KR20140024872A - 촉매를 사용하는 하이드록실아민의 제조 방법 - Google Patents

촉매를 사용하는 하이드록실아민의 제조 방법 Download PDF

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Publication number
KR20140024872A
KR20140024872A KR1020137027596A KR20137027596A KR20140024872A KR 20140024872 A KR20140024872 A KR 20140024872A KR 1020137027596 A KR1020137027596 A KR 1020137027596A KR 20137027596 A KR20137027596 A KR 20137027596A KR 20140024872 A KR20140024872 A KR 20140024872A
Authority
KR
South Korea
Prior art keywords
catalyst
hydroxylamine
promoter
heterogeneous hydrogenation
hydrogenation catalyst
Prior art date
Application number
KR1020137027596A
Other languages
English (en)
Korean (ko)
Inventor
매리즈케 힐드 린 그루더트
요한 토마스 틴지
루돌프 필리푸스 마리아 귀트
Original Assignee
디에스엠 아이피 어셋츠 비.브이.
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 디에스엠 아이피 어셋츠 비.브이. filed Critical 디에스엠 아이피 어셋츠 비.브이.
Publication of KR20140024872A publication Critical patent/KR20140024872A/ko

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C251/00—Compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C251/32—Oximes
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C249/00—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton
    • C07C249/04—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes
    • C07C249/08—Preparation of compounds containing nitrogen atoms doubly-bound to a carbon skeleton of oximes by reaction of hydroxylamines with carbonyl compounds
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/14—Hydroxylamine; Salts thereof
    • C01B21/1409—Preparation
    • C01B21/1418—Preparation by catalytic reduction of nitrogen oxides or nitrates with hydrogen
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D201/00—Preparation, separation, purification or stabilisation of unsubstituted lactams
    • C07D201/02—Preparation of lactams
    • C07D201/04—Preparation of lactams from or via oximes by Beckmann rearrangement
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D211/00—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings
    • C07D211/04—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D211/68—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member
    • C07D211/72—Heterocyclic compounds containing hydrogenated pyridine rings, not condensed with other rings with only hydrogen or carbon atoms directly attached to the ring nitrogen atom having one double bond between ring members or between a ring member and a non-ring member with hetero atoms or with carbon atoms having three bonds to hetero atoms, with at the most one bond to halogen, directly attached to ring carbon atoms
    • C07D211/74—Oxygen atoms
    • C07D211/76—Oxygen atoms attached in position 2 or 6
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07D—HETEROCYCLIC COMPOUNDS
    • C07D227/00—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00
    • C07D227/02—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom
    • C07D227/06—Heterocyclic compounds containing rings having one nitrogen atom as the only ring hetero atom, according to more than one of groups C07D203/00 - C07D225/00 with only hydrogen or carbon atoms directly attached to the ring nitrogen atom with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
    • C07D227/08—Oxygen atoms
    • C07D227/087—One doubly-bound oxygen atom in position 2, e.g. lactams
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/12—Systems containing only non-condensed rings with a six-membered ring
    • C07C2601/14—The ring being saturated
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C2601/00—Systems containing only non-condensed rings
    • C07C2601/18—Systems containing only non-condensed rings with a ring being at least seven-membered
    • C07C2601/20—Systems containing only non-condensed rings with a ring being at least seven-membered the ring being twelve-membered

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Catalysts (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020137027596A 2011-04-22 2012-04-16 촉매를 사용하는 하이드록실아민의 제조 방법 KR20140024872A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
EP11163583 2011-04-22
EP11163583.5 2011-04-22
PCT/EP2012/056924 WO2012143331A1 (en) 2011-04-22 2012-04-16 Catalyzed hydroxylamine preparation

Publications (1)

Publication Number Publication Date
KR20140024872A true KR20140024872A (ko) 2014-03-03

Family

ID=44209976

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020137027596A KR20140024872A (ko) 2011-04-22 2012-04-16 촉매를 사용하는 하이드록실아민의 제조 방법

Country Status (4)

Country Link
KR (1) KR20140024872A (zh)
CN (1) CN103492314B (zh)
TW (1) TW201247528A (zh)
WO (1) WO2012143331A1 (zh)

Family Cites Families (11)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
DE1767113C2 (de) * 1968-04-03 1981-10-15 Basf Ag, 6700 Ludwigshafen Verfahren zur Herstellung von Hydroxylammoniumsulfat
NL135679C (zh) 1968-11-12 1900-01-01
DE4022851A1 (de) * 1990-07-18 1992-01-23 Basf Ag Platin-graphittraeger-katalysatoren und deren verwendung
NL9201064A (nl) 1992-06-16 1994-01-17 Dsm Nv Werkwijze voor de bereiding en verwerking van een hydroxylammoniumzoutoplossing.
BE1009767A3 (nl) * 1995-11-10 1997-08-05 Dsm Nv Werkwijze voor de bereiding van hydroxylammoniumzouten.
CN1241165A (zh) * 1996-10-28 2000-01-12 Dsm有限公司 制备羟胺盐的方法
BE1010719A3 (nl) 1996-10-28 1998-12-01 Dsm Nv Werkwijze voor de bereiding van hydroxylammoniumzouten.
EP1275616A1 (en) 2001-07-11 2003-01-15 Dsm N.V. Process for the preparation of hydroxylammonium
ES2410810T5 (es) 2002-01-16 2022-02-18 Ube Industries Procesos para producir laurolactama a partir de ciclododecanona
CN101058550A (zh) * 2007-04-11 2007-10-24 巨化集团公司锦纶厂 一种丁酮肟的制备方法
CN101745392B (zh) * 2008-12-01 2012-12-26 中国石油化学工业开发股份有限公司 用于制备羟铵盐的催化剂组合物

Also Published As

Publication number Publication date
WO2012143331A1 (en) 2012-10-26
TW201247528A (en) 2012-12-01
CN103492314B (zh) 2016-09-21
CN103492314A (zh) 2014-01-01

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A201 Request for examination
E902 Notification of reason for refusal
E601 Decision to refuse application