KR20140143738A - 표면 산화된 티타늄-알루미늄-질화물 유리 이형 코팅을 구비한 재생 유리-형성 몰드 - Google Patents
표면 산화된 티타늄-알루미늄-질화물 유리 이형 코팅을 구비한 재생 유리-형성 몰드 Download PDFInfo
- Publication number
- KR20140143738A KR20140143738A KR1020147017203A KR20147017203A KR20140143738A KR 20140143738 A KR20140143738 A KR 20140143738A KR 1020147017203 A KR1020147017203 A KR 1020147017203A KR 20147017203 A KR20147017203 A KR 20147017203A KR 20140143738 A KR20140143738 A KR 20140143738A
- Authority
- KR
- South Korea
- Prior art keywords
- glass
- release coating
- aluminum
- mold
- nitride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Withdrawn
Links
- 238000000576 coating method Methods 0.000 title claims abstract description 107
- 239000011248 coating agent Substances 0.000 title claims abstract description 85
- 239000011521 glass Substances 0.000 title claims abstract description 54
- 238000007496 glass forming Methods 0.000 title claims abstract description 25
- NBIIXXVUZAFLBC-UHFFFAOYSA-K phosphate Chemical compound [O-]P([O-])([O-])=O NBIIXXVUZAFLBC-UHFFFAOYSA-K 0.000 claims abstract description 6
- PXGOKWXKJXAPGV-UHFFFAOYSA-N Fluorine Chemical compound FF PXGOKWXKJXAPGV-UHFFFAOYSA-N 0.000 claims abstract description 4
- 239000011737 fluorine Substances 0.000 claims abstract description 4
- 229910052731 fluorine Inorganic materials 0.000 claims abstract description 4
- 150000007522 mineralic acids Chemical class 0.000 claims abstract description 3
- 238000000034 method Methods 0.000 claims description 48
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims description 31
- 229910052710 silicon Inorganic materials 0.000 claims description 21
- XUIMIQQOPSSXEZ-UHFFFAOYSA-N Silicon Chemical compound [Si] XUIMIQQOPSSXEZ-UHFFFAOYSA-N 0.000 claims description 18
- 229910052760 oxygen Inorganic materials 0.000 claims description 18
- 239000001301 oxygen Substances 0.000 claims description 18
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims description 17
- 229910052751 metal Inorganic materials 0.000 claims description 17
- 239000002184 metal Substances 0.000 claims description 17
- 239000010703 silicon Substances 0.000 claims description 17
- 239000010410 layer Substances 0.000 claims description 16
- 229910052757 nitrogen Inorganic materials 0.000 claims description 16
- 239000002585 base Substances 0.000 claims description 15
- 239000005358 alkali aluminosilicate glass Substances 0.000 claims description 13
- 229910052783 alkali metal Inorganic materials 0.000 claims description 11
- 150000001340 alkali metals Chemical class 0.000 claims description 11
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 claims description 10
- 239000011734 sodium Substances 0.000 claims description 10
- 239000000203 mixture Substances 0.000 claims description 9
- 229910052708 sodium Inorganic materials 0.000 claims description 9
- DGAQECJNVWCQMB-PUAWFVPOSA-M Ilexoside XXIX Chemical compound C[C@@H]1CC[C@@]2(CC[C@@]3(C(=CC[C@H]4[C@]3(CC[C@@H]5[C@@]4(CC[C@@H](C5(C)C)OS(=O)(=O)[O-])C)C)[C@@H]2[C@]1(C)O)C)C(=O)O[C@H]6[C@@H]([C@H]([C@@H]([C@H](O6)CO)O)O)O.[Na+] DGAQECJNVWCQMB-PUAWFVPOSA-M 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 7
- 229910045601 alloy Inorganic materials 0.000 claims description 7
- 239000000956 alloy Substances 0.000 claims description 7
- 229910052782 aluminium Inorganic materials 0.000 claims description 6
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 claims description 6
- 229910001092 metal group alloy Inorganic materials 0.000 claims description 6
- 229910010037 TiAlN Inorganic materials 0.000 claims description 5
- NRTOMJZYCJJWKI-UHFFFAOYSA-N Titanium nitride Chemical compound [Ti]#N NRTOMJZYCJJWKI-UHFFFAOYSA-N 0.000 claims description 4
- 229910052759 nickel Inorganic materials 0.000 claims description 4
- 230000001172 regenerating effect Effects 0.000 claims description 4
- 239000002344 surface layer Substances 0.000 claims description 4
- 229910052758 niobium Inorganic materials 0.000 claims description 3
- 239000006133 sodium aluminosilicate glass Substances 0.000 claims description 2
- 229910052727 yttrium Inorganic materials 0.000 claims description 2
- 229910052726 zirconium Inorganic materials 0.000 claims description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims 1
- 239000011707 mineral Substances 0.000 claims 1
- 239000003513 alkali Substances 0.000 abstract description 12
- UQZIWOQVLUASCR-UHFFFAOYSA-N alumane;titanium Chemical compound [AlH3].[Ti] UQZIWOQVLUASCR-UHFFFAOYSA-N 0.000 abstract description 6
- 239000005354 aluminosilicate glass Substances 0.000 abstract description 3
- 239000000243 solution Substances 0.000 description 16
- 229910018509 Al—N Inorganic materials 0.000 description 13
- 239000000463 material Substances 0.000 description 12
- 238000011282 treatment Methods 0.000 description 11
- 238000000465 moulding Methods 0.000 description 10
- 230000015572 biosynthetic process Effects 0.000 description 8
- 230000008569 process Effects 0.000 description 7
- 238000011069 regeneration method Methods 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 5
- 230000008929 regeneration Effects 0.000 description 5
- 230000008901 benefit Effects 0.000 description 4
- 229910001026 inconel Inorganic materials 0.000 description 4
- 239000006060 molten glass Substances 0.000 description 4
- 150000004767 nitrides Chemical class 0.000 description 4
- 238000001004 secondary ion mass spectrometry Methods 0.000 description 4
- 238000010301 surface-oxidation reaction Methods 0.000 description 4
- TWQQBPRWLWTPOO-UHFFFAOYSA-N [F].P(O)(O)(O)=O.Cl Chemical compound [F].P(O)(O)(O)=O.Cl TWQQBPRWLWTPOO-UHFFFAOYSA-N 0.000 description 3
- 230000002378 acidificating effect Effects 0.000 description 3
- 230000001747 exhibiting effect Effects 0.000 description 3
- 238000005470 impregnation Methods 0.000 description 3
- KRHYYFGTRYWZRS-UHFFFAOYSA-M Fluoride anion Chemical compound [F-] KRHYYFGTRYWZRS-UHFFFAOYSA-M 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- -1 cast iron Chemical class 0.000 description 2
- 239000000919 ceramic Substances 0.000 description 2
- 238000013034 coating degradation Methods 0.000 description 2
- 239000000470 constituent Substances 0.000 description 2
- 238000009792 diffusion process Methods 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 238000001312 dry etching Methods 0.000 description 2
- 238000005530 etching Methods 0.000 description 2
- 230000009477 glass transition Effects 0.000 description 2
- 150000002739 metals Chemical class 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- 238000006467 substitution reaction Methods 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 229910018072 Al 2 O 3 Inorganic materials 0.000 description 1
- 229910000838 Al alloy Inorganic materials 0.000 description 1
- 229910001018 Cast iron Inorganic materials 0.000 description 1
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 description 1
- VYZAMTAEIAYCRO-UHFFFAOYSA-N Chromium Chemical compound [Cr] VYZAMTAEIAYCRO-UHFFFAOYSA-N 0.000 description 1
- 229910000881 Cu alloy Inorganic materials 0.000 description 1
- 229910000570 Cupronickel Inorganic materials 0.000 description 1
- 229910000990 Ni alloy Inorganic materials 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- 229910004349 Ti-Al Inorganic materials 0.000 description 1
- 229910010413 TiO 2 Inorganic materials 0.000 description 1
- ATJFFYVFTNAWJD-UHFFFAOYSA-N Tin Chemical compound [Sn] ATJFFYVFTNAWJD-UHFFFAOYSA-N 0.000 description 1
- RTAQQCXQSZGOHL-UHFFFAOYSA-N Titanium Chemical compound [Ti] RTAQQCXQSZGOHL-UHFFFAOYSA-N 0.000 description 1
- 229910004692 Ti—Al Inorganic materials 0.000 description 1
- YKTSYUJCYHOUJP-UHFFFAOYSA-N [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] Chemical compound [O--].[Al+3].[Al+3].[O-][Si]([O-])([O-])[O-] YKTSYUJCYHOUJP-UHFFFAOYSA-N 0.000 description 1
- 238000005299 abrasion Methods 0.000 description 1
- 239000003929 acidic solution Substances 0.000 description 1
- 150000007513 acids Chemical class 0.000 description 1
- PNEYBMLMFCGWSK-UHFFFAOYSA-N aluminium oxide Inorganic materials [O-2].[O-2].[O-2].[Al+3].[Al+3] PNEYBMLMFCGWSK-UHFFFAOYSA-N 0.000 description 1
- 238000013459 approach Methods 0.000 description 1
- 229910052791 calcium Inorganic materials 0.000 description 1
- 238000012512 characterization method Methods 0.000 description 1
- 229910052804 chromium Inorganic materials 0.000 description 1
- 239000011651 chromium Substances 0.000 description 1
- BIJOYKCOMBZXAE-UHFFFAOYSA-N chromium iron nickel Chemical compound [Cr].[Fe].[Ni] BIJOYKCOMBZXAE-UHFFFAOYSA-N 0.000 description 1
- 239000012459 cleaning agent Substances 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000011109 contamination Methods 0.000 description 1
- 229910052802 copper Inorganic materials 0.000 description 1
- 239000010949 copper Substances 0.000 description 1
- 230000001351 cycling effect Effects 0.000 description 1
- 238000000354 decomposition reaction Methods 0.000 description 1
- 230000007547 defect Effects 0.000 description 1
- 230000006735 deficit Effects 0.000 description 1
- 230000000694 effects Effects 0.000 description 1
- 238000000635 electron micrograph Methods 0.000 description 1
- 238000005516 engineering process Methods 0.000 description 1
- 238000009472 formulation Methods 0.000 description 1
- 238000010406 interfacial reaction Methods 0.000 description 1
- 150000002500 ions Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 229910052749 magnesium Inorganic materials 0.000 description 1
- 229910052748 manganese Inorganic materials 0.000 description 1
- 238000005259 measurement Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000005012 migration Effects 0.000 description 1
- 238000013508 migration Methods 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 239000012778 molding material Substances 0.000 description 1
- 229910052750 molybdenum Inorganic materials 0.000 description 1
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 1
- 230000003647 oxidation Effects 0.000 description 1
- 238000007254 oxidation reaction Methods 0.000 description 1
- 230000001590 oxidative effect Effects 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 150000002926 oxygen Chemical class 0.000 description 1
- 229940085991 phosphate ion Drugs 0.000 description 1
- 230000002685 pulmonary effect Effects 0.000 description 1
- 230000009257 reactivity Effects 0.000 description 1
- 230000009467 reduction Effects 0.000 description 1
- 230000003716 rejuvenation Effects 0.000 description 1
- 230000008439 repair process Effects 0.000 description 1
- 230000000979 retarding effect Effects 0.000 description 1
- 238000007493 shaping process Methods 0.000 description 1
- 239000005368 silicate glass Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 229910000601 superalloy Inorganic materials 0.000 description 1
- 230000009897 systematic effect Effects 0.000 description 1
- 239000010936 titanium Substances 0.000 description 1
- 229910052719 titanium Inorganic materials 0.000 description 1
Images
Classifications
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B11/00—Pressing molten glass or performed glass reheated to equivalent low viscosity without blowing
- C03B11/06—Construction of plunger or mould
- C03B11/08—Construction of plunger or mould for making solid articles, e.g. lenses
- C03B11/084—Construction of plunger or mould for making solid articles, e.g. lenses material composition or material properties of press dies therefor
- C03B11/086—Construction of plunger or mould for making solid articles, e.g. lenses material composition or material properties of press dies therefor of coated dies
-
- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09K—MATERIALS FOR MISCELLANEOUS APPLICATIONS, NOT PROVIDED FOR ELSEWHERE
- C09K13/00—Etching, surface-brightening or pickling compositions
- C09K13/04—Etching, surface-brightening or pickling compositions containing an inorganic acid
- C09K13/08—Etching, surface-brightening or pickling compositions containing an inorganic acid containing a fluorine compound
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2215/00—Press-moulding glass
- C03B2215/02—Press-mould materials
- C03B2215/08—Coated press-mould dies
- C03B2215/10—Die base materials
- C03B2215/11—Metals
-
- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03B—MANUFACTURE, SHAPING, OR SUPPLEMENTARY PROCESSES
- C03B2215/00—Press-moulding glass
- C03B2215/02—Press-mould materials
- C03B2215/08—Coated press-mould dies
- C03B2215/14—Die top coat materials, e.g. materials for the glass-contacting layers
- C03B2215/22—Non-oxide ceramics
Landscapes
- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Manufacturing & Machinery (AREA)
- Inorganic Chemistry (AREA)
- Re-Forming, After-Treatment, Cutting And Transporting Of Glass Products (AREA)
- Surface Treatment Of Glass (AREA)
- Cleaning By Liquid Or Steam (AREA)
- Glass Compositions (AREA)
Applications Claiming Priority (3)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| US201161563192P | 2011-11-23 | 2011-11-23 | |
| US61/563,192 | 2011-11-23 | ||
| PCT/US2012/064914 WO2013078038A1 (en) | 2011-11-23 | 2012-11-14 | Reconditioning glass - forming molds having a surface oxidized titanium -aluminum -nitride glass release coating |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20140143738A true KR20140143738A (ko) | 2014-12-17 |
Family
ID=47279060
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1020147017203A Withdrawn KR20140143738A (ko) | 2011-11-23 | 2012-11-14 | 표면 산화된 티타늄-알루미늄-질화물 유리 이형 코팅을 구비한 재생 유리-형성 몰드 |
Country Status (6)
| Country | Link |
|---|---|
| US (1) | US20130125590A1 (enExample) |
| JP (1) | JP6023818B2 (enExample) |
| KR (1) | KR20140143738A (enExample) |
| CN (1) | CN105102383A (enExample) |
| TW (1) | TWI549917B (enExample) |
| WO (1) | WO2013078038A1 (enExample) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180016173A (ko) * | 2016-08-05 | 2018-02-14 | 엘지전자 주식회사 | 3차원 형상 글래스 제조방법 |
Families Citing this family (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US20140224958A1 (en) * | 2013-02-11 | 2014-08-14 | Corning Incorporated | Coatings for glass-shaping molds and glass-shaping molds comprising the same |
| EP3116834B1 (en) | 2014-03-13 | 2021-06-02 | Corning Incorporated | Glass article and method for forming the same |
| TW201739704A (zh) * | 2016-01-20 | 2017-11-16 | 康寧公司 | 塑形玻璃基材料之具高溫用途之塗層之模具 |
| CN114605058B (zh) * | 2022-03-28 | 2024-01-26 | 维达力实业(深圳)有限公司 | 热转印模具和防眩光玻璃的制备装置 |
| CN114702235B (zh) * | 2022-03-28 | 2024-01-26 | 维达力实业(深圳)有限公司 | 防眩光玻璃及其制备方法和显示装置 |
Family Cites Families (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| US3015589A (en) * | 1959-07-16 | 1962-01-02 | Diamond Alkali Co | Chemical method |
| US3859222A (en) * | 1971-07-19 | 1975-01-07 | North American Rockwell | Silicon nitride-silicon oxide etchant |
| JP2898142B2 (ja) * | 1992-06-30 | 1999-05-31 | キヤノン株式会社 | 成形用型の再生方法 |
| DE60006176T2 (de) * | 1999-03-25 | 2004-04-22 | Central Glass Co., Ltd., Ube | Glaszusammensetzung, durch Ionenaustausch verstärkter Glasgegenstand und Verfahren zu dessen Herstellung |
| JP2001335340A (ja) * | 2000-05-23 | 2001-12-04 | Toyo Glass Co Ltd | ガラス成型用金型 |
| EP1295690A1 (en) * | 2001-05-21 | 2003-03-26 | SACMI COOPERATIVA MECCANICI IMOLA Soc. Coop. a r.l. | A process for the functional regeneration of the porosity of moulds used for moulding ceramic objects |
| EP1604757B1 (en) * | 2004-03-31 | 2008-12-24 | Konica Minolta Opto, Inc. | Manufacturing method of die for optical element molding |
| JP2009073693A (ja) * | 2007-09-20 | 2009-04-09 | Fujinon Corp | 光学素子成形用金型及びその製造方法 |
| CN101215099B (zh) * | 2008-01-16 | 2011-02-02 | 京东方科技集团股份有限公司 | 平板玻璃基板减薄蚀刻液 |
| TWI507573B (zh) * | 2010-04-15 | 2015-11-11 | Corning Inc | 剝除氮化物塗膜之方法 |
-
2012
- 2012-11-01 US US13/666,321 patent/US20130125590A1/en not_active Abandoned
- 2012-11-14 WO PCT/US2012/064914 patent/WO2013078038A1/en not_active Ceased
- 2012-11-14 KR KR1020147017203A patent/KR20140143738A/ko not_active Withdrawn
- 2012-11-14 CN CN201280057186.3A patent/CN105102383A/zh active Pending
- 2012-11-14 JP JP2014543494A patent/JP6023818B2/ja not_active Expired - Fee Related
- 2012-11-23 TW TW101143957A patent/TWI549917B/zh not_active IP Right Cessation
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| KR20180016173A (ko) * | 2016-08-05 | 2018-02-14 | 엘지전자 주식회사 | 3차원 형상 글래스 제조방법 |
Also Published As
| Publication number | Publication date |
|---|---|
| CN105102383A (zh) | 2015-11-25 |
| US20130125590A1 (en) | 2013-05-23 |
| TWI549917B (zh) | 2016-09-21 |
| TW201331144A (zh) | 2013-08-01 |
| JP6023818B2 (ja) | 2016-11-09 |
| WO2013078038A1 (en) | 2013-05-30 |
| JP2015516928A (ja) | 2015-06-18 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| PA0105 | International application |
Patent event date: 20140623 Patent event code: PA01051R01D Comment text: International Patent Application |
|
| PG1501 | Laying open of application | ||
| PC1203 | Withdrawal of no request for examination | ||
| WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |