KR890002004A - 니트릴의 제조방법 - Google Patents

니트릴의 제조방법 Download PDF

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Publication number
KR890002004A
KR890002004A KR1019880009449A KR880009449A KR890002004A KR 890002004 A KR890002004 A KR 890002004A KR 1019880009449 A KR1019880009449 A KR 1019880009449A KR 880009449 A KR880009449 A KR 880009449A KR 890002004 A KR890002004 A KR 890002004A
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KR
South Korea
Prior art keywords
group
alkylsubstituted
pyrazine
tungsten
compound
Prior art date
Application number
KR1019880009449A
Other languages
English (en)
Other versions
KR0120264B1 (ko
Inventor
신끼찌 시미즈
다까유끼 쇼오지
간지 고오노
도오루 나까이시
Original Assignee
호리 히데다로오
고오에이 가가꾸 고오교오 가부시끼가이샤
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Priority claimed from JP62189168A external-priority patent/JPS6431730A/ja
Priority claimed from JP62189170A external-priority patent/JP2604165B2/ja
Priority claimed from JP62189169A external-priority patent/JPS6431769A/ja
Application filed by 호리 히데다로오, 고오에이 가가꾸 고오교오 가부시끼가이샤 filed Critical 호리 히데다로오
Publication of KR890002004A publication Critical patent/KR890002004A/ko
Application granted granted Critical
Publication of KR0120264B1 publication Critical patent/KR0120264B1/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D213/00—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members
    • C07D213/02—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members
    • C07D213/04—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D213/60—Heterocyclic compounds containing six-membered rings, not condensed with other rings, with one nitrogen atom as the only ring hetero atom and three or more double bonds between ring members or between ring members and non-ring members having three double bonds between ring members or between ring members and non-ring members having no bond between the ring nitrogen atom and a non-ring member or having only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D213/78—Carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, e.g. ester or nitrile radicals
    • C07D213/84—Nitriles
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J23/00—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00
    • B01J23/16—Catalysts comprising metals or metal oxides or hydroxides, not provided for in group B01J21/00 of arsenic, antimony, bismuth, vanadium, niobium, tantalum, polonium, chromium, molybdenum, tungsten, manganese, technetium or rhenium
    • B01J23/24—Chromium, molybdenum or tungsten
    • B01J23/28—Molybdenum
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D241/00—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings
    • C07D241/02—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings not condensed with other rings
    • C07D241/10—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members
    • C07D241/14—Heterocyclic compounds containing 1,4-diazine or hydrogenated 1,4-diazine rings not condensed with other rings having three double bonds between ring members or between ring members and non-ring members with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D241/24—Carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Materials Engineering (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
  • Pyridine Compounds (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)

Abstract

내용 없음

Description

니트닐의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (7)

  1. 알킬치환된 헤테로 방향족 화합물을 분자상 산소 및 암모니아로 하기 구성의 촉매 존재하에 촉매 반응시켜, 헤테로 방향족 니트릴을 제조하는 방법.
    Mo(p)x (A)y(B)z(0)w (Ⅰ)
    위의 조성식애서, x,y,z 및 w는 몰리브덴에 대한 인, A,B 및 산소의 원자비를 나타내며, (ⅰ) x 및 z는 모두 0이고, y는 0.1 내지 5이고, A는 세리움 또는 텅스텐으로 이루어진 그룹으로부터 선택한 1이상의 원소이거나, (ⅱ)x는 0.1 내지 7이고 y는 0 내지 5이고, z는 0 내지 5이고, A는 세리움, 망간 및 텅스텐으로 이루어진 그룹으로부터 선택한 1이상의 기이고, B는 탈리움, 티타니움, 니오비움 및 알루미니움으로 이루어진 그룹으로부터 선택한 1이상의 원소이거나, (ⅲ)x는 0.5 내지 7이고, y는 0 내지 5이고, z는 0.01 내지 2이고, A는 세리움, 망간 및 텅스텅으로 이루어진 그룹으로부터 선택한 1이상의 원소이고, B는 바나디움이고, W는, 물리브덴, 인, 원소 A, 원소 B의 원자가와 X,Y 및 Z의 값으로 부터 결정된다.
  2. 제 1항에 있어서, 알킬치환된 화합물이 알킬치환된 피리딘 및 알킬칙환된 피라진으로 이루어진 그룹으로부터 선택한 1이상의 화합물인 제조방법.
  3. 제 2항에 있어서, 알킬 치확된 피리딘이 디알킬 치환된 피리딜인, 제조방법.
  4. 제 2항에 있어서, 알킬치환된 피라진이 디알킬치환된 피라진인, 제조방법.
  5. 제 1항에 있어서, 촉매를 담체상에 실려 실시하는 제조방법.
  6. 제5항에 있어서, 담체가 ??-알루미나 또는 실리콘카바이드인, 제조방법.
  7. 제 1항에 있어서 반응온도를 300℃ 내지 650℃에서 실시하는 제조방법.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880009449A 1987-07-29 1988-07-27 니트릴의 제조방법 KR0120264B1 (ko)

Applications Claiming Priority (9)

Application Number Priority Date Filing Date Title
JP62-189168 1987-07-29
JP189170 1987-07-29
JP87-189169 1987-07-29
JP62189168A JPS6431730A (en) 1987-07-29 1987-07-29 Production of nitriles
JP87-189168 1987-07-29
JP62189170A JP2604165B2 (ja) 1987-07-29 1987-07-29 ニトリル類の製法
JP87-189170 1987-07-29
JP189169 1987-07-29
JP62189169A JPS6431769A (en) 1987-07-29 1987-07-29 Process for production of nitriles

Publications (2)

Publication Number Publication Date
KR890002004A true KR890002004A (ko) 1989-04-07
KR0120264B1 KR0120264B1 (ko) 1997-11-04

Family

ID=27326137

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019880009449A KR0120264B1 (ko) 1987-07-29 1988-07-27 니트릴의 제조방법

Country Status (4)

Country Link
US (1) US4931561A (ko)
EP (1) EP0301540B1 (ko)
KR (1) KR0120264B1 (ko)
DE (1) DE3875008T2 (ko)

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100715365B1 (ko) * 2003-05-28 2007-05-07 로렐세이키 가부시키가이샤 지폐화상 검출장치

Families Citing this family (9)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR0124970B1 (ko) * 1994-04-27 1997-11-27 강박광 시안화합물 제조용 고체촉매와 그 제조방법
BE1008339A3 (nl) * 1994-05-03 1996-04-02 Dsm Nv Heterogene metathesekatalysator.
KR0128541B1 (ko) * 1994-08-26 1998-04-04 강박광 시아노피라진의 제조방법
DE10335454A1 (de) 2003-08-02 2005-02-24 Reilly Industries, Inc., Indianapolis Verfahren zur Herstellung von Cyanopyridinen und dafür geeignete Katalysatoren
DE102004022897A1 (de) * 2004-05-10 2005-12-08 Bayer Cropscience Ag Azinyl-imidazoazine
DE602005025106D1 (de) 2004-05-11 2011-01-13 Axiogenesis Ag Methoden zur medikamentenaufspürung auf der basis von in vitro differenzierten zellen
US7763225B2 (en) * 2007-06-25 2010-07-27 Ascend Performance Materials Llc Process of catalytic ammoxidation for hydrogen cyanide production
EP2428267A1 (en) 2010-09-08 2012-03-14 Leibniz-Institut für Katalyse e.V. an der Universität Rostock Catalyst, its preparation and use for the preparation of nitriles from alkyl aromatic or heteroaromatic compounds
CN107011274A (zh) * 2017-04-21 2017-08-04 苏州弘森药业股份有限公司 一种制备吡嗪酰胺的方法

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CA483155A (en) * 1952-05-13 Porter Frank Production of nitriles
US2294130A (en) * 1935-12-02 1942-08-25 Solvay Process Co Manufacture of dicarboxylic acid anhydride
US2861999A (en) * 1956-03-27 1958-11-25 Allied Chem Production of cyanopyridines
US3970659A (en) * 1975-11-18 1976-07-20 Merck & Co., Inc. Preparation of cyanopyridines
US3970657A (en) * 1975-11-18 1976-07-20 Merck & Co., Inc. Preparation of cyanopyridines
JPS56139444A (en) * 1980-04-01 1981-10-30 Takeda Chem Ind Ltd Production of aromatic nitrile
DE3107756A1 (de) * 1981-02-28 1982-09-16 Degussa Ag, 6000 Frankfurt Katalysatoren fuer die herstellung von 2-cyanpyrazin
US4603207A (en) * 1985-10-24 1986-07-29 The Standard Oil Company Conversion of a mixture of 3-methylpyridine and 3-methylpiperidine to 3-cyanopyridine
EP0253360B1 (en) * 1986-07-15 1993-12-01 Koei Chemical Co., Ltd. Process for preparing nitriles
US4778890A (en) * 1986-08-04 1988-10-18 Koei Chemical Co., Ltd. Process for preparing nitriles

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100715365B1 (ko) * 2003-05-28 2007-05-07 로렐세이키 가부시키가이샤 지폐화상 검출장치

Also Published As

Publication number Publication date
DE3875008D1 (de) 1992-11-05
US4931561A (en) 1990-06-05
EP0301540A1 (en) 1989-02-01
EP0301540B1 (en) 1992-09-30
DE3875008T2 (de) 1993-04-15
KR0120264B1 (ko) 1997-11-04

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