KR20110076470A - The composition and method manufacture of soap plant function use citron and leaf mustard - Google Patents

Abstract

PURPOSE: Natural plant soap using leaf mustard and citron is provided to prevent the separation of a protective layer of the skin, rough skin, eczema, dermatitis and skin troubles since artificial surfactants and artificial hardeners are not used. CONSTITUTION: A method for preparing functional natural plant soap comprises the steps of: obtaining extract of leaf mustard and citron; mixing olive oil, coconut oil and palm oil, and heating the mixture to melt the mixture oil; obtaining caustic soda; mixing the mixture oil, caustic soda solution, and palm oil in a ratio of 6 : 3 : 1 to form a soap base; mixing the soap base, leaf mustard extract, and citron extract and mixing them to form a soap mixture solution; pouring the soap mixture solution into a soap molding frame; demolding the shaped soap and aging; and packaging the aged soap.

Description

The composition and method manufacture of soap plant function use citron and leaf mustard}

The present invention relates to a method for producing natural plant soap using fresh fruit and citron, and more particularly, using an olive oil, coconut oil, palm oil, grape seed oil, fresh fruit and citron extract to prepare a vegetable soap of 100% artificial surfactant, Since no artificial hardener is used, the present invention relates to a method for producing a functional natural soap using soap and citron and a soap composition to prevent peeling of the protective film of the skin and use of rough skin, eczema, dermatitis and skin troubles.

Conventionally, soaps have been manufactured using various materials, but by using artificial surfactants and artificial curing agents in the manufacture of soaps, there is a problem that rough skin, eczema, dermatitis and skin troubles are generated by removing the protective film of the skin during use.

Looking at the prior art in this field, Patent Publication No. 10-2005-0019288 cosmetic soap composition relates to a cosmetic soap composition consisting of a cosmetic soap holder, a moisturizing component, and a surfactant, hydrogenated hydrogenated palm oil or hydrogenated palm kernel oil and glass It consists of a cosmetic soap composition consisting of fatty acids, a moisturizing component which is a liquid emulsifier of oils and polyhydric alcohols, and a surfactant which is sodium sodium cocoyl isionate, disodium laurylsulfosuccinate, and a mixture thereof. Increased hardness by adding the addition process and optional free fatty acids to increase the hardness, and improves moisture retention without cracking while maintaining the properties of palm oil or palm kernel oil's excellent foaming power, bubble stability, and cleaning effect It can be seen that the soap composition can be provided.

In other words, the surfactant is a substance that is adsorbed to the interface in a dilute solution to reduce the surface tension. Normally, both lipophilic substances with both lipophilic and hydrophilic groups in one molecule become surfactants. Substances of such surfactants generally have washing power, emulsifying power, dispersing power, osmotic power, foaming power, etc. I), foaming agent for cement, lubricating oil additive, disinfectant, paint dispersant and so on.

Therefore, when the surfactant is mixed in the soap, there is the ease of the upper form of the soap and the ease of washing power, while the skin's protective film is removed by using the washing power, causing rough skin, eczema, dermatitis and skin troubles and the main causes of water pollution. There is a problem.

The present invention is to solve this problem, 100% vegetable soap by using olive oil, coconut oil, palm oil, grape seed oil, gat and citron extract to prevent the use of artificial surfactants, artificial hardeners to protect the skin during use This prevents moisture evaporation, cold air or bacteria from being absorbed by the skin, and prevents peeling of the skin's protective film when using soap, and prevents rough skin, eczema, dermatitis and skin troubles. The present invention relates to a method for producing a functional natural soap using soap and citron and a soap composition for the purpose of preventing water pollution from being generated by washing.

The present invention relates to a method and composition for producing a functional natural plant soap using a mustard and citron extract. First, a pre-treatment step of extracting and extracting an extract using a green juice machine after collecting and washing fresh and citron is first;

Mixing 60 to 40% by weight of olive oil, 40 to 30% by weight of coconut oil, and 20 to 10% by weight of palm oil to heat the mixture to 45 to 55 ° C. to melt the mixed oil;

Mixing and dissolving in a ratio of purified water 2 to 3: caustic soda 1;

Mixing the olive oil, coconut oil, palm oil mixed oil 6: purified water mixed with caustic soda 3: mixed grape seed oil at a ratio of 1 to form a soap base;

50 to 90 wt% of the prepared soap base, 5 to 30 wt% of the freshly extracted extract, and 5 to 20 wt% of the extracted citron extract, followed by stirring for 1 to 2 hours to form a soap mixed solution;

Pouring the prepared soap mixture into a soap mold and curing at 30 to 40 ° C. for 3 days to mold the soap mixture;

Demolding or shaping the molded soap and then demolding the soap for 4 weeks at a storage temperature of 30 to 40 ° C;

Soap is prepared by the step of packaging the aged soap.

Soap composition of the present invention prepared as described above, the mixture oil 6: 60 to 40% by weight of olive oil, 40 to 30% by weight of coconut oil, 20 to 10% by weight of palm oil, melted by heating to 50 ~ 55 ℃ 6 purified water 2 -3: purified water mixed at the ratio of caustic soda 1 3: soap composition composed of 50 to 90% by weight of soap base mixed with palm oil 1, 5 to 30% by weight of fresh extract, 5 to 20% by weight of citron extract do.

Thus, the present invention is made of 100% vegetable soap to prevent the peeling of the protective film of the skin during use and to prevent the occurrence of rough skin, eczema, dermatitis and skin troubles at the same time used water is quickly decomposed water pollution It is to provide a functional natural soap manufacturing method and soap composition using a mustard and citron to reduce the amount.

Thus, the present invention does not use artificial surfactants and artificial hardeners by producing 100% vegetable soap, so that the skin's protective film is peeled off during use, and rough skin, eczema, dermatitis and skin troubles are prevented from occurring. Soap and water used by the use of pure vegetation and the use of pure vegetation, when mixed with water in a wastewater treatment plant, rivers, rivers, seas, etc., is decomposed within 12 hours to prevent water pollution.

Hereinafter, an embodiment of the present invention will be described in detail.

First step: pretreatment process to extract freshly prepared citron

In the present invention, a fresh pretreatment process for adding freshly prepared citron juice and soap is carried out, after the selective freshness of freshly prepared citron and citron, extracts the extract using a juicer.

At this time, the extracts of Gad and citron are separately prepared separately.

The mustard and citron are extracted using a juicer or a separate extractor.

In addition, when using a fresh powder as an embodiment of the present invention to clean and remove the water and then lyophilized to grind like flour. In this case, when preparing soap, freshly mixed with powder and citron mixed with extract to produce soap.

Second Process: Soap Base Manufacturing Process

a) Manufacture of mixed oils of olive oil, coconut oil and palm oil

60 to 40% by weight of olive oil, 40 to 30% by weight of coconut oil, and 20 to 10% by weight of palm oil are mixed and heated to 45 to 55 ° C to dissolve the mixed oil.

The olive oil, coconut oil, palm oil is purchased in the market and mixed at the mixing ratio and then heated to 45 ~ 55 ℃ olive oil, coconut oil, palm oil is well mixed with each other. The reason why the mixed oil is heated to 45 to 55 ° C. is that the components of the oils are heated so that they do not destroy and especially the oil does not oxidize.

b) Purified water mixed with purified water and caustic soda

Receive normal tap water and store it for 3 hours or more to settle and use only constant water, or use purified water cooled to 100 ℃ boiled water. At this time, jijisu may be used as water for improving the soap component. The purpose of using purified water in the present invention is to minimize the change of the components of the soap by the foreign matter contained in the water.

The purified water is mixed in a ratio of 2 to 3: caustic soda 1 so that purified water and caustic soda are completely dissolved. This caustic soda is mixed with purified water and melts as white foam is generated.

The formula of caustic soda is NaOH, molecular weight is 39.997 g / mol, and the representative strong base is pure sodium hydroxide with white crystals. Caustic soda is the most important factor in making soap, and the amount of mixture may vary depending on the amount of base oil used to make soap. When soap is manufactured using caustic soda, low-temperature manufacturing is performed. The characteristic of caustic soda is white foam, which is mixed with water, and the temperature rises to 80 ℃. So, caustic soda must be mixed with water. When handling, take care not to touch the body and wear protective equipment.

Also, caustic soda should be purchased and absorbed water vapor from the purified air to melt itself, so it should be kept in contact with air.

c) soap base manufacturing

Mixing the olive oil, coconut oil, palm oil mixed oil 6: purified water and caustic soda mixed 3: water of grape seed oil 1 to prepare a base of the soap.

At this time, a mixture of purified water and grapeseed oil mixed with caustic soda in a state where the temperature of the mixed oil is 45 ℃ to 55 ℃.

The reason for mixing grape seed oil in the present invention contains linolenic acid which is an essential fatty acid, tocopherol which acts as an antioxidant, beta-cytosterol, etc., which is effective in skin care and anti-aging. In addition, research results are known to prevent adult diseases such as arteriosclerosis and high blood pressure when taken, grape seed oil is characterized by a smoke point of 250 ℃ higher than ordinary cooking oil. Therefore, there is an advantage that does not burn easily even at high temperatures.

Grape seed oil was classified as a dietary supplement reported by the Commissioner of the Korea Food and Drug Administration.

Therefore, the present invention is to provide a functional soap having an effect on antioxidants and skin beauty by preparing a soap by mixing grape seed oil during soap production.

Step 3: Mixing the Fresh Extract and the Oil Extract

50 to 90% by weight of the prepared soap base, 5 to 30% by weight of the extracted fresh extract, 5 to 20% by weight of the extracted citron extract, and then stirred for 1 to 2 hours to prepare a soap mixture.

In the present invention, the ratio of the freshly prepared extract or the citron extract to the soap production ratio soap base may be performed in various forms of Tables as shown in Table 1.

As can be seen in Table 1, the ratio of the freshly prepared extract or citron extract to the soap base soap base may be mixed with 50% by weight of the soap base, 30% by weight of fresh extract, 20% by weight of citron extract, and 80% by weight of soap extract. , Can be mixed with 10% by weight of fresh extract, 10% by weight citron extract, 90% by weight of soap extract, 5% by weight of fresh extract, 5% by weight of citron extract can be optionally adjusted.

In addition, natural soaps can be divided into low-temperature aging soap (Cold Soap (CP soap)) and melted soap (Melt Pour: MP soap) according to the manufacturing method.

A brief summary of these is shown in Table 1 below.

Fourth Process: Soap Molding and Aging Process

The soap mixture of the prepared soap base and freshly extracted liquid and citron extract is poured into a soap mold and cured at 30 to 40 ° C. for 3 days to be molded.

The molded soap is demolded or cut and then demolded and aged for 4 weeks at a storage temperature of 30 to 40 ° C.

The demolding after demolding or cutting to make the soap mature after molding has a difference according to the mold of the soap. In other words, if the soap mold is a mold capable of molding one soap, pour the soap liquid into the mold each, and after 3 days have elapsed, the soap mold is demolished and aged in a storage cell for 4 weeks. After pouring the cured soap, it is cut again to meet the specifications of the soap, demolded and stored in a storage for 4 weeks to mature. At this time, the aging temperature of the soap stored in the storage is maintained at 30 ~ 40 ℃ so that the vegetable soap is fully aged, then packaged and distributed.

Referring to the embodiment of the CP soap by the manufacturing process as follows.

≪ Example 1 >

* Material for Making Soap *

Prepare 400 g of olive oil, 300 g of coconut oil, 250 g of palm oil, 50 g of grape seed oil, 353 g of purified water, 147 g of caustic soda, and 200 g of fresh extract and citron extract.

* CP soap production *

a) Mix 400g olive oil, 300g coconut oil and 250g palm oil to make 50 ~ 55 ℃ in winter, and prepare mixed oil according to temperature of 45 ~ 50 ℃ in summer.

b) Mix 353 g of purified water and 147 g of caustic soda. The caustic soda is explosive, so be sure to mix caustic soda with water to prepare caustic soda.

c) mixing the prepared mixed oil of a) and purified caustic soda water of b), but maintaining the temperature of the mixed oil at about 50 ° C. and then mixing the caustic soda water and stirring the mixture in the opposite direction for 1 hour 30 minutes. Stir until thickened (like a syrup).

After stirring for 1 hour and 30 minutes, 50 g of grapeseed oil is added and stirred to form a soap base.

d) 200 g of freshly extracted extract and 200 g of citron extract in the soap base and stir until evenly mixed.

At this time, in order to prevent the base of the soap is cured in the state of maintaining the temperature of 50 ℃ fresh extract and citron extract is mixed to form a soap mixture.

e) After the soap mixture is formed as described above, it is poured into a soap mold and cured for 3 days.

f) Soap cured in the mold for 3 days is demolded and aged in the storage for 4 weeks to complete soap production.

To receive the quality evaluation of the soaps manufactured as described above, 30 students aged 20 to 25 years (to be conducted at Yeonsu University Campus, Jeonnap University) were washed with soap, soap, aromas, foam, and washing. Preference for action, skin trouble, color, firmness, and shape (see FIGS. 2-4) was examined by a five-point scale (5 = very good, 3 = normal, 1 = very bad). The five-point scale questionnaire used the form shown in FIG. 5.

One type of soap used in the quality assessment included MP (transparent) soap containing fresh mustard and citron extract, CP (opaque) soap containing fresh mustard and citron extract, commercial D soap and other extracts. Pure soaps were evaluated. The evaluation criteria were based on empirical evaluations that subjectively feels while using soap.

 Results for Soap Evaluation In order to evaluate the quality of fresh soaps, the results compared to commercially available soaps and natural soaps are shown in Table 3.

As can be seen in Table 3, there was no significant difference between fresh soap and other soaps in the case of fragrance when washing hands, and the reverberation remaining after washing hands was not different from other soaps. In the case of foam, CP (natural B) soap containing freshness and citron was significantly higher than other soaps, especially commercially available soaps, and the washing effect was better than MP soap containing freshness and citron (natural A). Although it was highest in, it was not different from other fresh soaps and natural soaps, while it was significantly higher than commercial soaps. Skin trouble, color, and shape were not different from Gat Soap and Natural Soap, but were significantly higher than commercial soaps.

In addition, the hardness did not show a difference between the soaps. In the above results, fresh soaps produced in this study showed better results than commercial soaps in all items except fragrances, but there was no difference compared to non-added natural soaps. It is believed that excellent results can be obtained from the comparison of.

Looking at the components of the mustard and citron used in the present invention,

Unique irritation of freshly spicy is to mainly due to an allyl isothiocyanate volatile mustard main component of mustard or horseradish, which is an enzyme in the form of glucosinolate acids contained in the freshly sinigrin myrosinase (thioglucoside glucohydro -

lase ) is generated by action. Allyl extracted from mustard on hand isothiocyanate has recently been shown to exhibit antimicrobial activity against various bacteria, yeasts and fungi.

So far, the studies on the antioxidant activity of gat showed that the antioxidant activity of gat was stronger than that of spinach and that sinapine was isolated as one of the active ingredients.

Representative of the physiologically active component of gat is isothiocyanate unique to cruciferous plants, the main component of allyl isothiocyanate , as well as 2- phenyl ethyl isothiocyanate, 5- methyl thiopentyl isothiocyanate , benzyl isothiocyanate It was confirmed that there is a strong antimicrobial activity in derivatives such as, depending on the type of isothiocyanate spectrum It is reported that there is a difference in antimicrobial activity.

In addition, there has been confirmed freshly antimicrobial ingredients other than the isothiocyanate of antibacterial action of the freshly flavonoid extract from the strongest fraction

Isohamnetin -3-o-β- glucopyrano - side was isolated for antimicrobial activity.

Gad has been studied to have antifungal as well as antibacterial effects, which may be effective in improving athlete's foot, fungus and hair loss.

In particular, the anticancer properties of Dolsan gat were reported to have high activity in roots, and antioxidant and ACE inhibition rates in leaves.

As mentioned above, there have been many reports of efficacy and physiological activities for gat, but only studies on gat kimchi are used for gat. Therefore, the development of a variety of processed products using the lampshade, so in the present invention was to prepare a soap using a lampshade.

On the other hand, citron is a taxonomy, citrus, citrus, and citrus genus, semi-arictic, strong in water, upright, and resistant to cold and disease compared to other citrus. In Korea, it grows only in the southern coastal areas such as Jeju, Goheung, Geochang, Wando, Jangheung, Gangjin, Geoje and Namhae.

Citron is an alkaline fruit that contains rich vitamin C, minerals and about 4% citric acid. It is rich in juice and fragrant, so it is mostly used for cooking as an acidulant or for the production of citron. However, due to its sour taste, it is rarely used for reproduction. I'm not doing it.

In 1996, cultivated area of domestic citron grew to 5,100 ha and output reached 18,500 M / T. In recent years, the area of citron cultivation in the southern coastal area of Jeonnam, including Goheung, Jeonnam, has increased rapidly to 70.2% (1800 ha) nationwide, which can severely damage local farm incomes due to the plunge in the price of citron due to oversupply.

Citron has its own fragrance and many useful ingredients. Among them, pectin, which is present in large amounts in citron flesh, has a superior function as a dietary fiber compared to other pectins, and limonene compound, the main ingredient of citron bitterness, suppresses various cancers. It is reported to have a function.

In addition, limonene (limonoid), an essential oil component present in a large amount in the skin of citron, has a wide range of use because of its anti-cancer effect against antibacterial activity, stomach cancer, lung cancer and the like. In addition, flavonoid compounds have been reported to have effects such as antioxidant and anti-aging, anti-inflammatory, anti-allergic and the like.

Most of the consumption of citron in Korea is ornamental, citron soup, and citron drink. Recently, the citron juice obtained by juice of yuzu is exported to Japan, and in Japan, it is added to sweets and miso as a flavor material.

In this way, Gad and Yuja are representative foods of the Jeonnam region and have been used mainly for foods. However, by applying the food to not only foods but also daily necessities by applying to the acne, atopic skin, fungal skin, and skin supplying vitamin C. It seems to be.

Therefore, in the present invention, the antimicrobial and antifungal properties of gat studied up to now, the antibacterial properties of citron and vitamin C, citron fragrance is added to enhance the utilization of the gat and citron as a part of the skin care with functional properties using natural gat and citron Soap is manufactured.

Using the soap of the present invention prepared in this way and the commercially available general soap, the result of comparing the total number of bacteria before and after hand washing is shown in Table 4. Before using soap as a control, the total bacterial count was 5.8 × 10 ⁴ when washing with average soap at 6.0 × 10 ⁴ , and after using fresh citron soap at 6.7 × 10 ⁴ before using soap as a control It was 4.0 × 10 ⁴ , indicating that the total bacterial count of the fresh citron soap was larger than that of ordinary soap.

As described above, the present invention provides a natural soap using a shade and a citron to provide a natural soap rich in antibacterial, fungal and vitamin C by using a citrus discarded in a rural area and a citron. The region's specialties, gat and yuzu, have the effect of increasing income in rural areas and provide consumers with quality natural soap without irritating the skin.

Brief Description of the Drawings The following briefly describes the accompanying drawings of the present invention.

1 is a block diagram of a vegetable soap manufacturing process of the present invention, from the pre-treatment step to extract the fresh and citron, shows the process-specific step of demolding the soap in the mold for aging.

Figure 2 is a MP soap physical picture produced by the soap manufacturing method of the present invention, Figure 3 is a soap physical picture made in various colors by the mixing method of MP soap and CP soap produced by the soap manufacturing method of the present invention. 4 is a real picture of a soap freshly prepared by extracting a mixture of MP soap and CP soap prepared by the soap manufacturing method of the present invention, Figure 5 is a soap of various forms prepared by the manufacturing method of the present invention 3 to 5 show the products of the soap produced by the soap manufacturing method using the shade and citron of the present invention, Figure 5 is produced by the manufacturing method of the present invention Product photograph showing an example of packaging state of soap.

Figure 6 is an illustration of a questionnaire form for receiving an evaluation of the soap produced by the manufacturing method of the present invention, it shows a form for users to receive the questionnaire after using the soap prepared by the manufacturing method of the present invention. .

1 is a block diagram of a vegetable soap manufacturing process of the present invention.

Figure 2 is a physical soap MP soap produced by the soap manufacturing method of the present invention.

Figure 3 is a soap physical picture produced in various colors by the mixing method of MP soap and CP soap produced by the soap manufacturing method of the present invention.

Figure 4 Soap real picture of freshly prepared extract by the mixing method of MP soap and CP soap prepared by the soap production method of the present invention.

Figure 5 is a real picture showing the soap of various forms prepared by the production method of the present invention.

Figure 6 is an illustration of a questionnaire form received an evaluation of the soap produced by the manufacturing method of the present invention.

Claims (3)

In the vegetable soap manufacturing method, Pre-treatment step of extracting and washing fresh and yuza and extracting the extract using green juice; Mixing 60 to 40% by weight of olive oil, 40 to 30% by weight of coconut oil, and 20 to 10% by weight of palm oil to dissolve the mixed oil by heating to 50 to 55 ° C; Mixing and dissolving in a ratio of purified water 2 to 3: caustic soda 1; Mixing the olive oil, coconut oil, palm oil, mixed oil 6: purified water and caustic soda, mixed water 3: palm oil 1 to form a soap base; 50 to 90 wt% of the prepared soap base, 5 to 30 wt% of the freshly extracted extract, and 5 to 20 wt% of the extracted citron extract, followed by stirring for 1 to 2 hours to form a soap mixed solution; Pouring the prepared soap mixture into a soap mold and curing at 30 to 40 ° C. for 3 days to mold the soap mixture; Demolding or shaping the molded soap and then demolding the soap for 4 weeks at a storage temperature of 30 to 40 ° C .; Functional natural plant soap production method using a freshly prepared citron and citron characterized in that the step of packaging the aged soap. The method of claim 1, The natural vegetable extract mixed in the soap base is a functional natural plant soap manufacturing method using a fresh and yuzu, characterized in that any one of the fresh extract and citron extract is mixed Soap composition prepared by the manufacturing method of claim 1, 60 to 40% by weight of olive oil, 40 to 30% by weight of coconut oil, 20 to 10% by weight of palm oil mixed and melted by heating to 50 ~ 55 ℃ 6 purified water 2 to 3: Purified water mixed at a ratio of caustic soda 1 3: 50 to 90 wt% of a soap base mixed at a ratio of grape seed oil 1, 5 to 30 wt% of a fresh extract, and 5 to 20 wt% of a citron extract. Functional natural plant soap composition using a mustard and citron.

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