KR880701294A - 높은 순도의 지르코늄 및 그의 제조방법 - Google Patents

높은 순도의 지르코늄 및 그의 제조방법

Info

Publication number
KR880701294A
KR880701294A KR1019880700183A KR880700183A KR880701294A KR 880701294 A KR880701294 A KR 880701294A KR 1019880700183 A KR1019880700183 A KR 1019880700183A KR 880700183 A KR880700183 A KR 880700183A KR 880701294 A KR880701294 A KR 880701294A
Authority
KR
South Korea
Prior art keywords
sulfuric acid
zirconium
temperature
leaching
high purity
Prior art date
Application number
KR1019880700183A
Other languages
English (en)
Inventor
나라얀 신하 해리
리챠드 호친 말틴
Original Assignee
알프레드 펄내트
코몬웰스 사이언티픽 앤드 인더스트리얼 리서치 오르가니제이션
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 알프레드 펄내트, 코몬웰스 사이언티픽 앤드 인더스트리얼 리서치 오르가니제이션 filed Critical 알프레드 펄내트
Publication of KR880701294A publication Critical patent/KR880701294A/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B3/00—Extraction of metal compounds from ores or concentrates by wet processes
    • C—CHEMISTRY; METALLURGY
    • C04—CEMENTS; CONCRETE; ARTIFICIAL STONE; CERAMICS; REFRACTORIES
    • C04B—LIME, MAGNESIA; SLAG; CEMENTS; COMPOSITIONS THEREOF, e.g. MORTARS, CONCRETE OR LIKE BUILDING MATERIALS; ARTIFICIAL STONE; CERAMICS; REFRACTORIES; TREATMENT OF NATURAL STONE
    • C04B35/00—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products
    • C04B35/01—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics
    • C04B35/48—Shaped ceramic products characterised by their composition; Ceramics compositions; Processing powders of inorganic compounds preparatory to the manufacturing of ceramic products based on oxide ceramics based on zirconium or hafnium oxides, zirconates, zircon or hafnates
    • C04B35/486—Fine ceramics
    • C—CHEMISTRY; METALLURGY
    • C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
    • C22B—PRODUCTION AND REFINING OF METALS; PRETREATMENT OF RAW MATERIALS
    • C22B34/00—Obtaining refractory metals
    • C22B34/10—Obtaining titanium, zirconium or hafnium
    • C22B34/14—Obtaining zirconium or hafnium

Landscapes

  • Chemical & Material Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Organic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Materials Engineering (AREA)
  • Ceramic Engineering (AREA)
  • Mechanical Engineering (AREA)
  • Metallurgy (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Structural Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Environmental & Geological Engineering (AREA)
  • Composite Materials (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geology (AREA)
  • Inorganic Compounds Of Heavy Metals (AREA)
  • Silicates, Zeolites, And Molecular Sieves (AREA)
  • Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
  • Manufacture And Refinement Of Metals (AREA)

Abstract

내용 없음.

Description

높은 순도의 지르코늄 및 그의 제조방법
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음

Claims (6)

  1. 소량의 실리카를 포함하는 지르코늄 함유물질로부터 높은 순도의 산화지르코늄을 제조하는 방법에 있어서, 175℃내지 250℃ 온도에서 상기 소량의 실리카를 포함하는 지르코늄 함유물질을 황산과 함께 침출시키되 황산의 농도는 침출온도에서 끓는 농도로 조절하고 그 후 결과적인 지르코늄 함유 생성물을 회수하는 단계를 포함함을 특징으로 하는 높은 순도의 산화지르코늄 제조방법.
  2. 제 1항에 있어서, 개시 물질은 수산화나트륨에서 침출된 후 플라스마노에서 해리된 지르콘임을 특징으로 하는 높은 순도의 산화지르코늄 제조방법.
  3. 제 1항 또는 제 2항에 있어서, 상기 침출 과정은 그 과정의 온도에서 끓는 농도를 가지는 황산을 사용하여 개시하고 지속시킴을 특징으로 하는 높은 순도의 산화지르코늄 제조방법.
  4. 제 3항에 있어서, 상기 침출 과정은 80중량% 내지 88중량% 농도의 황산을 사용하여 200℃ 내지 250℃의 온도에서 진행함을 특징으로 하는 높은 순도의 산화지르코늄 제조방법.
  5. 제 1항 또는 2항에 있어서, 소량의 실리카를 포함하는 지르코늄 함유물질을 175℃ 내지 250℃의 온도에서 황산과 함게 침출시키되 반응 개시에 있어서 진한(98%) 황산을 사용함으로써 침출 온도에서 끓는 농도의 황산이 될 때까지 황산의 희석제로서 물이 생성됨을 특징으로 하는 높은 순도의 산화지르코늄 제조방법.
  6. 소량의 실리카를 포함하는 지르코늄 함유물질을 175℃ 내지 250℃의 온도에서 황산과 함게 침출시키되 황산은 그 침출온도에서 끓는 농도의 황산을 사용하고 그 후 결과적인 지르코늄 함유 생성물을 회수함으로써 소량의 싫리키를 포함하는 지르코늄 함유물질로부터 제조한 높은 순도의 산화지르코늄.
    ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
KR1019880700183A 1986-06-18 1987-06-05 높은 순도의 지르코늄 및 그의 제조방법 KR880701294A (ko)

Applications Claiming Priority (5)

Application Number Priority Date Filing Date Title
AUPH646486 1986-06-18
AUPH670086 1986-07-02
AU6700 1986-07-02
PCT/AU1987/000162 WO1987007915A1 (en) 1986-06-18 1987-06-05 Manufacture of high purity zirconia from low-silica zirconiferous materials
AU6464 1998-10-12

Publications (1)

Publication Number Publication Date
KR880701294A true KR880701294A (ko) 1988-07-26

Family

ID=25643112

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1019880700183A KR880701294A (ko) 1986-06-18 1987-06-05 높은 순도의 지르코늄 및 그의 제조방법

Country Status (11)

Country Link
EP (1) EP0270637B1 (ko)
JP (1) JPS63503536A (ko)
KR (1) KR880701294A (ko)
CN (1) CN87104300A (ko)
AT (1) ATE81677T1 (ko)
BR (1) BR8707354A (ko)
DE (1) DE3782319T2 (ko)
DK (1) DK84988A (ko)
ES (1) ES2004306A6 (ko)
NZ (1) NZ220626A (ko)
WO (1) WO1987007915A1 (ko)

Families Citing this family (8)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
ATE216688T1 (de) * 1993-07-28 2002-05-15 Univ Monash Zirkoniumoxid partikel
CN1039805C (zh) * 1995-03-31 1998-09-16 广东工学院 锆英石制取电子级二氧化锆的方法
CA2439768A1 (en) * 2001-03-08 2002-09-19 Cms Enterprises Development, L.L.C. Method for recovering zirconium values from a hard rock ore containing zircon and uranium
BR112012005455B1 (pt) * 2009-09-11 2018-01-02 The South African Nuclear Energy Corporation Limited Processo para tratamento de carga de alimentação compreendendo um mineral e/ou um óxido de metal/silicato derivados de ou associados com um mineral
CN106082339B (zh) * 2014-12-05 2017-07-04 三祥新材股份有限公司 一种采用锆英砂制备得到高纯度电熔氧化锆的方法
MY186928A (en) * 2015-02-09 2021-08-26 Iluka Resources Ltd Process for improving the grade and optical quality of zircons
CN112553480A (zh) * 2020-10-10 2021-03-26 吕梁学院 一种赤泥中锆的回收方法
CN118026256A (zh) * 2024-02-26 2024-05-14 山东鸿远新材料科技股份有限公司 一种二氧化锆废料再生工艺

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US1502422A (en) * 1921-08-10 1924-07-22 Kemet Lab Co Inc Zirconium containing composition and process of making the same
US1530139A (en) * 1923-05-23 1925-03-17 Lindsay Light Company Art of manufacturing zirconium compounds
US1618286A (en) * 1925-04-22 1927-02-22 Titanium Alloy Mfg Co Zirconium compound and method of making same
FR1087816A (fr) * 1953-05-11 1955-03-01 Bozel Maletra Procédé de traitement de minerais de zirconium et ses applications
GB889791A (en) * 1957-04-18 1962-02-21 British Titan Products Treatment of zirconiferous materials
DE1261121B (de) * 1958-10-08 1968-02-15 Nat Lead Co Verfahren zur Herstellung von wasserloesliche Kieselsaeure enthaltendem Natriumzirkonylsulfat
FR1255548A (fr) * 1960-02-18 1961-03-10 Columbia Southern Chem Corp Procédé pour séparer le zirconium de la silice
US3811907A (en) * 1971-08-03 1974-05-21 Humphreys Corp Processing of silicate ores and product thereof
FR2469462A1 (fr) * 1979-11-09 1981-05-22 Rhone Poulenc Ind Procede de traitement d'un minerai complexe de titane, zirconium et terres rares
GB8419226D0 (en) * 1984-07-27 1984-08-30 Cookson Group Plc Extraction process
WO1986004614A1 (en) * 1985-02-01 1986-08-14 Commonwealth Scientific And Industrial Research Or Process for the production of high purity zirconia

Also Published As

Publication number Publication date
EP0270637B1 (en) 1992-10-21
EP0270637A1 (en) 1988-06-15
DK84988D0 (da) 1988-02-18
DE3782319T2 (de) 1993-02-25
CN87104300A (zh) 1987-12-30
WO1987007915A1 (en) 1987-12-30
BR8707354A (pt) 1988-09-13
NZ220626A (en) 1989-11-28
ATE81677T1 (de) 1992-11-15
ES2004306A6 (es) 1988-12-16
DK84988A (da) 1988-02-18
JPS63503536A (ja) 1988-12-22
DE3782319D1 (de) 1992-11-26
EP0270637A4 (en) 1988-11-22

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