KR101222743B1 - Method for manufacturing leaf mustard soap and manufactured leaf mustard soap by that method - Google Patents

Abstract

PURPOSE: A manufacturing method of leaf mustard soap is provided to manufacture leaf mustard soak with high pore-minimizing effect by uniformly dispersing unique components of mustard soap into a natural soap base. CONSTITUTION: A manufacturing method of leaf mustard soap comprises: a step of preparing a natural soap base; a step of powderizing leaf mustard; a step of melting the natural soap base, injecting the leaf mustard powder into the melted natural soap for low-speed stirring; a step of mixing a jojoba or vitamin E into the mixture; a step of mixing an essential oil into the mixture at 40 °C or less; a step of adding perfumes into the mixture and injecting the mixture into a silicon mold; and a step of demolding solidified soap form the silicon mold.

Description

METHOD FOR MANUFACTURING LEAF MUSTARD SOAP AND MANUFACTURED LEAF MUSTARD SOAP BY THAT METHOD}

The present invention relates to a fresh soap production method and a fresh soap produced by the method, more specifically because it is a natural ingredient, there is no skin trouble, in particular to induce pores convergence effect to prevent hair loss, itching, skin inflammation calming effect The present invention relates to a freshly prepared soap and a freshly prepared soap.

In general, soaps are hydrolyzed in aqueous solution to show surface activity and lower surface tension to enable stable foam generation and thus have strong detergency. The soap is mainly boiled fat or oil with alkali hydroxide and ester is hydrolyzed by the action of alkali. It is prepared by adding a predetermined flavor and pigment to the saponified and dry solidified.

These soaps have recently been commercialized in the form of a myriad of functional soaps based on the rapid development of beauty and cleaning technologies and various needs of consumers.

For example, soaps of various types and types are overflowing from whitening soaps having far-infrared rays and anion dissipation functions to pharmacological soaps such as heat soaps, color soaps, and transparent soaps, and heat, soothing, anti-inflammatory and antibacterial agents.

However, most of these soaps use artificial surfactants or artificial hardeners, which are not only harmful to the skin, but also cause water pollution.

Recently, natural soaps have begun to appear, and these are also manufactured and sold as various functional soaps.

However, even though most natural soaps are not effective, false exaggeration is causing more damage to consumers.

In particular, in case of stress hair loss, oily skin, dry skin dermatitis, bacterial itch, etc., pharmacological soap is expensive, and most of pharmacological soaps use artificial surfactants. There are many problems, such as peeling phenomenon of the skin epidermis.

Therefore, the present inventors paid attention to the specialty of the specialty of Yeosu, Jeollanam-do, especially Dolsan gat, and worries whether there is no way to utilize it as a natural soap by combining it with soap.

While the research was conducted, it was confirmed that the Patent Application Publication No. 10-2011-0076470 published by Chonnam National University Industry-Academic Cooperation Foundation discloses a method and composition for preparing natural plant soap using fresh fruit and citron.

By the way, the present inventors think that the contents of the disclosed prior art were much different, for example, the disclosed technology does not use the powdered itself of the gat, not only using the extract extracted from the gat but also other citron extract It was judged that it is difficult for consumers to make it easily or buy it at low cost.

In particular, the disclosed patent technology does not disclose exactly how to extract the mustard and citron extract, there is no similarity in terms of utilizing the lampshade, but there are many differences from the technical spirit of the present inventors to be described later, and there is almost no mutual citation Therefore, it was necessary to develop a natural fresh soap with both pharmacological and functional properties.

The present invention was created in view of the above-mentioned problems in the prior art as described above, and after melting a natural soap base (soap), natural freshly mixed with powder and essential oils to prevent hair loss, itching and skin Its main purpose is to provide a method for producing a natural fresh soap containing fresh ingredients having excellent efficacy against inflammation and a natural fresh soap prepared by the method.

The present invention as a means for achieving the above object, preparing a known natural soap base; After collecting the fresh shade, the impurities are removed and then dried to less than 5% moisture, and pulverized with a grinder to finely powder the freshness to less than 0.05mm; The prepared natural soap base is slowly heated to a temperature of 85-95 ° C. and melted, and when the natural soap base is completely melted, 1 ~ 1.5 g of freshly prepared powder is added to 100g of natural soap base, followed by 10-20 minutes with a stirrer. A mixing step of uniformly mixing the freshly added powder by slow stirring (100 rpm or less); Preservative treatment step of adding 5 to 10g of jojoba oil or vitamin E which provides antiseptic at the end of the mixing step in a range of 5 to 10 g compared to 100 g of a natural soap base; When the temperature of the stirring solution after the antiseptic treatment step falls below 40 ℃ essential oil addition step of stirring for 5 to 10 minutes by putting the essential oil in a ratio of 1.5 ~ 2g compared to 100g of natural soap base; When the stirring is completed, the fragrance is added to less than 1g compared to the natural soap base 100g, the soap solidification step of injecting the stirring solution into the silicone mold and left for 1 to 3 hours to solidify in the form of a soap; When the soap solidification step is completed, demolding and packaging step of taking out the solidified soap from the silicone mold and packaging; provides a fresh soap manufacturing method comprising a.

At this time, the raw fresh powder powdering step is characterized in that the root, leaves, stems of the fresh freshly dried to less than 5% moisture and then pulverized each and then finely divided into a mixed form in a weight ratio of 1: 1: 1. have.

In addition, in the solidifying step of the soap, in order to enhance the sedation before the fragrance is added, the powdered seaweed (Cynanchum paniculatum) powdered to a particle size of 0.05mm or less after drying to 0.5g or less compared to 100g of a natural soap base. It also has its features.

Furthermore, there is a feature in providing the freshly soap itself prepared by the freshly soap manufacturing method described above.

According to the present invention, the unique ingredients contained in the freshly distributed evenly in the natural soap base to increase the pore-converging effect when washing or washing hair to prevent hair loss, soothing skin itching or skin inflammation, and most of all, it is inexpensive There is an advantage that can be manufactured.

Hereinafter, preferred embodiments according to the present invention will be described in detail.

The present invention provides a method for producing a natural fresh soap using a natural soap base and freshly powdered.

To this end, the natural soap base is known, but in more detail, as a solid state made by mixing natural oil and caustic soda (NaOH), in the present invention is used after melting it by heating it.

In particular, caustic soda, as disclosed in the above prior art, is a representative strong base and should be handled with care.

In addition, there may be various kinds of natural oils.

Representative natural oils may be a variety of olive oil, coconut oil, palm oil, grape seed oil, castor oil, sunflower oil, etc., may be mixed in the ratio disclosed in the prior art mentioned in the prior art to make a natural soap base You can make a natural soap base in any of the ways that have been published.

The present invention is not characterized by making a natural soap base, but is characterized by adding a fresh powder to a known natural soap base, and simply adding fresh powder does not have efficacy and characteristics, so the technical features therein It is.

In addition, the mustard used in the present invention (leaf mustard) has a unique irritant pungent, as well shown in the prior art, which is produced by the action of the enzyme myrosinase (thioglucoside glucohydrolase) to sinigrin, a kind of glucosinolates contained in the Known.

In addition, the studies on the gat showed that the antioxidant activity of the gat was stronger than that of spinach, and it was reported that sinapine was isolated as one of the active ingredients.

In addition, the most representative of the physiologically active components of gat is isothiocyanate, which is unique to cruciferous plants. In addition, it is reported that the antimicrobial specrum exhibits a difference in antimicrobial activity according to isothiocyanate type.

In particular, the antimicrobial component of isothiocyanate was also identified in the gat. Isolation of flavonoid isorhamnetin-3-o-β-glucopyrano-side from the strongest antimicrobial activity of gat extract confirmed the antimicrobial activity.

Gad has been studied to have antifungal activity as well as antimicrobial activity. In particular, the anticancer activity of Dolsan gat has been reported to have high activity in roots, and antioxidant and ACE inhibition rates in leaves.

The present invention has been studied in consideration of the efficacy of these lampshade.

Hereinafter, a method for preparing a fresh soap according to the present invention will be described.

First, a step of preparing a known natural soap base is performed.

As described above, the natural soap base does not need to be particularly limited because it uses known materials.

Subsequently, a fresh fresh powdering step is performed.

The step of pulverizing the fresh shade is a step of collecting the fresh shade, removing impurities, and drying it in a dryer or natural state to less than 5% moisture, and then pulverizing with a pulverizer to finely reduce the particle size to less than 0.05 mm.

At this time, as described above, the root portion of the fresh mustard is the most effective, so you may use the whole amount, but for leveling the effect, dry the roots, leaves, and stems to less than 5% of moisture, and then grind each 1: It is better to mix and use at a weight ratio of 1: 1.

Here, the reason why the fresh mustard should be dried to less than 5% is that the fresh mustard contains rich in folic acid, carotene, vitamin C and iron, and a unique spicy flavor In particular, the spicy flavor of shinny green is weak when drying, and if the moisture of less than 5% is reduced to about 85 to 90% of the spicy taste should be evenly and uniformly dried to have a water content in the above range.

The drying method is preferably hot air drying, but if necessary, rapid drying is also possible by using a principle used in a microtron, that is, a microwave oven.

In addition, the reason for limiting the freshness of the powder to the above granularity is that when it exceeds 0.05mm, it remains in the form of granules, and when it comes into contact with the skin, it cuts while roughening or polishing the skin epidermis, so that it can penetrate into the pores. The size should be limited to the above size.

Subsequently, a natural soap base and freshly ground powder mixing step is performed.

The mixing step is to slowly melt the natural soap base in the solid state to a temperature of 85 ~ 95 ℃, and when the natural soap base is completely melted 1 ~ 1.5g of freshly prepared powder compared to 100g of natural soap base 10 Slowly stir for 20 minutes (100 rpm or less) to allow the freshly added powder to be mixed sufficiently, evenly and evenly.

At this time, the reason why the fresh powder is limited to the range compared to the natural soap base is that although the spicy ingredient of the freshly evaporated during the drying process, the spicy ingredient still remains, so if it exceeds 1.5 g, it may cause skin side effects. In addition, the inherent characteristics of the soap is less foam expression, and when added to less than 1g should be limited to the above range because almost no characteristic pore convergence and itching and skin inflammation sedation is not expressed.

In this way, when the raw fresh powder is completely mixed in the molten natural soap base, a preservation step is then performed.

The antiseptic treatment step is made in the form of adding jojoba oil or vitamin E to provide antiseptic in view of the fact that the present invention is a natural soap, these should be added in the range of 5 ~ 10g compared to 100g of the natural soap base.

Here, jojoba oil is an oil having an ingredient similar to the sebum of the skin, and is used most frequently as an aromatherapy diluent oil because it is soft and well absorbed by the skin, and is mainly used to make soaps, body creams and body lotions.

In particular, there is an anti-oxidant component is excellent in preservatives and can be preserved for a long time, and when added to the soap is prescribed to put less than 10% of the total soap capacity in the present invention should be added to 10g or less than 100g of natural soap base If less than 5g is added, the anti-oxidation function is lowered, so it must be maintained in the above range.

In addition, vitamin E has a kind of antiseptic function to prevent rancidity because it is an antioxidant that protects cells.

In the present invention, both synthetic vitamin E as well as natural vitamin E can be used. For natural vitamin E, both tocopherol b-alpha and tocopherol b-beta can be used.

 In addition, when ingesting vitamin E, the recommended daily amount is limited to 7.5 ~ 9mmg, but the present invention soap is not ingested, so when used as a preservative should be mixed in the above-mentioned range.

The mixing method is preferably added at the end of the low-speed stirring after the freshly prepared powder is mixed and stirred for about 5 to 10 minutes, since the preservative should be added after the freshly prepared fresh powder is sufficiently and uniformly distributed. .

Subsequently, the essential oil addition step is performed.

The essential oil addition step should be stirred for 5 to 10 minutes after the antiseptic treatment step is added at a rate of 1.5 ~ 2g compared to 100g of the natural soap base when the temperature of the stirring solution drops below 40 ℃.

This is because the essential oil itself has some volatility, so that at a temperature exceeding 40 ° C., the volatilization increases rapidly, and thus, it is possible to sufficiently stir at a temperature lower than the desired effect.

Here, essential oils are volatile highly concentrated essential oils extracted from aromatic plants, and are added in the present invention to enhance disinfection and antiseptic properties.

In particular, the most preferable essential oil is one of lavender essential oil and tea tree essential oil, and when it is added below 1.5g, there is little disinfection and antiseptic strengthening function due to volatile matter, and when it exceeds 2g, saponification is delayed to reduce foaming. Therefore, it should be added in the above range.

After the agitation is completed for a sufficient time through this process, various types of fragrances are added to less than 1 g of the natural soap base 100g in an amount that does not inhibit the foaming, and the stirring is completed.

Thereafter, after the stirring is completed, the stirring solution is injected into the silicon mold, and then left to stand for about 1 to 3 hours to solidify in a soap form.

Subsequently, when the solidification step is completed, the product is packaged after demolding to remove the solidified soap from the silicon mold.

In addition, before the fragrance is added to enhance the sedation, acid seabac (Cynanchum paniculatum) may be dried and powdered into a fine particle size of 0.05 mm or less, and may be further added to 0.5 g or less than 100 g of a natural soap base.

Sanhaebak is also called Seojanggyeong, which grows in the sunny meadows of mountains and fields. The stems stand straight, thin, long nodes, and bloom in August to September, and have a light tan. The root of Sanhaebak is used as a medicine called Seo Jang-kyung in oriental medicine, and it is known to have analgesic, soothing, and antibacterial effects.

In the present invention, the freshness of the powder and reinforcing aid to increase the skin soothing effect, the amount of powder to be added is preferably added only up to 0.5g to prevent this because the foam does not foam when using the soap.

Hereinafter, examples will be described.

[Example]

In order to confirm the efficacy of the freshly prepared soap according to the present invention was tested as follows.

(1) cleaning power test

Skin cleansing power was measured after washing to check the washing power of the freshly soap according to the present invention, and the measuring method was selected from eight test subjects selected from a laboratory maintained at a temperature of 20 to 22 ° C. and a humidity of 40 to 60% (20 to 50 years old). The skin oil removal rate was measured for 6 hours at 2 hour intervals after washing the face. The measurement tool was AROMA-TS oil meter, and the average was divided into male and female.

As a result, the amount of oil after cleansing was shown in Table 1 as compared to before cleansing. For comparison, the same test was conducted on the products of domestic soap manufacturers L and D.

division Freshly soap L company soap A company soap man 68 → 61 64 → 59 59 → 57 Woman 62 → 57 61 → 57 58 → 56

As a result, it was proved that the fresh soap according to the present invention also had sufficient cleaning power, and had at least the same effect as that of L company and A company to be compared.

(2) foam test

In order to test the foaming properties of the freshly soaps according to the present invention, 1 g each of freshly soap, L company soap, and A company soap was put in a 500 ml flask and shaken in the same manner to visually check the foaming properties of each soap.

As a result of visual observation, all three soaps were excellent in foaming property.

Thus, it was confirmed that the fresh soap according to the present invention can also be used as a soap having sufficient foamability.

(3) pore convergence test

In order to test the pore astringency of the fresh soap according to the present invention, three males were selected for hair loss, and each was divided into freshly soap, L company soap, and A company soap, and then three days were taken for three days.

At this time, when changing the soap after three days was not allowed to use the soap for a day, when the soap is not used to use the same shampoo only once a day.

In addition, to report the number of hair falls out when the tricycle, it was collected, and the results are shown in Table 2.

division Male 1 Male 2 Male 3 Freshly soap 4 2 Three L company soap 6 5 6 A company soap 5 5 7

From the results of Table 2, it was confirmed that the freshly soap according to the present invention has excellent converging effect of shrinking pores, and thus hair was not easily pulled out because hair holding power was excellent at trituration.

In addition, itching and skin irritation sedative effects were also confirmed as clinical results, but it is difficult to quantitatively verify it is replaced with a brief description.

Thus, the fresh soap according to the present invention was found to have sufficient value as a functional soap.

Claims (4)

Preparing a known natural soap base;
After collecting the fresh shade, the impurities are removed and then dried to less than 5% moisture, and pulverized with a grinder to finely powder the freshness to less than 0.05mm;
The prepared natural soap base is slowly heated to a temperature of 85-95 ° C. and melted, and when the natural soap base is completely melted, 1 ~ 1.5 g of freshly prepared powder is added to 100g of natural soap base, followed by 10-20 minutes with a stirrer. A mixing step of uniformly mixing the freshly added powder by slow stirring (100 rpm or less);
Preservative treatment step of adding 5 to 10g of jojoba oil or vitamin E which provides antiseptic at the end of the mixing step in a range of 5 to 10 g compared to 100 g of a natural soap base;
When the temperature of the stirring solution after the antiseptic treatment step falls below 40 ℃ essential oil addition step of stirring for 5 to 10 minutes by putting the essential oil in a ratio of 1.5 ~ 2g compared to 100g of natural soap base;
When the stirring is completed, the fragrance is added to less than 1g compared to the natural soap base 100g, the soap solidification step of injecting the stirring solution into the silicone mold and left for 1 to 3 hours to solidify in the form of a soap;
Fresh soap production method comprising a; demolding and packaging step of taking out the solidified soap from the silicone mold when the soap solidification step is completed.
The method according to claim 1;
The fresh-fresh powdering step is a freshly prepared soap, characterized in that the roots, leaves, stems of the freshly freshly dried to less than 5% of moisture and then pulverized each of them to be finely divided into a mixed form in a weight ratio of 1: 1: 1. Way.
The method according to claim 1;
In the soap solidifying step, the powdered acid seaweed (Cynanchum paniculatum) powdered to a particle size of 0.05mm or less after drying to enhance the sedation before the fragrance is added to less than 0.5g compared to 100g of the natural soap base. Freshly soap production method.
Freshly prepared soaps according to any one of claims 1 to 3, freshly soap manufacturing method.