KR20230060598A - Composition for mask pack comprising Water (and) Opuntia Humifusa Leaf Extract and manufacturing the same and mask pack using the same - Google Patents

Abstract

The present invention relates to a mask pack composition containing a water-soluble extract of the stem of Opuntia humifusa, a method for manufacturing the same, and a mask pack using the same. Cole, Niacinamide, 1,2-Hexanediol, PEG-32, Betaine, Castor Seed Oil, Xanthan Gum, Panthenol, PEG-60 Hydrogenated Castor Oil, Caprylyl Glycol, Raw Sweet Blueberry extract, tomato extract, grapefruit extract, green tea extract, ethylhexylglycerin, xylityl glucoside, adenosine, disodium EDTA, anhydroxylitol, xylitol, glucose, sodium hyaluronate, yam root extract, cheonnyeoncho including spices Provided is a composition for a mask pack containing a water-soluble extract of the stem.
According to the manufacturing method of cheonnyeoncho stem water-soluble extract according to the present invention, by adjusting the viscosity of cheonnyeoncho, extracting a large amount of active ingredients of cheonnyeoncho, and manufacturing a mask pack with a water-soluble extract of cheonnyeoncho stem, which has antioxidant and skin inflammation improvement effects, skin brightness It has the advantage of being able to easily use a mask pack that is effective for improving wrinkles, wrinkles and moisturizing.

Description

Composition for mask pack containing a water-soluble extract of Astragalus stem, method for manufacturing the same, and mask pack using the same

The present invention relates to a composition for a mask pack containing a water-soluble extract of the stem of cinnamon plant, a method for manufacturing the same, and a mask pack using the same, and more particularly, by adjusting the viscosity of cinnamon plant and extracting a large amount of active ingredients of cinnamon plant to provide antioxidant and skin protection. A mask pack composition containing a water-soluble extract of the stem of the millennium that can be easily used by various age groups effective in improving skin brightness, wrinkles, and moisturizing by manufacturing a mask pack with a water-soluble extract of the stem of the millennium obtained by processing the plant with the effect of improving inflammation , its manufacturing method and mask pack using the same.

Due to environmental changes, particulate matter is frequently generated. It has been reported that fine dust particles can reach pores, thereby stimulating the dermal layer of the skin to generate active oxygen, eventually causing serious problems in the skin, further aggravating atopic symptoms. In response to this, fine dust protection cosmetics are growing in popularity day by day. In addition, the use of functional mask packs and creams that supply moisture and nutrients to the skin in a sufficiently short time and whiten / improve wrinkles are increasing.

Existing cosmetics with a lot of oil are easy to adhere to fine dust and pollutants in the air, which can cause irritation, so mask packs with enhanced ingredients, fabrics, and moisturizing time are popular. In particular, mask packs can be used very easily by those in their 20s to 50s, and play a big role in exports. In particular, through mask packs, consumers expect moisturizing power, whitening, and anti-wrinkle efficacy.

Cheonnyeoncho (Opuntia humifusa) is a cactus family plant and is called Opuntioideae, Opuntia. It is a native cactus, and its shape resembles a palm, so it is also called a palm cactus. Stems, fruits, roots, and flowers, excluding the thorns, have excellent commercial value because they contain nutrients and pigments, and can be commercialized by taking advantage of each characteristic. In particular, Cheonnyeoncho contains various nutrients important to the human body, such as phenolic substances, flavonoids, dietary fiber, vitamin C, calcium, minerals and amino acids, complex polysaccharides, etc. Among them, dietary fiber and calcium are contained in a large amount compared to other plants. .

Studies related to Cheonnyeoncho have been conducted on the antioxidant effect of Cheonnyeoncho cactus, the antioxidant activity of the hot water extract of the stem of Cheonnyeoncho, the effect of preventing liver damage from carbon tetrachloride, the anti-atherosclerosis effect and the improvement of aerobic exercise capacity, the antibacterial activity of the stem and fruit extract of Cheonnyeoncho, and the effect on cancer cells and breast cancer cells. Growth inhibitory effects have been reported. However, pectin, a high-molecular dietary fiber, is the main component of the fruit of cheonnyeoncho, and has a viscosity composed of arabinose, galactose, xylose, galacturonic acid, and rhamnose. It is known as a high-quality food.

When water is added during extraction from the raw material or powder of Cheonnyeoncho, there is a problem of high viscosity such as injeolmi, and in order to avoid this, when simply boiling the raw material, mucous active ingredients such as pectin cannot be used properly. On the other hand, it is difficult to use the fruit itself as a food material due to its high viscosity, so it is mostly used as a dry powder. On the other hand, in order to solve the problem of high viscosity, a fermentation technology using radiation or enzymes has been introduced. The technique of lowering the viscosity through fermentation is complicated and expensive in the extraction process and formulation.

Korean Registered Patent Publication No. 1445776 Korean Patent Publication No. 2012-0010687 Korean Registered Patent Publication No. 2227915

An object of the present invention is to provide a composition for a mask pack containing a water-soluble extract of the stem of Azalea, which can solve the viscosity problem of Cheonnyeoncho, a manufacturing method thereof, and a mask pack using the same.

In addition, the present invention is to increase the utilization of the active ingredient of cheonnyeoncho by adjusting the viscosity of cheonnyeoncho extract, and to provide a mask pack composition containing a cheonnyeoncho stem water-soluble extract with increased skin permeability, a manufacturing method thereof, and a mask pack using the same to be

In order to achieve the above object, the present invention contains Opuntia humifusa stem water-soluble extract as an active ingredient, purified water, butylene glycol, niacinamide, 1,2-hexanediol, PEG-32, betaine, Castor Seed Oil, Xanthan Gum, Panthenol, PEG-60 Hydrogenated Castor Oil, Caprylyl Glycol, Raw Sweet Blueberry Extract, Tomato Extract, Grapefruit Extract, Green Tea Extract, Ethylhexylglycerin, Xylityl Glucoside, Adenosine, Disodium EDTA, anhydroxylitol, xylitol, glucose, sodium hyaluronate, yam root extract, provides a composition for mask pack containing a water-soluble extract of Azalea stem containing fragrance.

According to another embodiment of the present invention, washing and drying the stems of the washed cheonnyeoncho (Opuntia humifusa) and then pulverizing them into small pieces; Microwave treatment of the pulverized cheonnyeoncho; Cooling the microwave-irradiated pulverized Cheonnyeoncho at room temperature and performing secondary pulverization; Mixing distilled water with the secondly crushed millennium millennium millet and centrifuging to prepare a millennium millet extract; And freeze-drying the cheonnyeoncho extract to prepare a cheonnyeoncho powder; It provides a method for producing a composition for a mask pack containing an extract of Cheonnyeoncho comprising a.

The present invention provides a mask pack containing the Cheonnyeoncho extract.

According to the manufacturing method of cheonnyeoncho stem water-soluble extract according to the present invention, the viscosity of cheonnyeoncho is adjusted, a large amount of active ingredients of cheonnyeoncho are extracted, and cheonnyeoncho, which has antioxidant and skin inflammation improvement effects, has the advantage of being able to be used by processing into cosmetics. there is.

In addition, there is an advantage that a mask pack effective in improving skin brightness, wrinkles, and moisturizing can be easily used in various age groups by preparing a mask pack with a water-soluble extract of the stem of perennial plant according to the present invention.

1 is a graph showing the results of toxicity evaluation on cells of the Cheonnyeoncho extract according to the present invention in HaCaT cells.
Figure 2 is a graph showing the anthropometric results of the skin brightness of the Cheonnyeoncho extract according to the present invention.
Figure 3 is a graph showing the skin brightness improvement rate of the test group of the Cheonnyeoncho extract according to the present invention,
Figure 4 is a graph showing the control skin brightness measurement results of the Cheonnyeoncho extract according to the present invention,
Figure 5 is a graph showing the control skin brightness improvement rate of the Cheonnyeoncho extract according to the present invention,
Figure 6 is a graph comparing the change in skin brightness of the Cheonnyeoncho extract according to the present invention,
7 is a graph showing the results of measuring the wrinkle roughness of the test group of the Cheonnyeoncho extract according to the present invention;
Figure 8 is a graph showing the improvement rate of the roughness of wrinkles around the eyes of the test group of the Cheonnyeoncho extract according to the present invention,
9 is a graph showing the results of measuring the roughness of wrinkles around the eyes of the control group of the Cheonnyeoncho extract according to the present invention;
10 is a graph showing the improvement rate of wrinkle roughness in the control group of the Cheonnyeoncho extract according to the present invention;
11 is a graph comparing the change in roughness of wrinkles around the eyes of the Cheonnyeoncho extract according to the present invention;
Figure 12 is a graph showing the skin moisturizing measurement results of the Cheonnyeoncho extract according to the present invention,
13 is a graph showing the skin moisturizing improvement rate of the Cheonnyeoncho extract according to the present invention.

It should be noted that in the following description, only parts necessary for understanding the embodiments of the present invention are described, and descriptions of other parts will be omitted without disturbing the gist of the present invention.

The terms or words used in this specification and claims described below should not be construed as being limited to ordinary or dictionary meanings, and the inventors have appropriately used the concept of terms to describe their inventions in the best way. It should be interpreted as a meaning and concept consistent with the technical spirit of the present invention based on the principle that it can be defined in the following way. Therefore, the embodiments described in this specification and the configurations shown in the drawings are only preferred embodiments of the present invention, and do not represent all of the technical spirit of the present invention, so various equivalents that can replace them at the time of the present application. It should be understood that there may be variations and variations.

The present invention relates to a composition for a mask pack containing a water-soluble extract of the stem of Azalea, a manufacturing method thereof, and a mask pack using the same.

Cheonnyeoncho (Opuntiahumifusa, Eastern prickly pear) is a cactus that can overwinter in the inland among Opuntia sp cacti native to Korea, and is distinguished from Baeknyeoncho, a cactus native to Jeju Island. The cheonnyeoncho is also called a palm cactus because the shape of the stem is similar to that of the palm. Cheonnyeoncho is a fleshy perennial plant, that is, a perennial flowering plant, and its stem is fleshy like a common cactus, and has several segments that are constricted like nodes. They are also classified according to their shape. The tibia has a tracheid duct, a vascular bundle near the epidermis, and the leaves on the new shoot are needle-like and fall off after they are fully grown as flesh. Cotyledons are lanceolate or triangular, and have the same flesh, with different perianths and bracts. In general, it is known that the cheonnyeoncho can reduce its own moisture to less than half, can overwinter without freezing even at minus 20 ° C, and can maintain vitality. Research on cheonnyeoncho has been conducted mainly on stems and fruits, especially stems, and as a result of these studies, cheonnyeoncho pulp and stems are sold as food.

The Cheonnyeoncho may preferably use the leaves, stems, fruits, and roots of Cheonnyeoncho, and the present invention uses the stem of Cheonnyeoncho.

The mask pack composition according to the present invention contains the water-soluble extract of Opuntia humifusa stem as an active ingredient, purified water, butylene glycol, niacinamide, 1,2-hexanediol, PEG-32, betaine, and castor bean. Seed Oil, Xanthan Gum, Panthenol, PEG-60 Hydrogenated Castor Oil, Caprylyl Glycol, Raw Sweet Blueberry Extract, Tomato Extract, Grapefruit Extract, Green Tea Extract, Ethylhexylglycerin, Xylityl Glucoside, Adenosine, Dai It contains sodium EDTA, anhydroxylitol, xylitol, glucose, sodium hyaluronate, yam root extract, and water-soluble extracts of the stems of Azaleas including spices.

The Cheonnyeoncho extract may be prepared according to a conventional method known in the art, that is, a conventional method for preparing a plant extract. For example, it may be prepared by methods such as cold extraction, warm extraction, thermal extraction, ultrasonic extraction, steam distillation, supercritical fluid extraction, subcritical fluid extraction, or microwave treatment. In order to carry out the extraction method, a conventional extractor, ultrasonic crusher, or fractionator may be used.

The content of the components is 1 to 10 parts by weight of the water-soluble extract of the stem of Azalea, 7 to 9 parts by weight of butylene glycol, 1 to 3 parts by weight of niacinamide, and 0.5 to 1.5 parts by weight of 1,2-hexanediol, based on a total of 100 parts by weight. , PEG-32 0.1 ~ 1.0 parts by weight, betaine 0.1 ~ 1.0 parts by weight, castor seed oil 0.1 ~ 0.5 parts by weight, xanthan gum 0.05 ~ 0.5 parts by weight, panthenol 0.05 ~ 0.5 parts by weight, PEG-60 Hydrogen Tied castor oil 0.05 ~ 0.5 parts by weight, caprylyl glycol 0.05 ~ 0.5 parts by weight, ethylhexylglycerin 0.001 ~ 0.1 parts by weight, xylityl glucoside 0.01 ~ 0.1 parts by weight, adenosine 0.01 ~ 0.1 parts by weight, disodium EDTA 0.01 ~ 0.1 parts by weight, anhydroxylitol 0.01 ~ 0.1 parts by weight, xylitol 0.01 ~ 0.1 parts by weight, glucose 0.001 ~ 0.01 parts by weight, sodium hyaluronate 0.0005 ~ 0.002 parts by weight, yam root extract 0.0005 ~ 0.002 parts by weight, flavoring 0.005 to 0.1 parts by weight and the remaining amount of purified water.

The composition for a mask pack containing the water-soluble extract of the stem of the millennium may further include 0.1 to 0.5 parts by weight of one or more natural extracts selected from the group consisting of low sweet blueberry extract, tomato extract, grapefruit extract, and green tea extract.

The composition containing the active ingredient of the present invention exhibits functions such as improving skin elasticity and anti-aging, and thus can be used in various cosmetics. The cosmetic composition of the present invention may contain one or more components selected from the group consisting of water-soluble vitamins, oil-soluble vitamins, high-molecular peptides, high-molecular polysaccharides, sphingolipids, and seaweed extracts.

Any water-soluble vitamin can be used as long as it can be formulated into cosmetics, but preferably vitamin B1, vitamin B2, vitamin B6, pyridoxine, pyridoxine hydrochloride, vitamin B12, pantothenic acid, nicotinic acid, nicotinic acid amide, folic acid, vitamin C, vitamin H, etc. salts (thiamin hydrochloride, sodium ascorbate, etc.) or derivatives (sodium ascorbic acid-2-phosphate, magnesium salt of ascorbic acid-2-phosphate, etc.) included Water-soluble vitamins can be obtained by conventional methods such as a microbial transformation method, a purification method from a microbial culture, an enzymatic method, or a chemical synthesis method.

Any useful vitamin may be used as long as it can be formulated into cosmetics, but preferably vitamin A, carotene, vitamin D2, vitamin D3, vitamin E (d1-alpha tocopherol, d-alpha tocopherol, d-alpha tocopherol), etc. are mentioned. , their derivatives (ascorbine palmitate, ascorbine stearate, ascorbine dipalmitate, dl-alpha tocopherol acetate, dl-alpha tocopherol nicotinate, vitamin E, DL-pantothenyl alcohol, D-pantothenyl alcohol, pantothenylethyl ether, etc.) and the like are also included in the useful vitamins used in the present invention. The useful vitamins can be obtained by conventional methods such as microbial transformation, purification from microbial culture, enzymatic or chemical synthesis.

Any polymeric peptide may be used as long as it can be formulated into cosmetics, but preferably collagen, hydrolyzed collagen, gelatin, elastin, hydrolyzed elastin, keratin and the like are mentioned. Polymer peptides can be purified and obtained by conventional methods such as a purification method from a culture medium of microorganisms, an enzyme method, or a chemical synthesis method, or can be used after being purified from natural products such as pig or cow dermis or silkworm silk fibers.

Any polymeric polysaccharide may be used as long as it can be incorporated into cosmetics, but hydroxyethyl cellulose, xanthan gum, sodium hyaluronate, chondroitin sulfate or a salt thereof (sodium salt or the like) is preferable. For example, chondroitin sulfate or a salt thereof can be used after being purified from mammals or fish.

In addition to the above essential components, the cosmetic composition of the present invention may contain other ingredients normally formulated in cosmetic products, if necessary. Other ingredients that may be added include fats and oils, humectants, emollients, surfactants, organic and inorganic pigments, organic powders, ultraviolet absorbers, preservatives, bactericides, antioxidants, plant extracts, pH adjusters, alcohols, pigments, fragrances, A blood circulation accelerator, a cooling agent, an antiperspirant, purified water, etc. are mentioned. Examples of the oil and fat component include ester oils, hydrocarbon oils, silicone oils, fluorine oils, animal fats and vegetable oils.

As ester-based fats and oils, triglyceryl 2-ethylhexanoate, cetyl 2-ethylhexanoate, isopropyl myristate, butyl myristate, isopropyl palmitate, ethyl stearate, octyl palmitate, isostearate isocetyl, stearic acid Butyl, ethyl linoleate, isopropyl linoleate, ethyl oleate, isocetyl myristate, isostearyl myristate, isostearyl palmitate, octyldodecyl myristate, isocetyl isostearate, diethyl sebacate, adipine Diisopropyl acid, isoalkyl neopentanoate, tri(capryl, capric acid) glyceryl, trimethylolpropane tri2-ethylhexanoate, trimethylolpropane triisostearate, pentaelislitol tetra2-ethylhexanoate , Cetyl caprylate, decyl laurate, hexyl laurate, decyl myristate, myristyl myristate, cetyl myristate, stearyl stearate, decyl oleate, cetyl ricinooleate, isostea laurate Lil, isotridecyl myristate, isocetyl palmitate, octyl stearate, isocetyl stearate, isocetyl oleate, octyldodecyl oleate, octyldodecyl linoleate, isopropyl isostearate, 2-ethylhexanoate Aryl, 2-ethyl stearyl hexanoate, hexyl isostearate, ethylene glycol dioctanoate, ethylene glycol dioleate, propylene glycol dicaprate, di(caprylic, capric acid) propylene glycol, propylene glycol dicaprylate, dicap Neopentyl glycol prinate, neopentyl glycol dioctanoate, glyceryl tricaprylate, glyceryl triundecylate, glyceryl triisopalmitate, glyceryl triisostearate, octyldodecyl neopentanoate, isostea octanoate Lil, octyl isononanoate, hexyldecyl neodecanoate, octyldodecyl neodecanoate, isocetyl isostearate, isostearyl isostearate, octyldecyl isostearate, polyglycerin oleate, polyglycerin isostearate , triisocetyl citrate, triisoalkyl citrate, triisooctyl citrate, lauryl lactate, myristyl lactate, cetyl lactate, octyldecyl lactate, triethyl citrate, acetyl triethyl citrate, acetyl tributyl citrate, trioctyl citrate, horse Diisostearyl acid, 2-ethylhexyl hydroxystearate, di2-ethylhexyl succinate, diisobutyl adipate, diisopropyl sebacate, dioctyl sebacate, cholesteryl stearate, cholesteryl isostearate , cholesteryl hydroxystearate, cholesteryl oleate, dihydrocholesteryl oleate, phyteryl isostearate, physteryl oleate, 12-stealoylisocetyl hydroxystearate, 12-stealo and esters such as stearyl ylhydroxystearate and isostearyl 12-stealoylhydroxystearate.

Animal or vegetable oils include avocado oil, almond oil, olive oil, sesame oil, rice bran oil, birdflower oil, soybean oil, corn oil, rapeseed oil, algae oil, palm kernel oil, palm oil, castor oil, sunflower oil, grape seed oil , cottonseed oil, palm oil, kukui nut oil, wheat germ oil, rice germ oil, shea butter, moonshine colostrum, marker damian nut oil, meadowsweet oil, egg yolk oil, beef tallow, horse oil, mink oil, orange raffia oil, jojoba oil , animal or plant fats and oils such as candelilla wax, carnaba wax, liquid lanolin, and hydrogenated castor oil.

Examples of the moisturizer include water-soluble low-molecular moisturizers, fat-soluble molecular moisturizers, water-soluble polymers, and oil-soluble polymers.

Examples of water-soluble low-molecular moisturizers include serine, glutamine, sorbitol, mannitol, pyrrolidone-sodium carboxylate, glycerin, propylene glycol, 1,3-butylene glycol, ethylene glycol, polyethylene glycol B (polymerization degree n = 2 or more), polypropylene Glycol (polymerization degree n = 2 or more), polyglycerol B (polymerization degree n = 2 or more), lactic acid, lactate, etc. are mentioned.

Cholesterol, cholesterol ester, etc. are mentioned as a fat-soluble low-molecular moisturizer.

Examples of water-soluble polymers include carboxyvinyl polymer, polyaspartate, tragacanth, xanthan gum, methyl cellulose, hydroxymethyl cellulose, hydroxyethyl cellulose, hydroxypropyl cellulose, carboxymethyl cellulose, water-soluble chitin, chitosan, dextrin, and the like. can

Examples of the fat-soluble polymers include polyvinylpyrrolidone and eicosene copolymers, polyvinylpyrrolidone and hexadecene copolymers, nitrocellulose, dextrin fatty acid esters, and high-molecular silicones. Examples of the emollient agent include long-chain acyl glutamic acid cholesteryl ester, hydroxystearic acid cholesteryl, 12-hydroxystearic acid, stearic acid, rosin acid, and lanolin fatty acid cholesteryl ester.

Examples of the surfactant include nonionic surfactants, anionic surfactants, cationic surfactants, and amphoteric surfactants.

Nonionic surfactants include self-emulsifying glycerin monostearate, propylene glycol fatty acid esters, glycerin fatty acid esters, polyglycerin fatty acid esters, sorbitan fatty acid esters, POE (polyoxyethylene) sorbitan fatty acid esters, POE sorbitan fatty acid esters, POE Glycerin fatty acid ester, POE alkyl ether, POE fatty acid ester, POE hydrogenated castor oil, POE castor oil, POE and POP (polyoxyethylene and polyoxypropylene) copolymer, POE and POP alkyl ether, polyether modified silicone, lauric acid alkanolamides, alkylamine oxides, hydrogenated soybean phospholipids, and the like.

Anionic surfactants include fatty acid soaps, alpha-acyl sulfonates, alkyl sulfonates, alkyl allyl sulfonates, alkyl naphthalene sulfonates, alkyl sulfates, POE alkyl ether sulfates, alkyl amide sulfates, alkyl phosphates, POE alkyl phosphates, alkyl amides. Phosphates, alkyloylalkyl taurine salts, N-acylamino acid salts, POE alkyl ether carboxylates, alkyl sulfosuccinates, sodium alkyl sulfoacetates, acylated hydrolyzed collagen peptide salts, perfluoroalkyl phosphate esters, and the like. there is.

As the cationic surfactant, alkyltrimethylammonium chloride, stearyltrimethylammonium chloride, stearyltrimethylammonium bromide, cetostearyltrimethylammonium chloride, distearyldimethylammonium chloride, stearyldimethylbenzylammonium chloride, behenyltrimethylammonium bromide, chloride Benzalkonium, diethylaminoethyl stearate, dimethylaminopropyl stearate, quaternary ammonium salts of lanolin derivatives, and the like. Amphoteric surfactants include carboxybetaine type, amidebetaine type, sulfobetaine type, hydroxysulfobetaine type, amide sulfobetaine type, phosphobetaine type, aminocarboxylate type, imidazoline derivative type, amideamine type, etc. An amphoteric surfactant etc. are mentioned.

As organic and inorganic pigments, silicic acid, silicic anhydride, magnesium silicate, talc, sericite, mica, kaolin, bengala, clay, bentonite, titanium-coated mica, bismuth oxychloride, zirconium oxide, magnesium oxide, zinc oxide, titanium oxide, aluminum oxide inorganic pigments such as calcium sulfate, barium sulfate, magnesium sulfate, calcium carbonate, magnesium carbonate, iron oxide, ultramarine blue, chromium oxide, chromium hydroxide, calamine and complexes thereof; polyamide, polyester, polypropylene, polystyrene, polyurethane, vinyl resin, urea resin, phenolic resin, fluororesin, silicon resin, acrylic resin, melamine resin, epoxy resin, polycarbonate resin, divinylbenzene and styrene copolymers, organic pigments such as silk powder, cellulose, CI pigment yellow and CI pigment orange, and composite pigments of these inorganic pigments and organic pigments.

Examples of the organic powder include metal soaps such as calcium stearate; Alkyl phosphate metal salts, such as zinc sodium cetylrate, zinc laurylate, and calcium laurylate; polyvalent metal salts of acyl amino acids such as N-lauroyl-beta-alanine calcium, N-lauroyl-beta-alanine zinc, and N-lauroyl glycine calcium; polyvalent metal salts of amide sulfonic acids such as N-lauroyl-taurine calcium and N-palmitoyl-taurine calcium; N-epsilon-lauroyl-L-lysine, N-epsilon-palmitoylizine, N-alpha-paritoylolnithine, N-alpha-lauroylarginine, N-alpha-hardened beef fatty acid acylarginine, etc. -acyl basic amino acids; N-acyl polypeptides such as N-lauroyl glycyl glycine; alpha-amino fatty acids such as alpha-aminocaprylic acid and alpha-aminolauric acid; polyethylene, polypropylene, nylon, polymethyl methacrylate, polystyrene, divinylbenzene and styrene copolymers, tetrafluoroethylene, and the like.

Examples of UV absorbers include para-aminobenzoic acid, ethyl para-aminobenzoate, amyl para-aminobenzoate, octyl para-aminobenzoate, ethylene glycol salicylate, phenyl salicylate, octyl salicylate, benzyl salicylate, butylphenyl salicylate, homomenthyl salicylate, and benzyl cinnamate. , paramethoxycinnamic acid-2-ethoxyethyl, paramethoxycinnamic acid octyl, diparamethoxycinnamic acid mono-2-ethylhexane glyceryl, paramethoxycinnamic acid isopropyl, diisopropyl and diisopropylcinnamic acid ester mixture, Urocanic acid, ethyl urocanate, hydroxymethoxybenzophenone, hydroxymethoxybenzophenonesulfonic acid and its salts, dihydroxymethoxybenzophenone, dihydroxymethoxybenzophenone disulfonic acid sodium, dihydroxybenzoate Phenone, tetrahydroxybenzophenone, 4-tert-butyl-4'-methoxydibenzoylmethane, 2,4,6-trianilino-p-(carbo-2'-ethylhexyl-1'-oxy)- 1,3,5-triazine, 2-(2-hydroxy-5-methylphenyl)benzotriazole, etc. are mentioned.

Bactericides include hinokitiol, triclosan, trichlorohydroxydiphenyl ether, chlorhexidine gluconate, phenoxyethanol, resorcin, isopropylmethylphenol, azulene, salicylic acid, zincophylthione, benzalkonium chloride, photosensitizer So No. 301, mononitroguacol sodium, undecyrenic acid, etc. are mentioned.

Examples of antioxidants include butylhydroxyanisole, propyl gallic acid, and elisorbic acid.

Examples of the pH adjuster include citric acid, sodium citrate, malic acid, sodium malate, fumaric acid, sodium fumalate, succinic acid, sodium succinate, sodium hydroxide, and sodium monohydrogenphosphate.

Examples of alcohol include higher alcohols such as cetyl alcohol.

In addition, the blending components that may be added other than these are not limited thereto, and any of the above components can be blended within a range not impairing the objects and effects of the present invention.

The cosmetic composition of the present invention may take the form of a solution, emulsion, viscous mixture or the like.

Ingredients included in the cosmetic composition of the present invention may include ingredients commonly used in cosmetic compositions as active ingredients, for example, stabilizers, solubilizers, conventional adjuvants and carriers such as vitamins, pigments and flavors. include

The cosmetic composition of the present invention may be prepared in any formulation conventionally prepared in the art, and examples thereof include emulsion, cream, lotion, pack, foundation, lotion, beauty essence, hair cosmetics, and the like.

The cosmetic composition according to the present invention includes an extract of Cheonnyeoncho as an active ingredient, and may additionally include functional substances for antioxidant activity and skin inflammation improvement, or materials such as excipients and diluents for improving physical properties. The functional material or material for improving physical properties may be added within the range of maintaining the effect of the present invention. More specifically, the cosmetic composition according to the present invention is a spray, soap, cleansing foam, cleansing lotion, cleansing cream, body lotion, body cleanser, skin lotion, skin softener, skin toner, lotion, milk lotion, moisture lotion, nutrient lotion, massage It may include formulations of cream, nutrient cream, moisture cream, hand cream, foundation, essence, nutrient essence, and pack.

For example, when the formulation of the present invention is a spray or powder, lactose, talc, silica, aluminum hydroxide, calcium silicate or polyamide powder may be used as a carrier component. In particular, when the formulation of the present invention is a spray It may additionally contain a propellant such as chlorofluorohydrocarbon, propane/butane or dimethyl ether.

When the formulation of the present invention is a solution or emulsion, a solvent, solvating agent, or emulsifying agent is used as a carrier component, such as water, ethanol, isopropanol, ethyl carbonate, ethyl acetate, benzyl alcohol, benzyl benzoate, 1,3 -It may be a fatty acid ester of butyl glycol oil, glycerol aliphatic ester, polyethylene glycol or sorbitan.

Specifically, the cosmetic composition of the present invention is skin lotion, skin softener, skin toner, milk lotion, astringent, lotion, moisture lotion, nutrient lotion, massage cream, nutrient cream, moisture cream, hand cream, foundation, essence, nutrient essence, It includes packs, soaps, cleansing foams, cleansing lotions, cleansing creams, hair lotions, hair tonics, hair essences, hair shampoos, hair rinses, hair treatments, body lotions and body cleansers.

A functional cosmetic composition with antioxidant activity and skin cell regeneration ability, containing as an active ingredient the ethyl acetate fraction of the methanol extract of Opintia humifusa stems having antioxidant activity and skin fibroblast regeneration ability, the methanol extract of the stems of Opintia humifusa The ethyl acetate fraction used is remarkably superior in antioxidant activity and dermal fibroblast regeneration ability compared to those using other solvents or other parts, and thus has excellent antioxidant function. 1 is a graph showing the results of toxicity evaluation on cells of the Cheonnyeoncho extract according to the present invention in HaCaT cells. As shown in FIG. 1, it was confirmed that the survival rate was higher as well as the reduction in toxicity during the evaluation of cytotoxicity.

However, since it is not possible to improve the viscosity of cheonnyeoncho itself, it is possible to adjust the viscosity through nanoization by irradiating microwaves in order to extract the active ingredient through the stem extract of cheonnyeoncho and apply it to cosmetics. Through this, the delivery rate of the skin through the extraction of abundant active ingredients of cheonnyeoncho itself, formulation of cosmetics, and nanoparticles is improved.

Another embodiment of the present invention provides a mask pack containing the Cheonnyeoncho extract of the present invention.

This is the result of a human application test for skin brightness, wrinkles, and moisturizing improvement of the mask pack containing the water-soluble extract of the stem of perennial plant according to the present invention. The above test site was the face, and a human application test was conducted on 21 healthy adult men and women aged 20 to 60 years old.

First, skin brightness and wrinkles were evaluated before product use, after 4 weeks of product use, after 8 weeks of product use, and after 12 weeks of product use, respectively. Skin moisturizing was evaluated before and after product use. As a measuring method, the measuring devices were Corneometer (Courage+Khazaka electronic GmbH, Germany), Spectrophotomter (Konica Minolta), and PRIMOS CR (CANFIELD), and the measurement results and questionnaire evaluation results of the devices were analyzed.

Skin brightness was measured at the same location on the face using a spectrophotometer (CM-26D), and changes were compared and evaluated before product use, after 4 weeks of product use, after 8 weeks of product use, and after 12 weeks of product use. and the control group were compared and compared between groups. The improvement rate was calculated as follows.

*n: 4,8,12

It was analyzed using SPSSS statistics of the data solution, and the test results were subjected to statistical analysis after the normality test was performed. As a result of the analysis, when the significance probability p<0.05 in the 95% confidence interval, it was judged that there was an improvement effect by using the test product. did For statistical analysis, paired samples t-test was used when the parametric method was used, and Wilcoxon signed rank test was used when the non-parametric method was used. Independent samples t-test was used when the parametric method was used. In the case of using a non-parametric method, it was analyzed using the Mann-Whitney U test.

In the before-and-after comparison of skin brightness, the skin brightness (L*value) measurement results of the test group were 59.55 A.U. before product use, 60.22 A.U. after 4 weeks of product use, 59.94 A.U. after 8 weeks of product use, and 12 after product use, as shown in FIG. After a week, the measured value increased at a statistically significant level to 60.22 A.U., and as shown in Figure 3, the skin brightness improvement rate in the test group was 1.50% after 4 weeks of product use, 0.96% after 8 weeks of product use, and 0.96% after 8 weeks of product use, compared to before product use. After 12 weeks, an improvement rate of 1.39% was shown (p<0.05).

As a result of measuring skin brightness (L*value) of the control group, as shown in FIG. 4, 58.65 A.U. before product use, 59.86 A.U. after 4 weeks of product use, 58.70 A.U. after 8 weeks of product use, and 58.79 A.U. after 12 weeks of product use. The measured value increased at a statistically significant level only after 2 weeks (p<0.05), and as shown in Figure 5, the skin brightness improvement rate in the control group was 239% after 4 weeks of product use, 0.10% after 8 weeks of product use, compared to before product use. After 12 weeks of using the product, an improvement rate of 0.28% was shown.

In the comparison of skin brightness between the test group and the control group, the test group showed a statistically significant increase in skin brightness after 4 weeks of product use, 8 weeks of product use, and 12 weeks of product use compared to before product use (p <0.05), the control group showed a statistically significant increase in skin brightness only after 4 weeks of product use compared to before product use (p<0.05).

Figure 6 shows the comparison results of skin brightness change (Δ) after 12 weeks of product use compared to before product use in the test group and control group. As shown in FIG. 6, the change amount (Δ) of the test group was 082, and the change amount (Δ) of the control group was 016, showing a statistically significant difference (p<0.05).

Next, the results of the human application test of the roughness of wrinkles around the eyes are shown.

The roughness of the same location on the face was measured using Primos CR (CANFIELD), and the changes in roughness were compared and evaluated before product use, after 4 weeks of use, after 8 weeks of product use, and after 12 weeks of product use, and the test group and control group were compared. and compared between groups

The improvement rate was calculated as follows.

*n: 4,8,12

Comparing before and after use of the mask pack according to the present invention, as a result of measuring the wrinkle roughness (Ra) of the test group, as shown in Figure 7, 19.529 A.U. before product use, 18.465 A.U. after 4 weeks of product use, and 16.528 A.U. , After 12 weeks of product use, the measured value decreased to a statistically significant level after 8 weeks and 12 weeks of product use, with 16.342 A.U. after 12 weeks of product use. 3.02% after 8 weeks of product use, 13.20% after 8 weeks of product use, and 15.04% after 12 weeks of product use (p<0.05).

On the other hand, as a result of measuring the wrinkle roughness (Ra) of the control group in FIG. 9, 19.194 A.U. before product use, 18.6858 A.U. after 4 weeks of product use, 17.952 A.U. after 8 weeks of product use, and 17.11 A.U. after 12 weeks of product use, statistically significant after 12 weeks of product use. , the measured value decreased to a significant level, and looking at the improvement rate of the wrinkle roughness of the control group shown in FIG. 10, 1.38% after 4 weeks of product use, 4.29% after 8 weeks of product use, and 8.82% after 12 weeks of product use compared to before product use showed an improvement rate (p<0.05).

In the group comparison between the test group and the control group of the roughness of the wrinkles around the eyes, the test group showed a statistically significant reduction in the roughness of the wrinkles around the eyes after 8 weeks and 12 weeks of product use compared to before product use (p<0.05), The control group showed a statistically significant reduction in the roughness of wrinkles around the eyes only after 12 weeks of product use compared to before product use (p<0.05).

As a result of comparing the change in roughness (Δ) of the test group and the control group after using the product compared to before using the product, as shown in FIG. However, there was no statistical significance in the test group compared to the control group (p>0.05).

For skin moisturizing, the moisture content of the skin at the same location on the face was measured using a Corneometer, and the change in moisture content before and after product use was compared and evaluated.

The improvement rate was calculated as follows.

In the skin moisturizing improvement test, as a result of measuring the skin moisture content of the test group as a result of comparison before and after, as shown in FIG. 12, 35.1 A.U. before product use and 84.9 A.U. immediately after product use. The measured value increased at a statistically significant level, and the skin moisturizing improvement rate shown in FIG. 13 showed an improvement rate of 147.58% immediately after using the product compared to before using the product (p <0.05).

When viewed through the results of the human body application test, it was confirmed that the mask pack of the present invention helps improve skin brightness, wrinkles, and moisturizing.

Claims (3)

Contains the water-soluble extract of Opuntia humifusa stem as an active ingredient,
Purified water, butylene glycol, niacinamide, 1,2-hexanediol, PEG-32, betaine, castor seed oil, xanthan gum, panthenol, PEG-60 hydrogenated castor oil, caprylyl glycol , Raw sweet blueberry extract, tomato extract, grapefruit extract, green tea extract, ethylhexyl glycerin, xylityl glucoside, adenosine, disodium EDTA, anhydroxylitol, xylitol, glucose, sodium hyaluronate, yam root extract, containing spices
A composition for a mask pack containing a water-soluble extract of the stem of Azalea. Washing and drying the stems of the washed Opuntia humifusa and grinding them into small pieces;
Microwave treatment of the pulverized cheonnyeoncho;
Cooling the microwave-irradiated pulverized Cheonnyeoncho at room temperature and secondary pulverization;
Mixing distilled water with the pulverized Cheonnyeoncho and centrifuging to prepare an extract of Cheonnyeoncho; and
Freezing the cheonnyeoncho extract to prepare a cheonnyeoncho powder;
Method for producing a composition for a mask pack containing an extract of Cheonnyeoncho comprising a. A mask pack containing the Cheonnyeoncho extract according to claim 1.

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