KR890010119A - 모노아조 안료, 이의 제조방법 및 용도 - Google Patents
모노아조 안료, 이의 제조방법 및 용도 Download PDFInfo
- Publication number
- KR890010119A KR890010119A KR1019880016688A KR880016688A KR890010119A KR 890010119 A KR890010119 A KR 890010119A KR 1019880016688 A KR1019880016688 A KR 1019880016688A KR 880016688 A KR880016688 A KR 880016688A KR 890010119 A KR890010119 A KR 890010119A
- Authority
- KR
- South Korea
- Prior art keywords
- cation
- active surfactant
- salt
- pigment
- added
- Prior art date
Links
- 239000000049 pigment Substances 0.000 title claims 4
- NYGZLYXAPMMJTE-UHFFFAOYSA-M metanil yellow Chemical group [Na+].[O-]S(=O)(=O)C1=CC=CC(N=NC=2C=CC(NC=3C=CC=CC=3)=CC=2)=C1 NYGZLYXAPMMJTE-UHFFFAOYSA-M 0.000 title 1
- 238000002360 preparation method Methods 0.000 title 1
- 238000000034 method Methods 0.000 claims 8
- 239000004094 surface-active agent Substances 0.000 claims 5
- 230000008878 coupling Effects 0.000 claims 3
- 238000010168 coupling process Methods 0.000 claims 3
- 238000005859 coupling reaction Methods 0.000 claims 3
- 239000004793 Polystyrene Substances 0.000 claims 2
- 239000007900 aqueous suspension Substances 0.000 claims 2
- 229920001577 copolymer Polymers 0.000 claims 2
- 229920000098 polyolefin Polymers 0.000 claims 2
- 229920002223 polystyrene Polymers 0.000 claims 2
- UIXFPIHXQQZAGX-UHFFFAOYSA-N 3-hydroxy-n-(4-methoxyphenyl)naphthalene-2-carboxamide Chemical compound C1=CC(OC)=CC=C1NC(=O)C1=CC2=CC=CC=C2C=C1O UIXFPIHXQQZAGX-UHFFFAOYSA-N 0.000 claims 1
- 238000002441 X-ray diffraction Methods 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 125000005211 alkyl trimethyl ammonium group Chemical group 0.000 claims 1
- 150000003863 ammonium salts Chemical class 0.000 claims 1
- 239000012736 aqueous medium Substances 0.000 claims 1
- 239000000987 azo dye Substances 0.000 claims 1
- 159000000007 calcium salts Chemical class 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 239000011248 coating agent Substances 0.000 claims 1
- 238000000576 coating method Methods 0.000 claims 1
- 238000004040 coloring Methods 0.000 claims 1
- 239000000975 dye Substances 0.000 claims 1
- 229940083124 ganglion-blocking antiadrenergic secondary and tertiary amines Drugs 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 239000002609 medium Substances 0.000 claims 1
- 239000000203 mixture Substances 0.000 claims 1
- 239000003607 modifier Substances 0.000 claims 1
- 239000003960 organic solvent Substances 0.000 claims 1
- 150000004714 phosphonium salts Chemical group 0.000 claims 1
- 239000004033 plastic Substances 0.000 claims 1
- 229920003023 plastic Polymers 0.000 claims 1
- 239000004800 polyvinyl chloride Substances 0.000 claims 1
- 229920000915 polyvinyl chloride Polymers 0.000 claims 1
- 150000003141 primary amines Chemical class 0.000 claims 1
- 150000003242 quaternary ammonium salts Chemical class 0.000 claims 1
- 150000003839 salts Chemical class 0.000 claims 1
- 238000001228 spectrum Methods 0.000 claims 1
- RWSOTUBLDIXVET-UHFFFAOYSA-O sulfonium group Chemical group [SH3+] RWSOTUBLDIXVET-UHFFFAOYSA-O 0.000 claims 1
- 229920002994 synthetic fiber Polymers 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0025—Crystal modifications; Special X-ray patterns
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0025—Crystal modifications; Special X-ray patterns
- C09B67/0028—Crystal modifications; Special X-ray patterns of azo compounds
- C09B67/0029—Crystal modifications; Special X-ray patterns of azo compounds of monoazo compounds
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B67/00—Influencing the physical, e.g. the dyeing or printing properties of dyestuffs without chemical reactions, e.g. by treating with solvents grinding or grinding assistants, coating of pigments or dyes; Process features in the making of dyestuff preparations; Dyestuff preparations of a special physical nature, e.g. tablets, films
- C09B67/0001—Post-treatment of organic pigments or dyes
- C09B67/0014—Influencing the physical properties by treatment with a liquid, e.g. solvents
- C09B67/0015—Influencing the physical properties by treatment with a liquid, e.g. solvents of azoic pigments
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10—TECHNICAL SUBJECTS COVERED BY FORMER USPC
- Y10S—TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y10S534/00—Organic compounds -- part of the class 532-570 series
- Y10S534/04—Azo compounds which are lakes
Landscapes
- Chemical & Material Sciences (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Organic Chemistry (AREA)
- Inks, Pencil-Leads, Or Crayons (AREA)
- Pigments, Carbon Blacks, Or Wood Stains (AREA)
- Paper (AREA)
- Coloring (AREA)
- Pretreatment Of Seeds And Plants (AREA)
- Paints Or Removers (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (10)
- Cu-Kα조사에서, X-선 회절 스펙트럼이 다음의 회절각 2θ(정확도±0.2°)21.9°에서 고강도 최대치의 반사를, 5.40°, 7.30°, 10.85°, 14.50° 및 27.60°에서 중강도 최대치의 반사를, 또한, 10.05°, 12.80°, 16.40°, 17.95°, 24.65° 및 25.80°에서 저강도 최대치의 반사를 보여줌을 특징으로 하는 변형체(β-변형체)로 존재하는 하기 구조식(I)의 안료.
- 유기 용매의 존재 또는 부재하에 수성 매질중에서 알칼리-용해된 2-하이드록시-4'-메톡시-3-나프트아닐리드 사에 디아조화된 N-(3-아미노-4-메틸벤조일)설파닐산을 커플링(coupling)시키고, 칼슘염을 가하여(늦어도 레이킹(laking)전에 하나 이상의 양이온-활성 계면활성제를 가한다) 커플링 생성물을 레이킹시킨 다음, 130 내지 180℃의 온도에서 레이킹 된 아조 염료의 수성 현탁액을 가열시킴을 특징으로 하여, 제1항에서 정의된 구조식(I)의 안료의 β-변형체를 제조하는 방법.
- 제2항에 있어서, 레이킹된 아조 염료의 수성 현탁액을 135 내지 106℃의 온도로 가열시키는 방법.
- 제2항 또는 3항에 있어서, 4급 암모늄염,4급 포스포늄 염, 3급 설포늄염, N,N-디알킬이미다졸린, N-알킬피리디늄 염 및 1급, 2급 및 3급 아민으로 이루어진 그룹중에서 선택된 하나이상의 양이온-활성 계면활성제를 가하는 방법.
- 제2항 내지 4항 중 어느 한 항에 있어서, 양이온-활성 계면활성제가 탄소수 8내지 24의 장쇄 알킬 라디칼을 하나이상 함유하는 방법.
- 제2항 내지 5항중 어느 한항에 있어서, 양이온-활성 계면활성제가 알킬트리메틸 암모늄염 또는 알킬디메틸벤질암모늄염인 방법.
- 제2항 내지 6항 중 어느 한 항에 있어서, 양이온-활성 계면활성제의 첨가량이 산형태인 커플링 생성물의 중량을 기준하여 1 내지 20중량%인 방법.
- 천연 및 합성 물질을 착색시키기 위한 β-변형체로 존재하는 제1항에서 정의된 안료를 사용하는 방법.
- 제8항에 있어서, 프린팅잉크, 표면 피복물, 플라스틱 조성물, 필라멘트 및 제지를 착색시키기 위한 방법.
- 제9항에 있어서, 폴리스티렌, 폴리스테렌계 공중합체, 폴리올레핀, 폴리올레핀의 공중합체 및 포리비닐클로라이드를 착색시키기 위한 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
DEP3742815.2 | 1987-12-17 | ||
DE19873742815 DE3742815A1 (de) | 1987-12-17 | 1987-12-17 | Monoazopigment, verfahren zu seiner herstellung und seine verwendung |
Publications (2)
Publication Number | Publication Date |
---|---|
KR890010119A true KR890010119A (ko) | 1989-08-05 |
KR960011061B1 KR960011061B1 (ko) | 1996-08-16 |
Family
ID=6342840
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019880016688A KR960011061B1 (ko) | 1987-12-17 | 1988-12-15 | 모노아조 안료, 이의 제조방법 및 용도 |
Country Status (7)
Country | Link |
---|---|
US (1) | US5128454A (ko) |
EP (1) | EP0320774B1 (ko) |
JP (1) | JP2667236B2 (ko) |
KR (1) | KR960011061B1 (ko) |
AU (1) | AU602278B2 (ko) |
DE (2) | DE3742815A1 (ko) |
ES (1) | ES2061617T3 (ko) |
Families Citing this family (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CH685162A5 (de) * | 1991-05-07 | 1995-04-13 | Ciba Geigy Ag | Pigmentzusammensetzungen. |
WO1995015920A1 (fr) * | 1993-12-09 | 1995-06-15 | Catalysts & Chemicals Industries Co., Ltd. | Procede et dispositif de production d'oxyde d'aluminium |
JP3839932B2 (ja) * | 1996-09-26 | 2006-11-01 | キヤノン株式会社 | プロセスカートリッジ及び電子写真画像形成装置及び電子写真感光体ドラム及びカップリング |
DE10138770A1 (de) * | 2001-08-07 | 2003-02-20 | Clariant Gmbh | Neue Azopigmente |
Family Cites Families (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
US2573851A (en) * | 1947-11-10 | 1951-11-06 | American Cyanamid Co | Light fast azoic pigments |
US2687410A (en) * | 1951-12-26 | 1954-08-24 | Du Pont | Azo pigment |
US3118870A (en) * | 1961-03-29 | 1964-01-21 | Hoechst Ag | Water-insoluble monoazo-dyestuffs |
US3928315A (en) * | 1970-09-02 | 1975-12-23 | Hoechst Ag | {65 -Modification of phenyl-azo-naphthol pigment |
BE794359A (fr) * | 1972-01-22 | 1973-07-23 | Hoechst Ag | Pigments monoazoiques et leur preparation |
US4002605A (en) * | 1974-08-28 | 1977-01-11 | American Cyanamid Company | Calcium and magnesium salts of 4-(2-hydroxy-1-naphthylazo)-1-naphthalenesulfonic acid for dyeing fiberglass |
DE2521655C2 (de) * | 1975-05-15 | 1983-10-20 | Hoechst Ag, 6230 Frankfurt | Azoverbindungen, Verfahren zu ihrer Herstellung und ihre Verwendung |
JPH0230346B2 (ja) * | 1981-07-22 | 1990-07-05 | Shiseido Co Ltd | Buririantokaamin6bnofukasakukagobutsunoseizoho |
US4453944A (en) * | 1982-04-07 | 1984-06-12 | Ciba-Geigy Corporation | Dye stable to dyeing, processes for producing it, and its use for dyeing and printing synthetic and semi-synthetic fibre materials |
DE3223888A1 (de) * | 1982-06-26 | 1983-12-29 | Hoechst Ag, 6230 Frankfurt | Neue kristallmodifikation von pigment red 53:1 |
-
1987
- 1987-12-17 DE DE19873742815 patent/DE3742815A1/de not_active Withdrawn
-
1988
- 1988-12-07 DE DE3851130T patent/DE3851130D1/de not_active Expired - Lifetime
- 1988-12-07 EP EP88120444A patent/EP0320774B1/de not_active Expired - Lifetime
- 1988-12-07 ES ES88120444T patent/ES2061617T3/es not_active Expired - Lifetime
- 1988-12-15 KR KR1019880016688A patent/KR960011061B1/ko not_active IP Right Cessation
- 1988-12-16 AU AU26957/88A patent/AU602278B2/en not_active Ceased
- 1988-12-16 JP JP63316610A patent/JP2667236B2/ja not_active Expired - Lifetime
-
1990
- 1990-02-21 US US07/482,692 patent/US5128454A/en not_active Expired - Lifetime
Also Published As
Publication number | Publication date |
---|---|
JPH021767A (ja) | 1990-01-08 |
AU602278B2 (en) | 1990-10-04 |
KR960011061B1 (ko) | 1996-08-16 |
JP2667236B2 (ja) | 1997-10-27 |
EP0320774A3 (de) | 1991-09-18 |
AU2695788A (en) | 1989-06-22 |
ES2061617T3 (es) | 1994-12-16 |
DE3851130D1 (de) | 1994-09-22 |
EP0320774A2 (de) | 1989-06-21 |
DE3742815A1 (de) | 1989-07-13 |
EP0320774B1 (de) | 1994-08-17 |
US5128454A (en) | 1992-07-07 |
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A201 | Request for examination | ||
G160 | Decision to publish patent application | ||
E701 | Decision to grant or registration of patent right | ||
GRNT | Written decision to grant | ||
FPAY | Annual fee payment |
Payment date: 20050620 Year of fee payment: 10 |
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LAPS | Lapse due to unpaid annual fee |