KR20130102588A - 폴리에테르 카보네이트 폴리올의 제조방법 - Google Patents

폴리에테르 카보네이트 폴리올의 제조방법 Download PDF

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Publication number
KR20130102588A
KR20130102588A KR1020137008882A KR20137008882A KR20130102588A KR 20130102588 A KR20130102588 A KR 20130102588A KR 1020137008882 A KR1020137008882 A KR 1020137008882A KR 20137008882 A KR20137008882 A KR 20137008882A KR 20130102588 A KR20130102588 A KR 20130102588A
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KR
South Korea
Prior art keywords
mixture
zinc
catalyst
methyl
metal cyanide
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Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Ceased
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KR1020137008882A
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English (en)
Korean (ko)
Inventor
크리스토프 귀틀러
외르그 호프만
아우렐 볼프
슈테판 그라서
Original Assignee
바이엘 인텔렉쳐 프로퍼티 게엠베하
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Application filed by 바이엘 인텔렉쳐 프로퍼티 게엠베하 filed Critical 바이엘 인텔렉쳐 프로퍼티 게엠베하
Publication of KR20130102588A publication Critical patent/KR20130102588A/ko
Ceased legal-status Critical Current

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/20—General preparatory processes
    • C08G64/32—General preparatory processes using carbon dioxide
    • C08G64/34—General preparatory processes using carbon dioxide and cyclic ethers
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G64/00—Macromolecular compounds obtained by reactions forming a carbonic ester link in the main chain of the macromolecule
    • C08G64/18—Block or graft polymers
    • C08G64/183—Block or graft polymers containing polyether sequences
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2603—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds the other compounds containing oxygen
    • C—CHEMISTRY; METALLURGY
    • C08—ORGANIC MACROMOLECULAR COMPOUNDS; THEIR PREPARATION OR CHEMICAL WORKING-UP; COMPOSITIONS BASED THEREON
    • C08G—MACROMOLECULAR COMPOUNDS OBTAINED OTHERWISE THAN BY REACTIONS ONLY INVOLVING UNSATURATED CARBON-TO-CARBON BONDS
    • C08G65/00—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule
    • C08G65/02—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring
    • C08G65/26—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds
    • C08G65/2642—Macromolecular compounds obtained by reactions forming an ether link in the main chain of the macromolecule from cyclic ethers by opening of the heterocyclic ring from cyclic ethers and other compounds characterised by the catalyst used
    • C08G65/2645—Metals or compounds thereof, e.g. salts
    • C08G65/2663—Metal cyanide catalysts, i.e. DMC's

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  • Chemical & Material Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Medicinal Chemistry (AREA)
  • Polymers & Plastics (AREA)
  • Organic Chemistry (AREA)
  • Toxicology (AREA)
  • Polyesters Or Polycarbonates (AREA)
  • Polyethers (AREA)
KR1020137008882A 2010-09-09 2011-09-06 폴리에테르 카보네이트 폴리올의 제조방법 Ceased KR20130102588A (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
DE102010040517.5 2010-09-09
DE102010040517A DE102010040517A1 (de) 2010-09-09 2010-09-09 Verfahren zur Herstellung von Polyetherpolyolen
PCT/EP2011/065364 WO2012032028A1 (de) 2010-09-09 2011-09-06 Verfahren zur herstellung von polyethercarbonatpolyolen

Publications (1)

Publication Number Publication Date
KR20130102588A true KR20130102588A (ko) 2013-09-17

Family

ID=44653291

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020137008882A Ceased KR20130102588A (ko) 2010-09-09 2011-09-06 폴리에테르 카보네이트 폴리올의 제조방법

Country Status (13)

Country Link
US (1) US9045592B2 (https=)
EP (1) EP2614102B1 (https=)
JP (1) JP5792310B2 (https=)
KR (1) KR20130102588A (https=)
CN (1) CN103189417B (https=)
BR (1) BR112013005783A2 (https=)
CA (1) CA2810559A1 (https=)
DE (1) DE102010040517A1 (https=)
ES (1) ES2506440T3 (https=)
MX (1) MX2013002484A (https=)
RU (1) RU2013115633A (https=)
SG (1) SG188278A1 (https=)
WO (1) WO2012032028A1 (https=)

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20230012227A (ko) * 2021-07-15 2023-01-26 아주대학교산학협력단 하이드로젠 헥사시아노코발테이트와 아연 카복실레이트의 조합으로 제조된 더블메탈시아나이드 촉매 및 이를 이용한 프로필렌 옥사이드 중합
KR20230036995A (ko) 2021-09-08 2023-03-15 주식회사 엘지화학 이중 금속 시아나이드 촉매, 이의 제조방법 및 상기 촉매를 이용한 폴리알킬렌 카보네이트의 제조방법
KR20230046237A (ko) 2021-09-29 2023-04-05 주식회사 엘지화학 폴리알킬렌 카보네이트 수지의 제조방법

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EP2548908A1 (de) * 2011-07-18 2013-01-23 Bayer MaterialScience AG Verfahren zur Herstellung von Polyetherpolyolen
US9790328B2 (en) * 2013-06-13 2017-10-17 Covestro Deutschland Ag Polyethercarbonate-polyoxymethylene block copolymers
EP2837648A1 (en) 2013-08-12 2015-02-18 Repsol, S.A. Process for preparing polyether carbonate polyols
EP2845871A1 (de) * 2013-09-05 2015-03-11 Bayer MaterialScience AG Vernetzung von Doppelbindungen enthaltenden Polyethercarbonatpolyolen durch Addition von Mercaptanen
EP2865700A1 (de) * 2013-10-23 2015-04-29 Bayer MaterialScience AG Verfahren zur Herstellung von Polyethercarbonatpolyolen
US9527958B2 (en) 2014-05-02 2016-12-27 Covestro Llc Process for purification of polyether carbonate polyols
KR102333890B1 (ko) * 2014-07-03 2021-12-02 코베스트로 도이칠란트 아게 폴리에테르 카르보네이트 폴리올의 제조 방법
US10119223B2 (en) 2016-07-15 2018-11-06 Covestro Llc Carpet and synthetic turf backings prepared from a polyether carbonate polyol
US10040903B2 (en) 2016-09-13 2018-08-07 Covestro Llc Polymer polyol quality
EP3538588B1 (en) 2016-11-11 2023-01-25 Dow Global Technologies LLC Polycarbonate based polyols
GB201703323D0 (en) * 2017-03-01 2017-04-12 Econic Tech Ltd Method for preparing polyols
CN110964191B (zh) * 2018-09-29 2021-02-02 杭州普力材料科技有限公司 一种混合酸改性的锌钴双金属氰化物催化剂及其制备方法
CN114144451A (zh) * 2019-07-31 2022-03-04 科思创德国股份有限公司 制备聚醚碳酸酯多元醇的方法
EP4093539B1 (de) * 2020-01-21 2023-10-04 Covestro Deutschland AG Verfahren zur herstellung von doppelmetallcyanid-katalysatoren
CN114524929B (zh) * 2021-09-24 2023-07-25 山东联欣环保科技有限公司 一种二氧化碳基四元共聚物的制备方法
CN114381252B (zh) * 2022-01-19 2023-02-10 成都理工大学 一种超高温下耐多价金属阳离子无固相修井液的制备方法

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GB1063525A (en) 1963-02-14 1967-03-30 Gen Tire & Rubber Co Organic cyclic oxide polymers, their preparation and tires prepared therefrom
JP2653236B2 (ja) 1990-10-05 1997-09-17 旭硝子株式会社 ポリエーテル化合物の製造方法
US5158922A (en) 1992-02-04 1992-10-27 Arco Chemical Technology, L.P. Process for preparing metal cyanide complex catalyst
US5482908A (en) 1994-09-08 1996-01-09 Arco Chemical Technology, L.P. Highly active double metal cyanide catalysts
WO1999019063A1 (de) 1997-10-13 1999-04-22 Bayer Aktiengesellschaft Kristalline doppelmetallcyanid-katalysatoren für die herstellung von polyetherpolyolen
US6376645B1 (en) 1999-07-09 2002-04-23 The Dow Chemical Company Complexing agent-modified hexacyanometallate hexanitrometallate catalysts
DE19958355A1 (de) 1999-12-03 2001-06-07 Bayer Ag Verfahren zur Herstellung von DMC-Katalysatoren
AU2001260217A1 (en) 2000-04-20 2001-11-07 Bayer Aktiengesellschaft Method for producing double metal cyanide (dmc) catalysts
DE10122019A1 (de) 2001-05-07 2002-11-14 Bayer Ag Doppelmetallcyanid-Katalysatoren für die Herstellung von Polyetherpolyolen
DE10147712A1 (de) 2001-09-27 2003-04-17 Basf Ag Verfahren zur Herstellung aliphatischer Polycarbonate
US6762278B2 (en) 2002-02-04 2004-07-13 Basf Corporation Process for the copolymerization of alkylene oxides and carbon dioxide using suspensions of multi-metal cyanide compounds
DE10219028A1 (de) 2002-04-29 2003-11-06 Bayer Ag Herstellung und Verwendung von hochmolekularen aliphatischen Polycarbonaten
EP1562999B1 (en) 2002-11-07 2012-12-19 Dow Global Technologies LLC Method for preparing metal cyanide catalysts using polymerizable complexing agents
US7378559B2 (en) 2003-03-07 2008-05-27 Dow Global Technologies Inc. Continuous process and system of producing polyether polyols
US20050101477A1 (en) * 2003-11-07 2005-05-12 George Combs Unsaturated tertiary alcohols as ligands for active dmc catalysts
US20060223973A1 (en) 2005-03-29 2006-10-05 Basf Corporation Method of forming a polyethercarbonate polyol
US7977501B2 (en) 2006-07-24 2011-07-12 Bayer Materialscience Llc Polyether carbonate polyols made via double metal cyanide (DMC) catalysis

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
KR20230012227A (ko) * 2021-07-15 2023-01-26 아주대학교산학협력단 하이드로젠 헥사시아노코발테이트와 아연 카복실레이트의 조합으로 제조된 더블메탈시아나이드 촉매 및 이를 이용한 프로필렌 옥사이드 중합
KR20230036995A (ko) 2021-09-08 2023-03-15 주식회사 엘지화학 이중 금속 시아나이드 촉매, 이의 제조방법 및 상기 촉매를 이용한 폴리알킬렌 카보네이트의 제조방법
WO2023038406A1 (ko) 2021-09-08 2023-03-16 주식회사 엘지화학 이중 금속 시아나이드 촉매, 이의 제조방법 및 상기 촉매를 이용한 폴리알킬렌 카보네이트의 제조방법
KR20230046237A (ko) 2021-09-29 2023-04-05 주식회사 엘지화학 폴리알킬렌 카보네이트 수지의 제조방법
WO2023054999A1 (ko) * 2021-09-29 2023-04-06 주식회사 엘지화학 폴리알킬렌 카보네이트 수지의 제조방법
CN116848175A (zh) * 2021-09-29 2023-10-03 株式会社Lg化学 制备聚碳酸亚烷基酯树脂的方法

Also Published As

Publication number Publication date
JP2013537245A (ja) 2013-09-30
CN103189417B (zh) 2016-08-03
EP2614102B1 (de) 2014-07-23
DE102010040517A1 (de) 2012-03-15
MX2013002484A (es) 2013-04-03
JP5792310B2 (ja) 2015-10-07
ES2506440T3 (es) 2014-10-13
RU2013115633A (ru) 2014-10-20
CA2810559A1 (en) 2012-03-15
WO2012032028A1 (de) 2012-03-15
CN103189417A (zh) 2013-07-03
US9045592B2 (en) 2015-06-02
EP2614102A1 (de) 2013-07-17
US20130184432A1 (en) 2013-07-18
BR112013005783A2 (pt) 2017-03-21
SG188278A1 (en) 2013-04-30

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