KR20170107168A - Method of manufacturing natural soaps - Google Patents

Method of manufacturing natural soaps Download PDF

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Publication number
KR20170107168A
KR20170107168A KR1020160030743A KR20160030743A KR20170107168A KR 20170107168 A KR20170107168 A KR 20170107168A KR 1020160030743 A KR1020160030743 A KR 1020160030743A KR 20160030743 A KR20160030743 A KR 20160030743A KR 20170107168 A KR20170107168 A KR 20170107168A
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South Korea
Prior art keywords
weight
parts
oil
mixture
powder
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KR1020160030743A
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Korean (ko)
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KR101844313B1 (en
Inventor
안욱
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주식회사 아미니
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    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/22Organic compounds, e.g. vitamins
    • C11D9/38Products in which the composition is not well defined
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D13/00Making of soap or soap solutions in general; Apparatus therefor
    • C11D13/02Boiling soap; Refining
    • CCHEMISTRY; METALLURGY
    • C11ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11DDETERGENT COMPOSITIONS; USE OF SINGLE SUBSTANCES AS DETERGENTS; SOAP OR SOAP-MAKING; RESIN SOAPS; RECOVERY OF GLYCEROL
    • C11D9/00Compositions of detergents based essentially on soap
    • C11D9/04Compositions of detergents based essentially on soap containing compounding ingredients other than soaps
    • C11D9/44Perfumes; Colouring materials; Brightening agents ; Bleaching agents
    • C11D9/442Perfumes

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  • Chemical & Material Sciences (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • Detergent Compositions (AREA)

Abstract

The present invention relates to a method for manufacturing natural soaps, which comprises the following steps: (a) mixing 5 to 7 wt% of a Hippocampus coronatus extract and 1 to 1.2 wt% of Hylocereus Undatus extract with respect to 100 wt% of base oil, stirring the mixture for 30 to 60 minutes, and heating to the temperature of 45 to 55C; (b) adding separate 35 to 55 wt% of a caustic soda diluted solution cooled to the temperature of 40 to 45 C and stirring the mixture; (c) mixing 1 to 2 wt% of a grape seed powder, 1 to 3 wt% of a plum seed powder, 10 to 13 wt% of aroma oil and 3 to 5 wt% of beeswax, filling the mixture into a soap mold, and aging the mixture for 4 to 6 weeks in the shade at the temperature of 20 to 25C, wherein the natural soaps contain the Hippocampus coronatus extract and the Hylocereus Undatus extract to have an excellent moisturizing effect, and contains a bamboo charcoal powder, Firmiana simplex or yellow soil balls are selectively added thereto, thereby preventing discoloration, deterioration or decomposition of the natural soaps for a long period of time.

Description

Method of manufacturing natural soaps

The present invention relates to a process for producing a natural soap having a good moisturizing effect.

Korean Registered Patent No. 1128361 (registered on Mar. 13, 2012, entitled: Natural Soap Using Lactic Oils and Method for Producing the same) is a method for producing natural soap, Stem or root, and the mixture is heated to 80 to 100 ° C., cooled to 20 to 25 ° C., filtered using a filter paper having a pore size of 10 to 20 μm, and then filtered in a fermentation chamber for 2 to 4 days (A) preparing a vegetable concentrate by aging; 10 to 30 wt% of tea oil, 20 to 25 wt% of coconut oil, 5 to 10 wt% of palm oil, 5 to 50 wt% of olive pure, 5 to 10 wt% of rapeseed oil, 5 to 10 wt% (B) mixing 5 to 10% by weight of free radicals to prepare a vegetable oil; 3 to 15% by weight of the vegetable concentrate prepared above, 50 to 70% by weight of vegetable oil, 7 to 10% by weight of caustic soda and 20 to 25% by weight of water, C); And a saponification step (D) of cooling the mixed mixture to 20 to 25 占 폚.

Such prior arts claim that natural soaps can be prepared by containing tea leaves with excellent skin moisturizing effect and whitening effect, while the steps of producing a plant concentrate obtained by concentrating a large variety of wildflower or herbal mixture in one or more of them are complicated There is a problem that mass production is difficult.

Korean Patent No. 1128299 (registered on Mar. 13, 2012, entitled "Natural Soap Using the Solution of Aging Medicament and Method for Producing the Same") is a method for producing natural soap by adding caustic soda, 6 to 9% by weight of leaves, 4 to 6% by weight of lotus root, 4 to 6% by weight of red ginseng, 4 to 6% by weight of vitamin tree leaves and stems, 4 to 6% by weight persimmon leaves, 4 to 6% 3 to 5 wt% of rosemary, 6 to 9 wt% of black beans, 3 to 5 wt% of black sesame, 5 to 8 wt% of aloe, 5 to 8 wt% of mulberry leaves, 1 to 3 wt% Containing 3 to 5% by weight of green tea, 5 to 8% by weight of pine needles, 4 to 6% by weight of mint, 4 to 6% by weight of sewage, 3 to 5% by weight of blueberry, and 3 to 5% Water washing and aging at 65 to 95 ° C for 3 to 15 days depending on the material (S100); The step (S200) of adding 15 to 25% by weight of the seasoned aged herbal medicines to distilled water or 75 to 85% by weight of boiled water in boiling water, boiling them with high heat, and firing them for about 48 to 72 hours for about 48 hours; Adding the distilled water or soft drink to 37 to 43% by weight of the fermented hot water, boiling it with high heat, and boiling it for 3 to 4 hours to prepare a refill (S300); (S 400) of mixing 7.5 to 8.5% by weight of herbal medicine with hot water for 24 to 36 hours after mixing the hot water and the remainder after removing the re-mixed herbal medicine; (S500) mixing 65 to 75% by weight of the crude drug solution with 25 to 35% by weight of caustic soda and cooling to 40 to 55 캜; 65 to 75% by weight of a mixed carrier oil including at least two of coconut oil palm oil, olive oil, camellia oil, castor oil bran oil, sunflower oil and grapeseed oil is heated to 40 to 55 캜, (S600) stirring the mixture while slowly adding 25 to 35% by weight of the crude drug-mixing bath mixture to the mixture; Adding and mixing 2 to 5% by weight of an essential oil mixed with at least two of lavender, lemon, clary sage, ylang ylang, rosemary, tea tree and cedar wood to 95 to 98% by weight of the saponified mixture, S700); Pouring the mixture to which the essential oil has been added into a mold and incubating at a temperature of 30 to 40 DEG C for 48 to 72 hours (S800); (S900) at room temperature aging at 22 to 28 DEG C for 4 to 6 weeks in a shaded and ventilated place by separating the solidified soap from the mold after aging by keeping the temperature at a constant temperature. A soap manufacturing method is disclosed.

This prior art technology can dramatically reduce the odor of the herbal medicines, thereby facilitating the use of the herbal medicines and reducing the characteristics of the herbal medicines separated from the carrier oil upon mixing. Thus, it is possible to mix various herbal medicines, It is a grain powder that is not a surfactant, and it has a disadvantage in that it has high washing power to prevent hair loss and promotes hair growth, while complicating the manufacturing steps.

An object of the present invention is to provide a natural soap which has good moisturizing effect and is not discolored, detached or deteriorated for a long period of time.

(A) 5 to 7 parts by weight of an extract of hippocampus and 1 to 1.2 parts by weight of an extract solution are mixed with 100 parts by weight of a base oil, stirred for 30 to 60 minutes and then heated to 45 to 55 ° C ; (b) 35 to 55 parts by weight of a caustic soda diluted solution cooled to 40 to 45 DEG C is further added and stirred; (c) 1 to 2 parts by weight of grape seed powder, 1 to 3 parts by weight of plum seed powder, 10 to 13 parts by weight of aroma oil and 3 to 5 parts by weight of beeswax are mixed and filled into a soap mold, Wherein the base oil is a mixture of 70 to 85 parts by weight of coconut oil, 50 to 65 parts by weight of olive oil and 15 to 30 parts by weight of grape seed oil per 100 parts by weight of palm oil, The aroma oil may be selected from the group consisting of rosewood, ginger, chamomile rosemary, bergamot, black pepper, lavender, line, lemon grass, rosemary, cypress, ylang ylang, jasmine, geranium, juniper berry, palmarosa, peppermint, And a method of manufacturing a natural soap characterized in that the natural soap is at least one selected from the group consisting of persimmon,

Preferably, the hippocampus extract of the present invention is prepared by mixing 3 to 7 parts by weight of hippocampal powder, 5 to 8 parts by weight of salt of sunflower, and 10 to 15 parts by weight of vegetable oil with 100 parts by weight of purified water, The mixture is heated for 6 hours and then filtered to cool. 50 to 70 parts by weight of anhydrous ethyl alcohol is further added, stirred for 18 to 24 hours, heated at 60 to 75 ° C for 30 to 45 minutes, and filtered.

Preferably, the solvent and the extract of the present invention are prepared by mixing 70 to 95 parts by weight of the finely divided powder and 5-7 parts by weight of mango powder with 100 parts by weight of purified water, heating at 100 to 110 ° C for 50 to 75 minutes 3 to 5 parts by weight of the salt of sunflower and 10 to 15 parts by weight of vegetable oil are further mixed and heated at 120 to 130 ° C for 10 to 30 minutes and then filtered to cool. 100 to 150 parts by weight of anhydrous ethyl alcohol is further mixed, The solution is allowed to stand for 7 to 9 days in a shade at a temperature of ~ 35 ° C, and then heated at 60 to 70 ° C for 3 to 5 hours in an open state, followed by filtration.

Preferably, the caustic soda dilution of step (b) of the present invention is mixed with 35 to 47 parts by weight of caustic soda with respect to 100 parts by weight of purified water.

Preferably, in step (c) of the present invention, 0.2 to 0.3 parts by weight of bamboo charcoal powder, 0.5 to 0.7 parts by weight of tin powder, and 3 to 5 parts by weight of loamy balls having a diameter of 1 to 2.5 mm are further added, Is prepared by mixing 70 to 85 parts by weight of loess powder and 2 to 2.5 parts by weight of talc powder with 100 parts by weight of purified water, molding the mixture into spheres having a diameter of 1 to 2.5 mm, and then heating the mixture at 1,200 to 1,350 ° C do.

The present invention as described above is to provide a method of preventing the discoloration, detachment or deterioration of natural soap for a long period of time by adding seaweed extract, solution and extract to provide excellent moisturizing effect and selectively adding bamboo charcoal powder, tungsten powder or loess ball It is effective.

Hereinafter, embodiments of the present invention will be described.

1. Making Soap

5 to 7 parts by weight of the hippocampus extract and 1 to 1.2 parts by weight of the extract and the extract are mixed with 100 parts by weight of the base oil, stirred for 30 to 60 minutes and then heated to 45 to 55 ° C. Here, the base oil is a mixture of 70 to 85 parts by weight of coconut oil, 50 to 65 parts by weight of olive oil and 15 to 30 parts by weight of grape seed oil based on 100 parts by weight of palm oil.

Then, 35 to 55 parts by weight of caustic soda diluted with 40 to 45 캜 of cold is further added and stirred to form a trace. Here, the caustic soda diluted solution is a mixture of 35 to 47 parts by weight of caustic soda with respect to 100 parts by weight of purified water.

1 to 2 parts by weight of grape seed powder, 1 to 3 parts by weight of plum seed powder, 10 to 13 parts by weight of aroma oil and 3 to 5 parts by weight of beeswax were mixed and filled into a soap mold, ~ 6 weeks. Here, the aroma oil is selected from the group consisting of rosewood, ginger, chamomile, bergamot, black pepper, lavender, line, lemon grass, rosemary, cypress, ylang ylang, jasmine, geranium, juniper berry, palmarosa, peppermint, Kinsense, Pyrrhio, and the like.

Finally, the aged soap is cut to a certain size and used.

In this embodiment, 0.2 to 0.3 parts by weight of bamboo charcoal powder, 0.5 to 0.7 part by weight of tin powder, and 3 to 5 parts by weight of loam balls of 1 to 2.5 mm in diameter and 1 to 2.5 mm in diameter are further added in order to prevent discoloration, Aging.

(a) Making seahorse extract

First, 3 to 7 parts by weight of hippocampal powder, 5 to 8 parts by weight of sun salt, and 10 to 15 parts by weight of marshmallow oil are mixed with 100 parts by weight of purified water, and the mixture is heated at 70 to 85 ° C for 4 to 6 hours.

Then, 50 to 70 parts by weight of anhydrous ethyl alcohol is further added, followed by stirring for 18 to 24 hours.

Finally, the mixture is heated at 60 to 75 ° C for 30 to 45 minutes and then filtered to cool.

(b) Making dragons and extracts

70 to 95 parts by weight of the finely divided powder and 5 to 7 parts by weight of the mango powder are mixed with 100 parts by weight of purified water, followed by heating at 100 to 110 DEG C for 50 to 75 minutes. Here, in the case of the medicines of this embodiment, the red seeding, 40 to 45 parts by weight and the 10 to 15 parts by weight were used for the kaolin and 100 parts by weight, and when the red sarcoma was less than 30 parts by weight, the color of the soap was unclear When the amount is more than the weight part, it becomes dark red, so it is preferable to comply with the content within the proposed range.

Then, 3 to 5 parts by weight of the salt of sunflower and 10 to 15 parts by weight of the vegetable oil are further mixed, heated at 120 to 130 ° C for 10 to 30 minutes, filtered and then cooled.

Subsequently, 100 to 150 parts by weight of anhydrous ethyl alcohol is further mixed, sealed, and then left for 7 to 9 days at a temperature of 30 to 35 DEG C in a shady place.

Finally, after opening, heat at 60 ~ 70 ℃ for 3 ~ 5 hours, and then filter and cool.

(c) Making loess balls

First, 70 to 85 parts by weight of loess powder and 2 to 2.5 parts by weight of talc powder are mixed with 100 parts by weight of purified water, molded into a sphere having a diameter of 1 to 2.5 mm, and then heated at 1,200 to 1,350 DEG C to produce loess balls do.

2. The natural soap produced by the manufacturing method according to this embodiment was superior to the ordinary soap sold in the market by moisture content of about 15 to 17% after 30 minutes from the cleansing, When used continuously for 7 to 10 days in a field or a bath, it was discolored, but it was not discolored even after 30 days.

While the present invention has been described with reference to exemplary embodiments, it is to be understood that the invention is not limited to the disclosed exemplary embodiments.

Claims (5)

(a) 5 to 7 parts by weight of an extract of hippocampus and 1 to 1.2 parts by weight of an extract and a solution are mixed with 100 parts by weight of base oil, stirred for 30 to 60 minutes, and then heated to 45 to 55 캜;
(b) 35 to 55 parts by weight of a caustic soda diluted solution cooled to 40 to 45 DEG C is further added and stirred;
(c) 1 to 2 parts by weight of grape seed powder, 1 to 3 parts by weight of plum seed powder, 10 to 13 parts by weight of aroma oil and 3 to 5 parts by weight of beeswax are mixed and filled into a soap mold, 4 to 6 weeks of aging,
The base oil is a mixture of 70 to 85 parts by weight of coconut oil, 50 to 65 parts by weight of olive oil and 15 to 30 parts by weight of grape seed oil based on 100 parts by weight of palm oil,
The aroma oil may be selected from the group consisting of rosewood, ginger, chamomile rosemary, bergamot, black pepper, lavender, line, lemon grass, rosemary, cypress, ylang ylang, jasmine, geranium, juniper berry, palmarosa, peppermint, Wherein the natural soap is at least one selected from the group consisting of soybean oil, soybean oil, soybean oil, and soybean oil.
The method according to claim 1,
3 to 7 parts by weight of hippocampus powder, 5 to 8 parts by weight of salt of horseshoe, and 10 to 15 parts by weight of vegetable oil were mixed with 100 parts by weight of purified water, heated at 70 to 85 ° C. for 4 to 6 hours, Adding 50 to 70 parts by weight of anhydrous ethyl alcohol, stirring the mixture for 18 to 24 hours, heating the mixture at 60 to 75 ° C for 30 to 45 minutes, and filtering the mixture.
The method according to claim 1,
The above-mentioned extract and the extract are mixed with 100 parts by weight of purified water, 70 to 95 parts by weight of the finely divided powder, 5 to 7 parts by weight of mango powder, heated at 100 to 110 ° C for 50 to 75 minutes, And 10-15 parts by weight of marine oil are further mixed and heated at 120-130 ° C. for 10-30 minutes. The mixture is filtered and cooled. 100-150 parts by weight of anhydrous ethyl alcohol is further mixed and sealed. The mixture is then shaded at a temperature of 30-35 ° C. For 7 to 9 days and then heated to 60 to 70 DEG C for 3 to 5 hours in an open state, and then filtered to produce a natural soap.
The method according to claim 1,
Wherein the caustic soda dilution liquid of step (b) is mixed with 35 to 47 parts by weight of caustic soda with respect to 100 parts by weight of purified water.
The method according to claim 1,
In the step (c), 0.2 to 0.3 parts by weight of bamboo charcoal powder, 0.5 to 0.7 parts by weight of tungsten powder and 3 to 5 parts by weight of loamy balls having a diameter of 1 to 2.5 mm are further added, , 70 to 85 parts by weight of loess powder and 2 to 2.5 parts by weight of talc powder are mixed to form a sphere having a diameter of 1 to 2.5 mm and heated at a temperature of 1,200 to 1,350 ° C.
KR1020160030743A 2016-03-15 2016-03-15 Method of manufacturing natural soaps KR101844313B1 (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20190064830A (en) * 2017-12-01 2019-06-11 사단법인 늘품교육문화협회 Manufacturing method of liquid soap using bamboo charcoal

Families Citing this family (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR102570858B1 (en) 2020-12-23 2023-08-28 전라남도 A skin massage composition for aromatherapy

Family Cites Families (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR101541289B1 (en) * 2015-04-13 2015-08-03 주식회사 코스메카코리아 Cosmetic composition containing sea horse, Eckloma cava and Gelidium amansii LAMOUROUX Extracts for anti-aging

Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20190064830A (en) * 2017-12-01 2019-06-11 사단법인 늘품교육문화협회 Manufacturing method of liquid soap using bamboo charcoal

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