KR20050078935A - Cosmetic soap and manufacturing process of the same - Google Patents

Cosmetic soap and manufacturing process of the same Download PDF

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KR20050078935A
KR20050078935A KR1020040007029A KR20040007029A KR20050078935A KR 20050078935 A KR20050078935 A KR 20050078935A KR 1020040007029 A KR1020040007029 A KR 1020040007029A KR 20040007029 A KR20040007029 A KR 20040007029A KR 20050078935 A KR20050078935 A KR 20050078935A
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soap
oil
caustic soda
weight
prepared
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Korean (ko)
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박수근
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박수근
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    • AHUMAN NECESSITIES
    • A41WEARING APPAREL
    • A41DOUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
    • A41D13/00Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
    • A41D13/05Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches protecting only a particular body part
    • A41D13/11Protective face masks, e.g. for surgical use, or for use in foul atmospheres
    • A41D13/1161Means for fastening to the user's head
    • AHUMAN NECESSITIES
    • A62LIFE-SAVING; FIRE-FIGHTING
    • A62BDEVICES, APPARATUS OR METHODS FOR LIFE-SAVING
    • A62B18/00Breathing masks or helmets, e.g. affording protection against chemical agents or for use at high altitudes or incorporating a pump or compressor for reducing the inhalation effort
    • A62B18/02Masks
    • A62B18/025Halfmasks
    • AHUMAN NECESSITIES
    • A41WEARING APPAREL
    • A41DOUTERWEAR; PROTECTIVE GARMENTS; ACCESSORIES
    • A41D13/00Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches
    • A41D13/05Professional, industrial or sporting protective garments, e.g. surgeons' gowns or garments protecting against blows or punches protecting only a particular body part
    • A41D13/11Protective face masks, e.g. for surgical use, or for use in foul atmospheres
    • A41D13/1107Protective face masks, e.g. for surgical use, or for use in foul atmospheres characterised by their shape
    • A41D13/1138Protective face masks, e.g. for surgical use, or for use in foul atmospheres characterised by their shape with a cup configuration

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  • Health & Medical Sciences (AREA)
  • General Health & Medical Sciences (AREA)
  • Physical Education & Sports Medicine (AREA)
  • Engineering & Computer Science (AREA)
  • Textile Engineering (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Zoology (AREA)
  • Pulmonology (AREA)
  • Business, Economics & Management (AREA)
  • Emergency Management (AREA)
  • Cosmetics (AREA)
  • Detergent Compositions (AREA)

Abstract

본 발명은 화장비누 및 그 제조방법에 관한 것으로, 70∼75중량%의 정제수에 25∼30중량%의 가성소다를 용해시켜 제조한 가성소다수를 올리브오일과 코코넛 오일 및 팜유가 각각 30∼35중량%의 비율로 혼합된 지방산 오일에 첨가·교반함으로써 제조되는 지방산 나트륨비누 90∼95중량%에 뽕잎분말 1∼3중량%, 황토분말 4∼7중량%를 첨가하여 제조함으로써 사용시 주름발생 억제효과 및 피부노화 억제효과를 발휘할 수 있도록 하고, 피지와 노폐물 흡수효과를 발휘할 수 있도록 하며, 지성피부에 사용시 세안감을 현저히 향상시킬 수 있도록 한 것이다. The present invention relates to a cosmetic soap and a method for manufacturing the same, wherein caustic soda water prepared by dissolving caustic soda at 25 to 30 wt% in 70 to 75 wt% purified water is 30 to 35 wt%, respectively, of olive oil, coconut oil and palm oil. Inhibition of wrinkle occurrence during use by adding 1 to 3% by weight of mulberry leaf powder and 4 to 7% by weight of ocher powder to 90 to 95% by weight of fatty acid sodium soap prepared by addition and stirring to mixed fatty acid oil in a ratio of It is to make skin aging inhibitory effect, to sebum and waste absorbing effect, and to improve the face wash when used on oily skin.

Description

화장비누 및 그 제조방법{COSMETIC SOAP AND MANUFACTURING PROCESS OF THE SAME} Cosmetic soap and its manufacturing method {COSMETIC SOAP AND MANUFACTURING PROCESS OF THE SAME}

본 발명은 화장비누 및 그 제조방법에 관한 것으로, 보다 상세하게는 주요 성분인 지방산 나트륨비누에 일정 양의 뽕잎분말과 황토분말을 첨가함으로써 사용시 주름발생 억제효과 및 피부노화 억제효과를 발휘할 수 있도록 하고, 피지와 노폐물 흡수효과를 발휘할 수 있도록 하며, 지성피부에 사용시 세안감을 현저히 향상시킬 수 있도록 한 화장비누 및 그 제조방법에 관한 것이다. The present invention relates to a cosmetic soap and a method for manufacturing the same, and more particularly, by adding a certain amount of mulberry leaf powder and ocher powder to the fatty acid sodium soap, which is a main component, to exert an anti-wrinkle effect and an anti-aging effect upon use. The present invention relates to a cosmetic soap and a method of manufacturing the same, which can exert sebum and waste absorbing effect and remarkably improve cleansing feeling when used on oily skin.

일반적으로, 화장비누는 각종 동물성 유지 또는 식물성 유지를 수산화나트륨(NaOH)을 이용하여 비누화반응(Saponification)을 시켜 수분 12∼15% 정도의 니트비누(Neat soap)을 만든 다음 불쾌한 취기를 제거하기 위하여 향을 첨가하고, 피부의 보습성, 윤활성을 위하여 각종 유연제나 보습제 등 필요에 따라 여러 가지 첨가제를 추가로 배합하여 고형으로 제조한 것을 일컫는다. In general, cosmetic soap is saponification using various kinds of animal or vegetable oils with sodium hydroxide (NaOH) to make neat soap of about 12-15% of moisture and then remove unpleasant odor. It refers to the one prepared by adding various flavors and adding various additives as necessary, such as various softening agents or moisturizers, for the purpose of moisturizing and lubricity of the skin.

이와 같은 화장비누는 수분과 접촉하는 경우에 발생되는 풍부한 기포와 강한 세정력 때문에 오래전부터 세안용으로 널리 사용되어져 오고 있다. Such cosmetic soaps have been widely used for washing for a long time because of the abundant air bubbles and strong detergency generated in contact with moisture.

이와 같은 화장비누를 제조하는 과정은 비누기재(Soap base)를 제조하는 습식공정과, 상기 습식공정을 통하여 제조된 비누기재에 향, 색소, 산화방지제 등을 첨가하여 균일하게 혼합한 후 압출시켜 절단, 타형을 거쳐 최종제품을 생산하는 건식공정으로 이루어진다.The process of manufacturing the cosmetic soap is a wet process for manufacturing a soap base (Soap base), and by adding the fragrance, pigments, antioxidants, etc. to the soap base produced through the wet process, uniformly mixed, extruded and cut It consists of a dry process that produces the final product after being crushed.

상기 비누기재를 제조하는 습식공정으로는 지방산 오일에 가성소다를 부가하여 제조하는 감화법(Saponification), 지방산 오일에 가성소다를 부가하여 제조하는 중화법(Neutralization) 및 유지를 메탄올로 처리하여 메틸에스테르를 제조한 후, 메틸에스테르와 가성소다를 반응시켜 비누를 생성시키는 메틸에스테르 감화법(Methylester saponification)반응으로 나뉠 수 있다.In the wet process for preparing the soap base, saponification prepared by adding caustic soda to fatty acid oil, neutralization process prepared by adding caustic soda to fatty acid oil, and methyl ester by treating fat or oil with methanol After the preparation, it can be divided into a methyl ester saponification reaction of reacting methyl ester with caustic soda to produce soap.

한편, 특수한 비누에 유용한 사포니플렉스(Saponiflex)공정이 있는데, 이는 독립적인 배치(Batch)방식으로서 지방산으로부터 완전히 혼합된 비누까지를 모두 단일 공정으로 수행할 수 있도록 한 비교적 새로운 공정이다.On the other hand, there is a saponiflex process that is useful for special soaps, which is a relatively new process that allows all batches of soaps from fatty acids to fully mixed soaps in a single batch process.

그러나, 현재 대부분의 비누기재를 제조하는 습식공정은 지방산에 가성소다를 부가하여 제조하는 중화법이 적용되고 있는 실정이다.However, the current wet process for manufacturing most soap base is a situation that the neutralization method of adding caustic soda to the fatty acid is applied.

한편, 건식공정에서는 위에서 기술한 바와 같이 다양한 습식공정을 통하여 제조된 니트비누(Neat soap)를 적절한 온도와 압력조건하에서 열교환기를 거쳐 스프레이건조기(Spray dryer)에서 분무하여 건조시킨다.On the other hand, in the dry process, as described above, the wet soap (Neat soap) manufactured through a variety of wet process is sprayed and dried in a spray dryer (Spray dryer) through a heat exchanger under an appropriate temperature and pressure conditions.

그 후, 제조된 비누칩에 산화방지제, 증백제, 향, 색소를 혼합하고, 압출공정 및 롤밀(Roll-Mill)을 거쳐 균일하게 혼합한 후 둥근 바(Bar) 형태로 압출시키고 일정 크기로 잘라 프레스로 성형한 후 포장하는 것이다.Then, antioxidants, brighteners, fragrances, and pigments are mixed with the prepared soap chips, uniformly mixed through an extrusion process and a roll mill, and extruded into a round bar shape, and cut into a predetermined size. It is molded by pressing and then packed.

이와 같은 비누의 제조시에 가장 중요한 역할을 하는 것은 사용되는 지방산 오일인데, 상기 지방산 오일의 종류로는 야자유, 팜유, 대두유, 피마자유, 올리브유, 팜핵유 등이 있다.The most important role in the production of such a soap is the fatty acid oil used, the type of fatty oil is palm oil, palm oil, soybean oil, castor oil, olive oil, palm kernel oil and the like.

한편, 화장비누의 제조과정에서는 단순히 기포를 발생시키고 부드러우면서도 매끄러운 세안감을 부여할 뿐만 아니라, 사용시 보습효과를 높이거나 각질을 제거하는 등의 여러 가지 효과를 얻고자 하기 위한 여러 종류의 기능성 첨가제 또는 아로마테라피(Aromatherapy)효과를 얻기 위한 아로마 에센셜 오일이 보조재료로 첨가된다.Meanwhile, in the manufacturing process of the cosmetic soap, various types of functional additives for generating various effects such as simply generating bubbles and giving a soft and smooth face wash, as well as enhancing moisturizing effect or removing dead skin cells during use or Aromatherapy essential oils are added as supplementary ingredients to achieve the aromatherapy effect.

상기 기능성 첨가제의 예로는 강력한 보습효과를 갖는 계란 노른자, 사포닌이 함유되어 피부와 모공의 기름과 때를 흡수하여 분해시켜주는 팥, 미네랄과 비타민이 풍부하여 피부와 머리카락에 좋은 해조류 등이 있다.Examples of the functional additives include egg yolks having a powerful moisturizing effect, and saponins, which are rich in red beans, minerals, and vitamins, which absorb and decompose oil and dirt in the skin and pores, which are good for skin and hair.

또, 아로마테라피효과를 얻을 수 있는 아로마 에센셜 오일 같은 보조재료로는 달콤한 발삼향이 발향되면서 불면증, 두통, 두근거림에 효과가 있는 라벤더(Lavender), 강하고 깨끗하며, 상쾌한 약초내음이 발향되면서 머리를 맑게 하고, 기억력을 높여주는 효능을 갖는 로즈마리(Rosemary), 달콤한 꽃내음이 발향되면서 긴장완화효과가 있는 쟈스민(Jasmin) 등이 있다. In addition, supplementary ingredients such as aromatherapy essential oils, which can achieve aromatherapy effect, have a sweet balm fragrance, which is effective for insomnia, headache, and palpitations, and a strong, clean, refreshing medicinal odor makes the hair clear. Rosemary, which has the effect of improving memory, and sweet scent of flowers are scented and Jasmin has a relaxing effect.

본 발명의 목적은 지방산 나트륨비누에 일정양의 뽕잎분말과 황토분말을 첨가함으로써 지속적인 사용시 주름발생 억제효과 및 피부노화 억제효과를 발휘할 수 있도록 하고, 피지와 노폐물 흡수효과를 발휘할 수 있도록 하며, 지성피부에 사용시 세안감을 현저히 향상시킬 수 있도록 한 새로운 화장비누 및 그 제조방법을 제공하는 것이다. The object of the present invention is to add a certain amount of mulberry leaf powder and ocher powder to the fatty acid sodium soap to exert the effect of inhibiting wrinkles and inhibiting skin aging under continuous use, to exert sebum and waste absorbing effect, oily skin It is to provide a new cosmetic soap and a method for manufacturing the same so as to significantly improve the face wash when used in.

이와 같은 목적을 달성하기 위하여, 본 발명에 의한 화장비누는 70∼75중량%의 정제수에 25∼30중량%의 가성소다를 용해시켜 제조한 가성소다수를 올리브오일과 코코넛 오일 및 팜유가 각각 30∼35중량%의 비율로 혼합된 지방산 오일에 첨가·교반함으로써 제조되는 지방산 나트륨비누 90∼95중량%에 뽕잎분말 1∼3중량%, 황토분말 4∼7중량%를 첨가하여 주름발생 억제효과와 피부노화 억제효과 및 피지와 노폐물 흡수효과를 발휘할 수 있도록 한 특징을 갖는다.In order to achieve the above object, the cosmetic soap according to the present invention is caustic soda water prepared by dissolving caustic soda at 25 to 30 wt% in 70 to 75 wt% purified water and 30 to 30 g each of olive oil, coconut oil and palm oil. Wrinkles inhibiting wrinkles by adding 1 to 3% by weight of mulberry leaf powder and 4 to 7% by weight of ocher powder to 90 to 95% by weight of fatty acid sodium soap prepared by adding and stirring to fatty acid oil mixed at 35% by weight. It has the characteristics to exert aging inhibitory effect and sebum and waste absorbing effect.

본 발명의 목적을 달성하기 위하여, 본 발명에 따른 화장비누의 제조방법은 깨끗하게 세척하여 그늘에서 건조한 뽕잎을 2∼4cm의 크기로 절단한 후 90∼110℃에서 쪄 1차 증숙시키고, 1차증숙된 뽕잎을 그늘에서 냉각시킨 다음 170∼190℃에서 덖음하여 2차 증숙시킨 후 건조기를 이용하여 건조시킨 후 분쇄하여 뽕잎분말을 준비하는 공정과; 채취한 황토로부터 이물질을 제거한 다음 그늘에 말린 후 곱게 갈아 황토분말을 준비하는 공정과; 소정의 체적을 갖는 내열 용기에 준비된 정제수를 넣고, 가성소다(NaOH)를 천천히 넣으면서 저어서 완전히 녹인 다음, 40∼45℃ 이내가 되도록 식혀 가성소다수를 제조하는 공정과; 별도의 용기에 올리브 오일, 코코넛 오일, 팜유를 계량하여 넣고, 약한 불로 가열하면서 저어 완전히 녹인 다음 42∼45℃로 식혀 지방산 오일을 만드는 공정과; 가성소다수를 지방산 오일에 천천히 부으면서 혼합시킨 다음 20∼30분 동안 조금 빠른 속도로 계속 교반하여 비누화반응이 발생되도록 하여 비누용액을 제조하는 공정과; 비누용액에 트레이스(Trace: 비누용액을 떨어뜨렸을 때 자국이 생기는 현상)가 나타나면, 비누용액 90∼95중량%에 대하여 뽕잎분말 1∼3중량%, 황토분말 4∼7중량% 비율로 첨가하고 교반하여 균일하게 혼합시키는 공정과; 준비된 비누틀에 뽕잎분말 및 황토분말이 혼합된 비누용액을 넘치지 않도록 붓고, 밀봉한 후 따뜻한 장소에서 24시간 이상 보온처리하는 공정과; 비누틀에 의해 성형된 비누를 소정의 크기로 절단한 후 4주이상 건조시키는 공정을 포함한다. In order to achieve the object of the present invention, the manufacturing method of the cosmetic soap according to the present invention is washed cleanly cut mulberry leaves dried in the shade to the size of 2 ~ 4cm 쪄 primary steaming at 90 ~ 110 ℃, primary steaming Cooling the mulberry leaves in a shade, and then steaming them at 170 to 190 ° C. for second steaming, drying them using a dryer, and then grinding them to prepare mulberry leaf powder; Removing the foreign matter from the collected ocher and then drying it in the shade and grinding finely to prepare the ocher powder; Adding purified water to a heat-resistant container having a predetermined volume, stirring the mixture slowly while adding caustic soda (NaOH), and cooling the mixture to 40 to 45 ° C to produce caustic soda water; Weighing olive oil, coconut oil and palm oil in a separate container, stir while heating on a low heat, and completely melt and cool to 42-45 ° C. to form fatty oil; Mixing the caustic soda water with fatty acid oil slowly and continuously stirring the mixture at a high speed for 20 to 30 minutes to cause a saponification reaction to produce a soap solution; If traces appear on the soap solution, add 1 to 3% by weight of mulberry leaf powder and 4 to 7% by weight of ocher powder with respect to 90 to 95% by weight of the soap solution. And uniformly mixing; Pouring soap solution mixed with mulberry leaf powder and ocher powder to the prepared soap frame so as not to overflow, and sealing and warming at a warm place for 24 hours; The soap molded by the soap mold is cut to a predetermined size and then dried for at least 4 weeks.

이하, 본 발명의 바람직한 실시예를 보다 상세하게 설명한다.Hereinafter, preferred embodiments of the present invention will be described in more detail.

본 발명에 따른 화장비누는 각각 30∼35중량%의 비율로 혼합된 지방산 오일에 가성소다수를 첨가·교반하여 만들어지는 지방산 나트륨비누에 뽕잎분말과 황토분말을 일정 중량비로 첨가한 것이다.In the cosmetic soap according to the present invention, the mulberry leaf powder and the ocher powder are added to the fatty acid sodium soap made by adding and stirring caustic soda water to the fatty acid oil mixed in the proportion of 30 to 35% by weight, respectively.

본 발명의 화장비누에서 상기 가성소다수는 정제수 70∼75중량%에 20∼25중량%의 가성소다를 용해함으로써 제조된다.In the cosmetic soap of the present invention, the caustic soda water is prepared by dissolving 20 to 25 wt% of caustic soda in 70 to 75 wt% of purified water.

또, 상기 지방산 나트륨비누 90∼95중량%에 대하여 뽕잎분말은 1∼3중량%로 첨가되고, 황토분말은 4∼7중량%로 첨가된다.The mulberry leaf powder is added in an amount of 1 to 3% by weight, and the ocher powder in an amount of 4 to 7% by weight based on 90 to 95% by weight of the fatty acid sodium soap.

본 발명의 화장비누에 첨가되는 상기 뽕잎분말은 콜라겐대사를 활발하게 하여 주름발생을 억제하고, 피부노화를 억제하는 효과가 있는 것으로서 다음과 같이 만들어진다.The mulberry leaf powder added to the cosmetic soap of the present invention is made as follows as it has an effect of activating collagen metabolism to suppress wrinkles and inhibit skin aging.

뽕잎을 채취한 후 표면에 묻어 있는 먼지 등 이물질을 깨끗이 세척하고, 그늘에서 하루동안 건조시킨다.After collecting the mulberry leaves, clean the foreign substances such as dirt on the surface and dry them in the shade for a day.

그늘에서 건조된 뽕잎을 2∼4cm의 크기로 절단한 후 90∼110℃에서 쪄 1차 증숙시키고, 1차증숙된 뽕잎을 그늘에서 냉각시킨다.The mulberry leaves dried in the shade is cut to a size of 2 to 4 cm and then steamed at 90 to 110 ° C. for the first time, and the primary steamed mulberry leaves are cooled in the shade.

그런 다음 170∼190℃에서 덖음하여 2차 증숙시킨 다음 건조기를 이용하여 건조시키고 분쇄하여 뽕잎분말을 준비한다.Then steamed at 170 ~ 190 ℃ secondary steaming, dried using a dryer and pulverized to prepare a mulberry leaf powder.

한편, 붉은 빛이 나는 황토를 채취한 다음 이물질을 제거하고 그늘에 말린 후 미세한 분말형태로 분쇄하여 황토분말을 준비한다.On the other hand, red ocher is collected and then the foreign matter is removed, dried in the shade and pulverized into a fine powder to prepare the ocher powder.

이와 같이 만들어지는 뽕잎분말에는 조단백질 16.38%(질소계수 6.25), 조지방 4.32%, 식이섬유 48.54%, 탄수화물 65.88%이 함유되어 있고, 뽕잎분말 100g에 대하여 나트륨 66.16㎎, 비타민C 36.95㎎이 함유되며, 그 열량은 192.88Kcal인 특성을 갖는다.The mulberry leaf powder prepared in this way contains crude protein 16.38% (nitrogen coefficient 6.25), crude fat 4.32%, dietary fiber 48.54%, carbohydrate 65.88%, and 100.g of mulberry leaf powder contains sodium 66.16mg, vitamin C 36.95mg, The calorie has a characteristic of 192.88 Kcal.

또, 본 발명의 화장비누에 분말형태로 첨가되는 황토는 원적외선을 발생시켜 세포의 생리작용이 활발하게 이루어지도록 하고, 열에너지를 발생시켜 유해물질을 방출하는 광전효과를 발휘하며, 정화력과 분해력이 있어 여분의 피지와 노폐물을 흡수하고 지성피부에 세안감을 향상시키는 특성을 갖는다.In addition, the ocher added in powder form to the cosmetic soap of the present invention generates far-infrared rays so that the physiological action of the cells is actively performed, and exhibits the photoelectric effect of releasing harmful substances by generating thermal energy, and has purification and degrading power. It absorbs excess sebum and wastes and improves cleansing of oily skin.

상기 황토분말은 시판되는 것을 사용할 수 도 있다.The ocher powder may be commercially available.

본 발명에 의한 화장비누는 다음과 같이 저온법(Cold process)에 의하여 제조된다.The cosmetic soap according to the present invention is prepared by a cold process as follows.

먼저, 본 발명에 따른 화장비누를 제조하기 위한 재료로서, 정제수 260g, 가성소다(NaOH) 105g, 올리브 오일 250g, 코코넛 오일, 250g, 팜유 250g과 기능성 첨가제로서 뽕잎분말 10g, 황토분말 50g을 준비한다.First, as a material for preparing a cosmetic soap according to the present invention, 260 g of purified water, 105 g of sodium hydroxide (NaOH), 250 g of olive oil, coconut oil, 250 g, palm oil 250 g and mulberry leaf powder 10 g, ocher powder 50 g are prepared as functional additives. .

소정의 체적을 갖는 내열 용기에 준비된 정제수를 넣고, 가성소다를 천천히 넣으면서 저어서 완전히 녹인 다음, 40∼45℃ 이내가 되도록 식혀둔다.The prepared purified water is added to a heat-resistant container having a predetermined volume, and the caustic soda is slowly added while stirring to dissolve completely, and then cooled to within 40 to 45 ° C.

스테인레스재의 용기에 준비된 올리브 오일, 코코넛 오일, 팜유를 계량하여 넣고, 약한 불로 가열하면서 저어 완전히 녹이고, 42∼45℃가 되면 불을 끈다.Weigh the prepared olive oil, coconut oil and palm oil in a stainless steel container, stir it completely while heating on low heat, and turn off the fire when it reaches 42-45 ℃.

상기 정제수에 가성소다를 녹여 만든 가성소다수를 스테인레스 용기내의 지방산 오일에 천천히 부으면서 혼합시킨다. Caustic soda water made by dissolving caustic soda in purified water is mixed while slowly pouring into fatty acid oil in a stainless container.

가성소다수를 다 부은 후에도 20∼30분 동안 조금 빠른 속도로 계속 교반하여 비누화반응이 가속되도록 하고, 트레이스(Trace : 비누용액을 떨어뜨렸을 때 자국이 생기는 현상)가 나타나는지 확인한다.After pouring the caustic soda water, continue to stir a little faster for 20-30 minutes to accelerate the saponification reaction, and check if the trace (trace) occurs when the soap solution is dropped.

트레이스가 나타나면, 준비된 뽕잎분말과 황토분말을 첨가하고 교반하여 균일하게 혼합되도록 한다.When the trace appears, add the prepared mulberry leaf powder and ocher powder and stir to ensure uniform mixing.

상기한 뽕잎분말은 올리브 오일, 코코넛 오일, 팜유로 만들어지는 지방산 나트륨비누 90∼95중량%에 대하여 1∼3중량%의 비율로 첨가되고, 황토분말은 4∼7중량%의 비율로 첨가되는 것이 바람직하다.The mulberry leaf powder is added in an amount of 1 to 3% by weight relative to 90 to 95% by weight of fatty acid sodium soap made of olive oil, coconut oil and palm oil, and the ocher powder is added in an amount of 4 to 7% by weight. desirable.

이 때 원하는 색소와 향을 첨가할 수 있다.At this time, a desired pigment and flavor can be added.

준비된 비누틀에 뽕잎분말 및 황토분말의 기능성 첨가제가 혼합된 비누원료를 넘치지 않도록 붓고, 밀봉한 후 담요나 모포로 감싼 상태에서 따뜻한 장소에서 24시간 이상 보온 처리한다.The prepared soap frame is poured with the mulberry leaf powder and the ocher powder functional additives so as not to overflow the soap raw material, and then sealed and warmed at a warm place for 24 hours in a blanket or blanket.

그런 다음 비누틀로부터 비누를 빼내어 적당한 크기로 절단하고, 4주 이상 건조시킨 후 사용한다. Then remove the soap from the soap mold, cut it to the appropriate size, and dry it for at least 4 weeks before use.

실시예 Example

본 발명에 따른 화장비누를 다음과 같이 제조하였다.Cosmetic soap according to the present invention was prepared as follows.

먼저, 그늘에서 건조된 뽕잎을 3cm크기로 절단한 후 솥에 넣고 100℃로 찐 다음, 그늘에서 식힌 후 다시 솥에 넣어 180℃의 온도에서 덖음하여 건조기로 건조시킨다.First, the mulberry leaves dried in the shade is cut into 3cm size, put in a pot and steamed at 100 ℃, cooled in the shade and put in a pot again and steamed at a temperature of 180 ℃ and dried with a dryer.

이와 같이 건조기에서 건조된 뽕잎을 분쇄기에 넣어 분쇄시켜 뽕잎분말 10g을 준비하였다.Thus, the mulberry leaves dried in the dryer was put into a grinder to grind to prepare a mulberry leaf powder 10g.

한편, 붉은색이 나는 황토를 채취하여 이물질을 제거하고 그늘에서 말린 후 분쇄하여 미세한 황토분말 50g을 준비하였다. On the other hand, red ocher was taken to remove foreign substances, dried in the shade and crushed to prepare a fine ocher powder 50g.

한편, 본 발명에 따른 화장비누를 제조하기 위한 다른 재료로서 정제수 260g, 가성소다(NaOH) 105g, 올리브 오일 250g, 코코넛 오일, 250g, 팜유 250g를 준비하였다.On the other hand, 260 g of purified water, 105 g of caustic soda (NaOH), 250 g of olive oil, coconut oil, 250 g, and 250 g of palm oil were prepared as another material for preparing the cosmetic soap according to the present invention.

먼저, 소정의 체적을 갖는 내열 용기에 준비된 정제수를 넣고, 가성소다를 천천히 넣으면서 저어서 완전히 녹인 다음, 40∼45℃ 이내가 되도록 식혀 가성소다수를 제조하였다. First, the prepared purified water was added to a heat-resistant container having a predetermined volume, and the caustic soda was slowly dissolved while slowly adding caustic soda, and cooled to be within 40 to 45 ° C. to prepare caustic soda water.

별도의 스테인레스재 용기에 상기한 올리브 오일, 코코넛 오일, 팜유를 계량하여 넣고, 약한 불로 가열하면서 저어 완전히 녹인 다음 42∼45℃로 유지되게 하여 지방산 오일을 제조하였다.The olive oil, coconut oil, and palm oil were weighed in a separate stainless steel container, and stirred while heating with a weak fire to completely dissolve and then maintained at 42 to 45 ° C. to prepare a fatty acid oil.

상기 가성소다수를 스테인레스 용기내의 지방산 오일에 천천히 부으면서 교반하여 혼합시키고, 가성소다수를 다 부은 후에도 20∼30분 동안 조금 빠른 속도로 계속 저어주어 비누화반응이 가속되도록 하면서 트레이스(Trace : 비누용액을 떨어뜨렸을 때 자국이 생기는 현상)가 나타나는지 확인하였다.Slowly pour the caustic soda water into the fatty acid oil in the stainless container, stir and mix, and continue to stir a little faster for 20-30 minutes even after pouring the caustic soda to accelerate the saponification reaction trace (Trace: Soap solution was dropped The appearance of marks).

비누용액에 트레이스가 나타나는 것을 확인한 후 준비된 뽕잎분말과 황토분말을 첨가하고 교반하여 균일하게 혼합하였다.After confirming that traces appear in the soap solution, the prepared mulberry leaf powder and ocher powder were added and stirred and mixed uniformly.

이 때, 상기 뽕잎분말은 올리브 오일, 코코넛 오일, 팜유로 만들어지는 지방산 나트륨비누 95중량%에 대하여 1중량%로 첨가하고, 황토분말은 4중량%로 첨가하였다.At this time, the mulberry leaf powder was added in 1% by weight relative to 95% by weight of fatty acid sodium soap made of olive oil, coconut oil, palm oil, ocher powder was added in 4% by weight.

그런 다음 미리 준비한 비누틀에 뽕잎분말 및 황토분말이 혼합된 비누원료를 넘치지 않도록 붓고, 밀봉한 후 담요로 감싼 상태에서 따뜻한 장소에서 24시간 이상 보온처리한 다음, 비누틀로부터 비누를 빼내어 적당한 크기로 절단하고, 4주 이상 건조시킨 후 사용하였다. Then, pour the soap raw material mixed with mulberry leaf powder and ocher powder in a ready-to-prepared soap frame, seal it, wrap it with a blanket, keep warm for at least 24 hours in a warm place, and then remove the soap from the soap frame to a suitable size. Cut and used for 4 weeks or more after drying.

이와 같은 본 발명을 적용하면, 비누에 콜라겐 대사를 활발하게 하는 뽕잎분말과, 미네랄이 풍부하게 함유되고 원적외선을 방사시키는 황토분말이 첨가됨에 따라 지속적인 사용시에 주름발생과 피부노화가 억제되는 효과를 얻을 수 있고, 피지와 노폐물이 흡수제거됨에 따라 지성피부에 사용시 세안감이 현저히 향상된다는 효과가 있다. According to the present invention, the mulberry leaf powder that activates collagen metabolism and the ocher powder which is rich in minerals and emits far-infrared rays are added to soap, so that wrinkles and skin aging can be suppressed during continuous use. The sebum and the waste are absorbed and removed, so that the use of oily skin has a significant improvement in the sense of washing.

Claims (3)

70∼75중량%의 정제수에 25∼30중량%의 가성소다를 용해시켜 제조한 가성소다수를 올리브오일과 코코넛 오일 및 팜유가 각각 30∼35중량%의 비율로 혼합된 지방산 오일에 첨가·교반함으로써 제조되는 지방산 나트륨비누 90∼95중량%에 뽕잎분말 1∼3중량%, 황토분말 4∼7중량%를 첨가하여 제조된 것을 특징으로 하는 화장비누.Caustic soda water prepared by dissolving caustic soda at 25 to 30 wt% in 70 to 75 wt% purified water is added to the fatty acid oil mixed with olive oil, coconut oil and palm oil at a ratio of 30 to 35 wt%, respectively. Cosmetic soap characterized in that it is prepared by adding 1 to 3% by weight of mulberry leaf powder, 4 to 7% by weight of ocher powder to 90 to 95% by weight of the fatty acid sodium soap to be prepared. 깨끗하게 세척하여 그늘에서 건조한 뽕잎을 2∼4cm의 크기로 절단한 후 90∼110℃에서 쪄 1차 증숙시키고, 1차증숙된 뽕잎을 그늘에서 냉각시킨 다음 170∼190℃에서 덖음하여 2차 증숙시킨 후 건조기를 이용하여 건조시킨 후 분쇄하여 뽕잎분말을 준비하는 공정과; After washing cleanly, cut the mulberry leaves dried in the shade to a size of 2 ~ 4cm, 증 primary steaming at 90 ~ 110 ℃, the first steamed mulberry leaves cooled in the shade and then steamed at 170 ~ 190 ℃ secondary steaming After drying using a dryer and then pulverized to prepare a mulberry leaf powder; 채취한 황토로부터 이물질을 제거한 다음 그늘에 말린 후 곱게 갈아 황토분말을 준비하는 공정과; Removing the foreign matter from the collected ocher and then drying it in the shade and grinding finely to prepare the ocher powder; 소정의 체적을 갖는 내열 용기에 준비된 정제수를 넣고, 가성소다(NaOH)를 천천히 넣으면서 저어서 완전히 녹인 다음, 40∼45℃ 이내가 되도록 식혀 가성소다수를 제조하는 공정과; Adding purified water to a heat-resistant container having a predetermined volume, stirring the mixture slowly while adding caustic soda (NaOH), and cooling the mixture to 40 to 45 ° C to produce caustic soda water; 별도의 용기에 올리브 오일, 코코넛 오일, 팜유를 계량하여 넣고, 약한 불로 가열하면서 저어 완전히 녹인 다음 42∼45℃로 식혀 지방산 오일을 만드는 공정과; Weighing olive oil, coconut oil and palm oil in a separate container, stir while heating on a low heat, and completely melt and cool to 42-45 ° C. to form fatty oil; 가성소다수를 지방산 오일에 천천히 부으면서 혼합시킨 다음 20∼30분 동안 조금 빠른 속도로 계속 교반하여 비누화반응이 발생되도록 하여 비누용액을 제조하는 공정과; Mixing the caustic soda water with fatty acid oil slowly and continuously stirring the mixture at a high speed for 20 to 30 minutes to cause a saponification reaction to produce a soap solution; 비누용액에 트레이스(Trace: 비누용액을 떨어뜨렸을 때 자국이 생기는 현상)가 나타나면, 비누용액 90∼95중량%에 대하여 뽕잎분말 1∼3중량%, 황토분말 4∼7중량% 비율로 첨가하고 교반하여 균일하게 혼합시키는 공정과; If traces appear on the soap solution, add 1 to 3% by weight of mulberry leaf powder and 4 to 7% by weight of ocher powder with respect to 90 to 95% by weight of the soap solution. And uniformly mixing; 준비된 비누틀에 뽕잎분말 및 황토분말이 혼합된 비누용액을 넘치지 않도록 붓고, 밀봉한 후 따뜻한 장소에서 24시간 이상 보온처리하는 공정과; Pouring soap solution mixed with mulberry leaf powder and ocher powder to the prepared soap frame so as not to overflow, and sealing and warming at a warm place for 24 hours; 비누틀에 의해 성형된 비누를 소정의 크기로 절단한 후 4주이상 건조시키는 공정을 포함하는 것을 특징으로 하는 화장비누의 제조방법.Method for producing a cosmetic soap comprising the step of cutting the soap molded by a soap mold to a predetermined size and then dried for at least 4 weeks. 제2항에 있어서, The method of claim 2, 상기 비누용액은 70∼75중량%의 정제수에 25∼30중량%의 가성소다를 용해시켜 제조한 가성소다수를 올리브오일과 코코넛 오일 및 팜유가 각각 30∼35중량%의 비율로 혼합된 지방산 오일에 첨가·교반함으로써 제조되는 것을 특징으로 하는 화장비누의 제조방법.The soap solution is caustic soda water prepared by dissolving caustic soda at 25 to 30 wt% in 70 to 75 wt% purified water to fatty acid oil mixed with olive oil, coconut oil and palm oil at a ratio of 30 to 35 wt%, respectively. A method for producing a cosmetic soap, which is prepared by adding and stirring.
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Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100816675B1 (en) * 2006-11-09 2008-03-27 김성일 Loess soap manufacturing method
KR100830125B1 (en) * 2007-01-12 2008-05-20 주승호 The soap and product method of a loess soap
KR100837796B1 (en) * 2007-12-06 2008-06-13 김홍열 Neutral calcium-yellow soil soup and the producing method
KR100851954B1 (en) * 2007-03-30 2008-08-12 권세환 Method for preparing soap added by bamboo extracts and soap made thereby
KR100959695B1 (en) * 2008-10-09 2010-05-26 전정례 Manufacturing method of eco-friendly detergent composition
KR101138417B1 (en) * 2009-12-29 2012-04-26 전남대학교산학협력단 The composition and method manufacture of soap plant function use citron and leaf mustard
KR101444692B1 (en) * 2012-08-09 2014-09-26 호형철 Functional soap and manufacturing method thereof

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR100816675B1 (en) * 2006-11-09 2008-03-27 김성일 Loess soap manufacturing method
KR100830125B1 (en) * 2007-01-12 2008-05-20 주승호 The soap and product method of a loess soap
KR100851954B1 (en) * 2007-03-30 2008-08-12 권세환 Method for preparing soap added by bamboo extracts and soap made thereby
KR100837796B1 (en) * 2007-12-06 2008-06-13 김홍열 Neutral calcium-yellow soil soup and the producing method
KR100959695B1 (en) * 2008-10-09 2010-05-26 전정례 Manufacturing method of eco-friendly detergent composition
KR101138417B1 (en) * 2009-12-29 2012-04-26 전남대학교산학협력단 The composition and method manufacture of soap plant function use citron and leaf mustard
KR101444692B1 (en) * 2012-08-09 2014-09-26 호형철 Functional soap and manufacturing method thereof

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