KR870008901A - 건식 반응 공정 - Google Patents
건식 반응 공정 Download PDFInfo
- Publication number
- KR870008901A KR870008901A KR870002466A KR870002466A KR870008901A KR 870008901 A KR870008901 A KR 870008901A KR 870002466 A KR870002466 A KR 870002466A KR 870002466 A KR870002466 A KR 870002466A KR 870008901 A KR870008901 A KR 870008901A
- Authority
- KR
- South Korea
- Prior art keywords
- reaction zone
- active
- compound
- bronsted acid
- salt
- Prior art date
Links
- 238000006243 chemical reaction Methods 0.000 title claims 11
- 238000000034 method Methods 0.000 claims 13
- 150000001875 compounds Chemical class 0.000 claims 8
- 230000000361 pesticidal effect Effects 0.000 claims 7
- 239000007848 Bronsted acid Substances 0.000 claims 6
- 150000003839 salts Chemical class 0.000 claims 6
- 239000000575 pesticide Substances 0.000 claims 4
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims 2
- 239000002585 base Substances 0.000 claims 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims 2
- UKZAGFGNPPELKU-UHFFFAOYSA-N 1,2-dihydropyrazine-3,6-dione Chemical compound O=C1NCC(=O)N=C1 UKZAGFGNPPELKU-UHFFFAOYSA-N 0.000 claims 1
- OWZPCEFYPSAJFR-UHFFFAOYSA-N 2-(butan-2-yl)-4,6-dinitrophenol Chemical compound CCC(C)C1=CC([N+]([O-])=O)=CC([N+]([O-])=O)=C1O OWZPCEFYPSAJFR-UHFFFAOYSA-N 0.000 claims 1
- 239000003341 Bronsted base Substances 0.000 claims 1
- 239000002253 acid Substances 0.000 claims 1
- 150000008044 alkali metal hydroxides Chemical class 0.000 claims 1
- 229910001860 alkaline earth metal hydroxide Inorganic materials 0.000 claims 1
- 150000001412 amines Chemical class 0.000 claims 1
- 229910021529 ammonia Inorganic materials 0.000 claims 1
- 125000004122 cyclic group Chemical group 0.000 claims 1
- XDDAORKBJWWYJS-UHFFFAOYSA-N glyphosate Chemical compound OC(=O)CNCP(O)(O)=O XDDAORKBJWWYJS-UHFFFAOYSA-N 0.000 claims 1
- 229910010272 inorganic material Inorganic materials 0.000 claims 1
- 239000011147 inorganic material Substances 0.000 claims 1
- 125000001449 isopropyl group Chemical group [H]C([H])([H])C([H])(*)C([H])([H])[H] 0.000 claims 1
- JXTHEWSKYLZVJC-UHFFFAOYSA-N naptalam Chemical compound OC(=O)C1=CC=CC=C1C(=O)NC1=CC=CC2=CC=CC=C12 JXTHEWSKYLZVJC-UHFFFAOYSA-N 0.000 claims 1
- 238000010008 shearing Methods 0.000 claims 1
- 239000007787 solid Substances 0.000 claims 1
- 239000007790 solid phase Substances 0.000 claims 1
- 239000002904 solvent Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07F—ACYCLIC, CARBOCYCLIC OR HETEROCYCLIC COMPOUNDS CONTAINING ELEMENTS OTHER THAN CARBON, HYDROGEN, HALOGEN, OXYGEN, NITROGEN, SULFUR, SELENIUM OR TELLURIUM
- C07F9/00—Compounds containing elements of Groups 5 or 15 of the Periodic Table
- C07F9/02—Phosphorus compounds
- C07F9/28—Phosphorus compounds with one or more P—C bonds
- C07F9/38—Phosphonic acids [RP(=O)(OH)2]; Thiophosphonic acids ; [RP(=X1)(X2H)2(X1, X2 are each independently O, S or Se)]
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
- B01J19/0086—Processes carried out with a view to control or to change the pH-value; Applications of buffer salts; Neutralisation reactions
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
- A01N25/14—Powders or granules wettable
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J8/00—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes
- B01J8/0095—Chemical or physical processes in general, conducted in the presence of fluids and solid particles; Apparatus for such processes in which two different types of particles react with each other
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Chemical & Material Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Health & Medical Sciences (AREA)
- Organic Chemistry (AREA)
- Pest Control & Pesticides (AREA)
- Plant Pathology (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- Wood Science & Technology (AREA)
- Zoology (AREA)
- Environmental Sciences (AREA)
- Toxicology (AREA)
- Agronomy & Crop Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Biochemistry (AREA)
- Molecular Biology (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
내용없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (12)
- 활성 살충염을 형성하는 브뢴스테드 산과 이에 대조되는 브뢴스테드 염기를 반응대역의 한쪽 끝에서 투입하고 ; 이 화합물을 상기 반응대역에 통과시키며 ; 반응 조건이 조절된 상기 반응대역에서 높은 전단하 조화합물을 고르게 혼합하고 ; 다음에 반응대역의 다른 한쪽 끝으로부터 고체상의 활성 살충염을 취출해내는 단계로 구성된 활성 살충염의 연속 제도방법.
- 제1항에 있어서, 환성 살충염을 형성하는 브뢴스테드산이 고체상으로 반응대역에 투입되고, 브뢴스테드 염기는 50중량% 이하의 용매와 함께 투입되는 방법.
- 제1항에 있어서, 반응대역에서 취출되는 활성살충염의 잔류 수분이 15% 이하인 방법.
- 제1항에 있어서, 반응열의 최소한 일부를 흡수하기 위해 불활성인 무기물질을 반응대역에서 화합물에 혼합해 줌을 특징으로 하는 방법.
- 제1항에 있어서, 반응이 진행되는 방법 반응대역으로부터 수증기를 회수함을 특징으로 하는 방법.
- 제1항에서 있어서, 상기 활성 살충염이 수용성인 방법.
- 제1항에 있어서, 상기 브뢴스테드 염기가 알카리금속 수산화물, 알카리토금속 수산화물, 암모니아 또는 유기 아민인 방법.
- 제1항에 있어서, 활성 살충 화합물의 브뢴스테드 산이 N-1-나프틸프탈람 산인 방법.
- 제1항에 있어서, 활성 살충 화합물의 브뢴스테드 산이 N-(포스포노메틸)글리신인 방법.
- 제1항에 있어서, 활성 살충 화합물의 브뢴스테드 산이 3-(1-메틸에틸)-1H-2,1,3-벤로티아디아진-4(3H)-은 2,2-디옥시드인 방법.
- 제1항에 있어서, 활성 살충 화합물의 브뢴스테드 산이 2-(1-메틸프로필)-4,6-디니트로페놀인 방법.
- 제1항에 있어서, 활성 살충 화합물의 브뢴스테드 산이 1,2-디히드로피리나진-3,6-디온인 방법.※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
US84190486A | 1986-03-20 | 1986-03-20 | |
US841,904 | 1986-03-20 | ||
US06/841904 | 1986-03-20 |
Publications (2)
Publication Number | Publication Date |
---|---|
KR870008901A true KR870008901A (ko) | 1987-10-22 |
KR910007349B1 KR910007349B1 (ko) | 1991-09-25 |
Family
ID=25285999
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
KR1019870002466A KR910007349B1 (ko) | 1986-03-20 | 1987-03-18 | 건식 반응 공정 |
Country Status (14)
Country | Link |
---|---|
EP (1) | EP0238240B2 (ko) |
JP (1) | JPS62230701A (ko) |
KR (1) | KR910007349B1 (ko) |
AR (1) | AR243150A1 (ko) |
AT (1) | ATE93361T1 (ko) |
AU (1) | AU602137B2 (ko) |
BR (1) | BR8701100A (ko) |
CA (1) | CA1297696C (ko) |
DE (1) | DE3787107T3 (ko) |
ES (1) | ES2058106T5 (ko) |
FI (1) | FI89666C (ko) |
GR (1) | GR3024401T3 (ko) |
IL (1) | IL81919A (ko) |
ZA (1) | ZA871571B (ko) |
Families Citing this family (10)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
BR8600460A (pt) * | 1986-02-04 | 1987-09-01 | Monsanto Brasil | Processo para preparacao de um sal de metal alcalino particulado de n-fosfonometilglicina |
GB8909380D0 (en) * | 1989-04-25 | 1989-06-14 | Marks A H & Co Ltd | Water soluble pesticide solution |
US5633397A (en) * | 1995-06-07 | 1997-05-27 | Monsanto Company | Preparation of ammonium glyphosate via a gas-solid reaction system |
US5614468A (en) * | 1995-06-07 | 1997-03-25 | Monsanto Company | Preparation of ammonium glyphosate using aqueous ammonium hydroxide in a liquid-solid reaction system |
DE19624607A1 (de) * | 1996-06-20 | 1998-01-02 | Basf Ag | Verfahren zur Herstellung von Salzen von Säuregruppen tragenden pharmazeutischen Wirkstoffen |
US6218337B1 (en) * | 1996-09-27 | 2001-04-17 | Basf Aktiengesellschaft | Solid mixtures of 3-isopropyl-2,1,3-benzothiadiazin-4-one-2,2,-dioxide or its salts |
DE60014389T2 (de) * | 1999-07-28 | 2005-10-06 | Monsanto Technology Llc | Verfahren zur herstellung einer nachhaltig verarbeitbaren ammonium glyphosat paste |
US6734142B2 (en) | 2001-04-23 | 2004-05-11 | Monsanto Technology Llc | Ammonium glyphosate compositions and process for their preparation |
CN100531573C (zh) | 2002-08-31 | 2009-08-26 | 孟山都技术公司 | 含有二羧酸组分的干燥农药组合物的制备方法 |
WO2018111459A1 (en) * | 2016-12-14 | 2018-06-21 | Dow Global Technologies Llc | Method for generating salts of pharmaceutical active ingredients |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
FR1488369A (fr) * | 1966-06-01 | 1967-07-13 | Procédé de fabrication directe sous forme solide d'un sel alcalin d'un acide insoluble ou peu soluble | |
DE1642967A1 (de) * | 1967-03-25 | 1971-06-03 | Budenheim Rud A Oetker Chemie | Verfahren zur Herstellung fester Reaktionsprodukte durch Neutralisieren von fliessfaehigen sauren mit fliessfaehigen basischen Stoffen |
DE1906399C3 (de) * | 1969-02-08 | 1979-01-04 | Hoechst Ag, 6000 Frankfurt | Verfahren zur kontinuierlichen Herstellung von Dinatrium-m-Benzol· disulfonat |
BR8600460A (pt) * | 1986-02-04 | 1987-09-01 | Monsanto Brasil | Processo para preparacao de um sal de metal alcalino particulado de n-fosfonometilglicina |
-
1987
- 1987-03-04 ZA ZA871571A patent/ZA871571B/xx unknown
- 1987-03-09 AT AT87301990T patent/ATE93361T1/de not_active IP Right Cessation
- 1987-03-09 ES ES87301990T patent/ES2058106T5/es not_active Expired - Lifetime
- 1987-03-09 DE DE3787107T patent/DE3787107T3/de not_active Expired - Lifetime
- 1987-03-09 EP EP87301990A patent/EP0238240B2/en not_active Expired - Lifetime
- 1987-03-11 BR BR8701100A patent/BR8701100A/pt not_active IP Right Cessation
- 1987-03-17 IL IL81919A patent/IL81919A/xx not_active IP Right Cessation
- 1987-03-18 KR KR1019870002466A patent/KR910007349B1/ko not_active IP Right Cessation
- 1987-03-19 CA CA000532398A patent/CA1297696C/en not_active Expired - Lifetime
- 1987-03-19 AU AU70195/87A patent/AU602137B2/en not_active Expired
- 1987-03-19 JP JP62065513A patent/JPS62230701A/ja active Granted
- 1987-03-19 FI FI871213A patent/FI89666C/fi not_active IP Right Cessation
- 1987-03-20 AR AR87307071A patent/AR243150A1/es active
-
1997
- 1997-08-11 GR GR970402045T patent/GR3024401T3/el unknown
Also Published As
Publication number | Publication date |
---|---|
ES2058106T5 (es) | 1997-08-01 |
EP0238240B1 (en) | 1993-08-25 |
EP0238240B2 (en) | 1997-06-18 |
EP0238240A2 (en) | 1987-09-23 |
FI89666B (fi) | 1993-07-30 |
ATE93361T1 (de) | 1993-09-15 |
BR8701100A (pt) | 1987-12-29 |
AR243150A1 (es) | 1993-07-30 |
DE3787107T2 (de) | 1994-01-20 |
GR3024401T3 (en) | 1997-11-28 |
ES2058106T3 (es) | 1994-11-01 |
IL81919A (en) | 1991-06-10 |
AU602137B2 (en) | 1990-10-04 |
JPS62230701A (ja) | 1987-10-09 |
ZA871571B (en) | 1987-08-24 |
DE3787107D1 (de) | 1993-09-30 |
FI89666C (fi) | 1993-11-10 |
DE3787107T3 (de) | 1997-08-21 |
FI871213A0 (fi) | 1987-03-19 |
JPH041721B2 (ko) | 1992-01-14 |
IL81919A0 (en) | 1987-10-20 |
FI871213A (fi) | 1987-09-21 |
KR910007349B1 (ko) | 1991-09-25 |
EP0238240A3 (en) | 1990-02-07 |
AU7019587A (en) | 1987-09-24 |
CA1297696C (en) | 1992-03-24 |
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