) | 1993-05-19 | 
| IT8583302A0 (it) | 1985-01-04 | 
| FR2557876A1 (fr) | 1985-07-12 | 
| NZ210678A (en) | 1987-03-06 | 
| KR850005425A (ko) | 1985-08-26 | 
| AT393124B (de) | 1991-08-26 | 
| IE843247L (en) | 1985-07-05 | 
| BR8500032A (pt) | 1985-08-13 | 
| EG16900A (en) | 1990-10-30 | 
| AU3737685A (en) | 1985-07-18 | 
| ATA2185A (de) | 1991-01-15 | 
| ES8606303A1 (es) | 1986-04-16 | 
| AU568469B2 (en) | 1987-12-24 | 
| JPH0557984B2 (GUID-C5D7CC26-194C-43D0-91A1-9AE8C70A9BFF.html) | 1993-08-25 | 
| MX164901B (es) | 1992-09-30 | 
| GB8500197D0 (en) | 1985-02-13 | 
| NO176795B (no) | 1995-02-20 | 
| GB2152505B (en) | 1987-07-29 | 
Similar Documents
| Publication | Publication Date | Title | 
|---|---|---|
| US4565867A (en) | Anhydrous high-pressure melamine synthesis | |
| KR100472913B1 (ko) | 고압,비촉매방법에의해생성된순도가개선된멜라민 | |
| JP2011513348A (ja) | 尿素から高純度メラミンを製造する方法 | |
| KR920001740B1 (ko) | 멜라민을 제조하는 연속법 및 이를 위한 플랜트 시스템 | |
| JPH1045730A (ja) | 尿素反応生成物からメラミンを回収する方法及びメラミン溶融液から固体メラミンを回収する方法 | |
| CA1128515A (en) | Method for the preparation of melamine | |
| KR0129004B1 (ko) | 암모니아와 이산화황의 생성방법 | |
| WO2003095516A1 (en) | Process for the production of melamine from urea, and particularly to obtain melamine-free off-gas in the first separation step | |
| CN101903361A (zh) | 三聚氰胺的制备方法 | |
| AU715825B2 (en) | Method for the preparation of melamine | |
| KR100509078B1 (ko) | 멜라민의 제조방법 | |
| US3578664A (en) | Process for the recovery of melamine from a synthesis gas mixture containing hot melamine vapour | |
| KR100495262B1 (ko) | 멜라민의 제조방법 | |
| US6303781B1 (en) | Method for preparing melamine | |
| WO2024112197A1 (en) | Multiproduct low biuret urea production | |
| DE3500188A1 (de) | Wasserfreie hochdruck-melamin-synthese | |
| MXPA00011109A (en) | Method for preparing melamine | 
Legal Events
| Date | Code | Title | Description | 
|---|---|---|---|
| PA0109 | Patent application | 
             Patent event code: PA01091R01D Comment text: Patent Application Patent event date: 19841231  | 
        |
| PG1501 | Laying open of application | ||
| A201 | Request for examination | ||
| PA0201 | Request for examination | 
             Patent event code: PA02012R01D Patent event date: 19891229 Comment text: Request for Examination of Application Patent event code: PA02011R01I Patent event date: 19841231 Comment text: Patent Application  | 
        |
| G160 | Decision to publish patent application | ||
| PG1605 | Publication of application before grant of patent | 
             Comment text: Decision on Publication of Application Patent event code: PG16051S01I Patent event date: 19920127  | 
        |
| E701 | Decision to grant or registration of patent right | ||
| PE0701 | Decision of registration | 
             Patent event code: PE07011S01D Comment text: Decision to Grant Registration Patent event date: 19920509  | 
        |
| GRNT | Written decision to grant | ||
| PR0701 | Registration of establishment | 
             Comment text: Registration of Establishment Patent event date: 19920626 Patent event code: PR07011E01D  | 
        |
| PR1002 | Payment of registration fee | 
             Payment date: 19920626 End annual number: 3 Start annual number: 1  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 19941209 Start annual number: 4 End annual number: 4  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 19951218 Start annual number: 5 End annual number: 5  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 19961118 Start annual number: 6 End annual number: 6  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 19980203 Start annual number: 7 End annual number: 7  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 19990128 Start annual number: 8 End annual number: 8  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 20000217 Start annual number: 9 End annual number: 9  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 20010220 Start annual number: 10 End annual number: 10  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 20020222 Start annual number: 11 End annual number: 11  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 20030214 Start annual number: 12 End annual number: 12  | 
        |
| FPAY | Annual fee payment | 
             Payment date: 20040219 Year of fee payment: 13  | 
        |
| PR1001 | Payment of annual fee | 
             Payment date: 20040219 Start annual number: 13 End annual number: 13  | 
        |
| EXPY | Expiration of term | ||
| PC1801 | Expiration of term |