KR840000512A - 벤조트리아졸의 제조방법 - Google Patents
벤조트리아졸의 제조방법 Download PDFInfo
- Publication number
- KR840000512A KR840000512A KR1019820002851A KR820002851A KR840000512A KR 840000512 A KR840000512 A KR 840000512A KR 1019820002851 A KR1019820002851 A KR 1019820002851A KR 820002851 A KR820002851 A KR 820002851A KR 840000512 A KR840000512 A KR 840000512A
- Authority
- KR
- South Korea
- Prior art keywords
- acid ester
- formula
- compound
- sulfuric acid
- sulfonic acid
- Prior art date
Links
- 238000000034 method Methods 0.000 title claims 3
- QRUDEWIWKLJBPS-UHFFFAOYSA-N benzotriazole Chemical compound C1=CC=C2N[N][N]C2=C1 QRUDEWIWKLJBPS-UHFFFAOYSA-N 0.000 title 1
- 239000012964 benzotriazole Substances 0.000 title 1
- 150000001875 compounds Chemical class 0.000 claims 3
- 150000003459 sulfonic acid esters Chemical class 0.000 claims 3
- QAOWNCQODCNURD-UHFFFAOYSA-N sulfuric acid Substances OS(O)(=O)=O QAOWNCQODCNURD-UHFFFAOYSA-N 0.000 claims 3
- -1 sulfuric acid ester Chemical class 0.000 claims 3
- 239000003054 catalyst Substances 0.000 claims 2
- 125000003903 2-propenyl group Chemical group [H]C([*])([H])C([H])=C([H])[H] 0.000 claims 1
- ZAMOUSCENKQFHK-UHFFFAOYSA-N Chlorine atom Chemical group [Cl] ZAMOUSCENKQFHK-UHFFFAOYSA-N 0.000 claims 1
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims 1
- 125000000217 alkyl group Chemical group 0.000 claims 1
- 125000004432 carbon atom Chemical group C* 0.000 claims 1
- 230000003197 catalytic effect Effects 0.000 claims 1
- 239000007795 chemical reaction product Substances 0.000 claims 1
- 239000000460 chlorine Chemical group 0.000 claims 1
- 229910052801 chlorine Chemical group 0.000 claims 1
- VAYGXNSJCAHWJZ-UHFFFAOYSA-N dimethyl sulfate Chemical group COS(=O)(=O)OC VAYGXNSJCAHWJZ-UHFFFAOYSA-N 0.000 claims 1
- 238000010438 heat treatment Methods 0.000 claims 1
- 229910052739 hydrogen Inorganic materials 0.000 claims 1
- 239000001257 hydrogen Substances 0.000 claims 1
- 125000004435 hydrogen atom Chemical group [H]* 0.000 claims 1
- 239000012442 inert solvent Substances 0.000 claims 1
- VUQUOGPMUUJORT-UHFFFAOYSA-N methyl 4-methylbenzenesulfonate Chemical compound COS(=O)(=O)C1=CC=C(C)C=C1 VUQUOGPMUUJORT-UHFFFAOYSA-N 0.000 claims 1
- 239000003444 phase transfer catalyst Substances 0.000 claims 1
- 239000007858 starting material Substances 0.000 claims 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D249/00—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms
- C07D249/16—Heterocyclic compounds containing five-membered rings having three nitrogen atoms as the only ring hetero atoms condensed with carbocyclic rings or ring systems
- C07D249/18—Benzotriazoles
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N43/00—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds
- A01N43/64—Biocides, pest repellants or attractants, or plant growth regulators containing heterocyclic compounds having rings with three nitrogen atoms as the only ring hetero atoms
- A01N43/647—Triazoles; Hydrogenated triazoles
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Life Sciences & Earth Sciences (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Plant Pathology (AREA)
- Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Dentistry (AREA)
- General Health & Medical Sciences (AREA)
- Agronomy & Crop Science (AREA)
- Zoology (AREA)
- Pest Control & Pesticides (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
- Pharmaceuticals Containing Other Organic And Inorganic Compounds (AREA)
- Plural Heterocyclic Compounds (AREA)
- Nitrogen And Oxygen Or Sulfur-Condensed Heterocyclic Ring Systems (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
- Saccharide Compounds (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
- Preventing Corrosion Or Incrustation Of Metals (AREA)
- Nitrogen Condensed Heterocyclic Rings (AREA)
Abstract
내용 없음
Description
본 내용은 요부공개 건이므로 전문내용을 수록하지 않았음
Claims (7)
- a) 일반식(Ⅱa) 또는 (Ⅱb)의 화합물을 적당하게는 불활성 용매중에서 R그룹을 도입시키는데 적당한 황산 에스테르 또는 설폰산 에스테르와 함께 몇시간동안 가열하고 생성된 반응생성물을 분리하거나, b) 일반식(Ⅲ)의 화합물을 촉매적량의 황산 에스테르 또는 설폰산에스테르나 통상의 상 전이촉매의 존재하에서 가열시킴을 특징으로 하여 일반식(Ⅰ)의 화합물을 제조하는 방법.
-
- 상기 식에서
- R은 탄소수 1 내지 4의 직쇄 또는 측쇄의 알킬그룹이거나 알릴이며, X는 수소 또는 염소이다.
- 제1항 b)에 있어서, 촉매로서 사용된 황산 에스테르 또는 설폰산에스테르가 일반식 ROH의 알콜(여기에서 R은 출발물질인 일반식(Ⅲ)에서 정의되는 바와 같다)로 부터 제조됨이 특징인 방법.
- 제1항에 있어서, 촉매가 디메틸설페이트 또는 메틸-p-톨루엔설포네이트임이 특징인 방법.
- ※ 참고사항 : 최초출원 내용에 의하여 공개하는 것임.
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19813125112 DE3125112A1 (de) | 1981-06-26 | 1981-06-26 | Neue benzotriazole, ihre herstellung und ihre verwendung als fungizide. |
| DEP3125112.9 | 1981-06-26 | ||
| DE3125112.9 | 1981-06-26 |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| KR840000512A true KR840000512A (ko) | 1984-02-22 |
| KR880001318B1 KR880001318B1 (ko) | 1988-07-23 |
Family
ID=6135422
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR8202851A KR880001318B1 (ko) | 1981-06-26 | 1982-06-25 | 벤조트리아졸의 제조방법 |
Country Status (13)
| Country | Link |
|---|---|
| EP (1) | EP0070384B1 (ko) |
| JP (1) | JPS584776A (ko) |
| KR (1) | KR880001318B1 (ko) |
| AT (1) | ATE10629T1 (ko) |
| AU (1) | AU551489B2 (ko) |
| BR (1) | BR8203716A (ko) |
| CA (1) | CA1169076A (ko) |
| DE (2) | DE3125112A1 (ko) |
| EG (1) | EG17841A (ko) |
| ES (2) | ES513424A0 (ko) |
| HU (1) | HU188579B (ko) |
| SU (1) | SU1153810A3 (ko) |
| ZA (1) | ZA824531B (ko) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100496924B1 (ko) * | 2002-03-29 | 2005-06-23 | 오세인 | 유압 프레싱 필름의 제조방법 |
Families Citing this family (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JPS5359737A (en) * | 1976-11-10 | 1978-05-29 | Onoda Cement Co Ltd | Electrostatic powder coating and its equipment |
| AU508457B2 (en) * | 1976-11-10 | 1980-03-20 | Onoda Cement Co. Ltd. | Electrostatic coating |
| JPH0639717B2 (ja) * | 1985-06-12 | 1994-05-25 | 大塚化学株式会社 | 家具、什器又は建具類の処理方法 |
| JPH01146176U (ko) * | 1988-03-31 | 1989-10-09 |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| DE2945689A1 (de) * | 1979-11-13 | 1981-06-04 | Bayer Ag, 5090 Leverkusen | Neue oxybenztriazolderivate, verfahren zu ihrer herstellung und ihre verwendung als synergisten in schaedlingsbekaempfungsmitteln |
-
1981
- 1981-06-26 DE DE19813125112 patent/DE3125112A1/de not_active Withdrawn
-
1982
- 1982-06-04 DE DE8282104913T patent/DE3261449D1/de not_active Expired
- 1982-06-04 EP EP82104913A patent/EP0070384B1/de not_active Expired
- 1982-06-04 AT AT82104913T patent/ATE10629T1/de not_active IP Right Cessation
- 1982-06-16 CA CA000405306A patent/CA1169076A/en not_active Expired
- 1982-06-21 SU SU823454839A patent/SU1153810A3/ru active
- 1982-06-25 ZA ZA824531A patent/ZA824531B/xx unknown
- 1982-06-25 BR BR8203716A patent/BR8203716A/pt unknown
- 1982-06-25 JP JP57110575A patent/JPS584776A/ja active Granted
- 1982-06-25 ES ES513424A patent/ES513424A0/es active Granted
- 1982-06-25 AU AU85360/82A patent/AU551489B2/en not_active Ceased
- 1982-06-25 HU HU822070A patent/HU188579B/hu unknown
- 1982-06-25 KR KR8202851A patent/KR880001318B1/ko active
- 1982-06-26 EG EG383/82A patent/EG17841A/xx active
- 1982-12-28 ES ES518607A patent/ES518607A0/es active Granted
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR100496924B1 (ko) * | 2002-03-29 | 2005-06-23 | 오세인 | 유압 프레싱 필름의 제조방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| JPH0360825B2 (ko) | 1991-09-17 |
| AU551489B2 (en) | 1986-05-01 |
| EP0070384A1 (de) | 1983-01-26 |
| ES8401480A1 (es) | 1983-12-16 |
| CA1169076A (en) | 1984-06-12 |
| ATE10629T1 (de) | 1984-12-15 |
| JPS584776A (ja) | 1983-01-11 |
| EP0070384B1 (de) | 1984-12-05 |
| ES513424A0 (es) | 1983-12-16 |
| DE3125112A1 (de) | 1983-01-13 |
| ES8402584A1 (es) | 1984-02-01 |
| KR880001318B1 (ko) | 1988-07-23 |
| EG17841A (en) | 1990-08-30 |
| SU1153810A3 (ru) | 1985-04-30 |
| ZA824531B (en) | 1984-02-29 |
| BR8203716A (pt) | 1983-06-21 |
| HU188579B (en) | 1986-04-28 |
| AU8536082A (en) | 1983-01-06 |
| ES518607A0 (es) | 1984-02-01 |
| DE3261449D1 (en) | 1985-01-17 |
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