KR20080105955A - 불소 치환 환상 탄산 에스테르의 제조방법 - Google Patents
불소 치환 환상 탄산 에스테르의 제조방법 Download PDFInfo
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- KR20080105955A KR20080105955A KR1020070096779A KR20070096779A KR20080105955A KR 20080105955 A KR20080105955 A KR 20080105955A KR 1020070096779 A KR1020070096779 A KR 1020070096779A KR 20070096779 A KR20070096779 A KR 20070096779A KR 20080105955 A KR20080105955 A KR 20080105955A
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- Prior art keywords
- carbonate
- fluorine
- cyclic carbonate
- substituted cyclic
- ammonium chloride
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- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07D—HETEROCYCLIC COMPOUNDS
- C07D317/00—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms
- C07D317/08—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3
- C07D317/10—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings
- C07D317/32—Heterocyclic compounds containing five-membered rings having two oxygen atoms as the only ring hetero atoms having the hetero atoms in positions 1 and 3 not condensed with other rings with hetero atoms or with carbon atoms having three bonds to hetero atoms with at the most one bond to halogen, e.g. ester or nitrile radicals, directly attached to ring carbon atoms
- C07D317/42—Halogen atoms or nitro radicals
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J27/00—Catalysts comprising the elements or compounds of halogens, sulfur, selenium, tellurium, phosphorus or nitrogen; Catalysts comprising carbon compounds
- B01J27/24—Nitrogen compounds
- B01J27/25—Nitrates
-
- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
- B01J31/00—Catalysts comprising hydrides, coordination complexes or organic compounds
- B01J31/02—Catalysts comprising hydrides, coordination complexes or organic compounds containing organic compounds or metal hydrides
- B01J31/0201—Oxygen-containing compounds
- B01J31/0204—Ethers
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/052—Li-accumulators
- H01M10/0525—Rocking-chair batteries, i.e. batteries with lithium insertion or intercalation in both electrodes; Lithium-ion batteries
-
- H—ELECTRICITY
- H01—ELECTRIC ELEMENTS
- H01M—PROCESSES OR MEANS, e.g. BATTERIES, FOR THE DIRECT CONVERSION OF CHEMICAL ENERGY INTO ELECTRICAL ENERGY
- H01M10/00—Secondary cells; Manufacture thereof
- H01M10/05—Accumulators with non-aqueous electrolyte
- H01M10/056—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes
- H01M10/0564—Accumulators with non-aqueous electrolyte characterised by the materials used as electrolytes, e.g. mixed inorganic/organic electrolytes the electrolyte being constituted of organic materials only
- H01M10/0566—Liquid materials
- H01M10/0569—Liquid materials characterised by the solvents
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- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02E—REDUCTION OF GREENHOUSE GAS [GHG] EMISSIONS, RELATED TO ENERGY GENERATION, TRANSMISSION OR DISTRIBUTION
- Y02E60/00—Enabling technologies; Technologies with a potential or indirect contribution to GHG emissions mitigation
- Y02E60/10—Energy storage using batteries
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Organic Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Materials Engineering (AREA)
- Manufacturing & Machinery (AREA)
- Electrochemistry (AREA)
- General Chemical & Material Sciences (AREA)
- Physics & Mathematics (AREA)
- Inorganic Chemistry (AREA)
- General Physics & Mathematics (AREA)
- Condensed Matter Physics & Semiconductors (AREA)
- Low-Molecular Organic Synthesis Reactions Using Catalysts (AREA)
- Catalysts (AREA)
Abstract
Description
Claims (13)
- 원료로서 염소 치환 환상 탄산 에스테르와 알칼리 금속 불화물 및 알칼리 토금속 불화물을 상 전이 촉매(phase transfer catalyst)의 존재 하에 용제 중에 반응시켜 불소 치환 환상 탄산 에스테르의 반응 혼합물을 생성하는 것을 특징으로 하는 불소 치환 환상 탄산 에스테르 제조방법.
- 제1항에 있어서, 상기 불소 치환 환상 탄산 에스테르를 포함한 반응 혼합물을 감압 정류시켜 순수한 불소 치환 환상 탄산 에스테르를 얻는 것을 특징으로 하는 제조방법.
- 제1항 또는 제2항에 있어서, 상기 용제는 디알킬 카보네이트 또는 환상 탄산 에스테르인 것을 특징으로 하는 제조방법.
- 제3항에 있어서, 상기 용제는 디메틸카보네이트, 디에틸카보네이트, 디프로필카보네이트, 메틸에틸 카보네이트, 메틸프로필 카보네이트, 에틸프로필 카보네이트, 5-헥실에틸렌 카보네이트, 에틸렌 카보네이트, 디페닐 카보네이트, 5-페닐에틸렌 카보네이트, 프로필렌 카보네이트, 페닐(메틸)페닐 카보네이트 중 하나 또는 이들의 혼합물인 것인 제조방법.
- 제1항 또는 제 2항에 있어서, 상기 상 전이 촉매는 제4 암모늄염 촉매 또는 크라운 에테르인 것을 특징으로 하는 제조방법.
- 제6항에 있어서, 상기 제4암모늄염 촉매는 브롬화 테트라메틸암모늄, 브롬화 테트라에틸암모늄, 브롬화 테트라부틸암모늄, 브롬화 테트라옥틸암모늄, 브롬화 트리옥틸메틸 암모늄, 브롬화 테트라페닐암모늄, 브롬화 트리페닐메틸 암모늄, 브롬화 벤질트리페닐 암모늄, 염화 테트라메틸 암모늄, 염화 테트라에틸 암모늄, 염화 테트라부틸 암모늄, 염화 테트라옥틸 암모늄, 염화 트리옥틸메틸 암모늄, 염화 테트라페닐 암모늄, 염화 트리페닐메틸 암모늄 및 염화 벤질트리페닐 암모늄 중 하나 또는 이들의 혼합물인 것을 특징으로 하는 제조방법.
- 제1항 또는 제2항에 있어서, 상기 알칼리 금속 불화물 또는 알칼리 토금속 불화물은 KF, LiF, NaF, MgF2, CaF2 또는 BaF2인 것을 특징으로 하는 제조방법.
- 제1항 또는 제2항에 있어서, 상기 반응을 70 ~ 150℃의 온도 범위에서 진행시키는 것을 특징으로 하는 제조방법.
- 제2항에 있어서, 상기 감압 정류의 온도범위는 40 ~ 150℃이고 진공도 범위는 0.1 ~ 200 kPa인 것을 특징으로 하는 제조방법.
- 제1항 또는 제2항에 있어서, 상기 반응원료인 염소 치환 환상 탄산 에스테르와 알칼리 금속 불화물 또는 알칼리 토금속 불화물의 몰 비율은 1:10 ~ 10:1의 범위 내에 있으며, 여기서 알칼리 금속 불화물 또는 알칼리 토금속 불화물은 불소 원자의 몰 수치로 계산하는 것을 특징으로 하는 제조방법.
Applications Claiming Priority (2)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN200710041599.3 | 2007-06-01 | ||
CNB2007100415993A CN100558721C (zh) | 2007-06-01 | 2007-06-01 | 氟代环状碳酸酯的制备方法 |
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KR20080105955A true KR20080105955A (ko) | 2008-12-04 |
KR100942901B1 KR100942901B1 (ko) | 2010-02-16 |
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KR1020070096779A KR100942901B1 (ko) | 2007-06-01 | 2007-09-21 | 불소 치환 환상 탄산 에스테르의 제조방법 |
Country Status (3)
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JP (1) | JP4789892B2 (ko) |
KR (1) | KR100942901B1 (ko) |
CN (1) | CN100558721C (ko) |
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
KR20150034771A (ko) * | 2012-08-13 | 2015-04-03 | 에이치에스씨 코포레이션 | 트리플루오로메틸 환상 탄산에스테르의 제조방법 |
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JP5135926B2 (ja) * | 2007-07-13 | 2013-02-06 | ダイキン工業株式会社 | 4−フルオロ−1,3−ジオキソラン−2−オンの製造方法 |
TW201105646A (en) * | 2009-05-28 | 2011-02-16 | Solvay Fluor Gmbh | Process for the preparation of 4-fluoro-4-R-5-R'-1,3-dioxolane-2-ones |
CN101597275B (zh) * | 2009-07-16 | 2012-05-30 | 太仓华一化工科技有限公司 | 一种氟代碳酸亚乙酯的纯化方法 |
JP5714578B2 (ja) | 2009-07-16 | 2015-05-07 | ゾルファイ フルーオル ゲゼルシャフト ミット ベシュレンクテル ハフツングSolvay Fluor GmbH | フルオロアルキル(フルオロ)アルキルカーボネートおよびカルバメートの調製方法 |
TW201121938A (en) * | 2009-09-28 | 2011-07-01 | Solvay Fluor Gmbh | Manufacture of difluoroethylene carbonate, trifluoroethylene carbonate and tetrafluoroethylene carbonate |
CN102766130A (zh) * | 2012-07-18 | 2012-11-07 | 太仓华一化工科技有限公司 | 一种二氟代碳酸乙烯酯的制备方法 |
CN103113345B (zh) * | 2013-01-21 | 2014-11-05 | 张家港瀚康化工有限公司 | 氟代碳酸乙烯酯的制备方法 |
CN104072473B (zh) * | 2014-07-08 | 2016-04-06 | 昆明合起工贸有限公司 | 一种用氟硅酸合成氟代碳酸乙烯酯的生产工艺 |
CN106916136B (zh) * | 2017-03-01 | 2019-06-14 | 山东永浩新材料科技有限公司 | 一种氟代碳酸乙烯酯的合成方法 |
CN114736185B (zh) * | 2022-04-21 | 2024-01-02 | 上海东庚化工技术有限公司 | 一种超纯氟代碳酸乙烯酯节能生产工艺及系统 |
WO2023201999A1 (zh) * | 2022-04-21 | 2023-10-26 | 上海东庚化工技术有限公司 | 一种电解液添加剂的生产方法及系统 |
CN115626907B (zh) * | 2022-11-03 | 2024-04-16 | 多氟多新材料股份有限公司 | 一种4-三氟代甲基碳酸乙烯酯的制备方法 |
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CN115772150A (zh) * | 2022-11-10 | 2023-03-10 | 广州理文科技有限公司 | 一种碳酸乙烯酯氟代衍生物的制备方法 |
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JPH09286785A (ja) * | 1996-01-10 | 1997-11-04 | Sanyo Chem Ind Ltd | 含フッ素ジオキソラン、電解液用有機溶媒、リチウム二次電池および電気二重層コンデンサ |
TW588041B (en) | 2001-12-27 | 2004-05-21 | Asahi Kasei Chemicals Corp | Method for producing a carbonic ester |
JP4848684B2 (ja) * | 2005-06-28 | 2011-12-28 | セントラル硝子株式会社 | 高純度の4−フルオロ−1,3−ジオキソラン−2−オンの製造方法 |
JP4848683B2 (ja) * | 2005-06-28 | 2011-12-28 | セントラル硝子株式会社 | 高純度の4−フルオロ−1,3−ジオキソラン−2−オンの製造方法 |
JP5061635B2 (ja) * | 2007-02-15 | 2012-10-31 | ダイキン工業株式会社 | 4−フルオロ−1,3−ジオキソラン−2−オンの製造法 |
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- 2007-06-01 CN CNB2007100415993A patent/CN100558721C/zh active Active
- 2007-09-12 JP JP2007236041A patent/JP4789892B2/ja active Active
- 2007-09-21 KR KR1020070096779A patent/KR100942901B1/ko active IP Right Grant
Cited By (1)
Publication number | Priority date | Publication date | Assignee | Title |
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KR20150034771A (ko) * | 2012-08-13 | 2015-04-03 | 에이치에스씨 코포레이션 | 트리플루오로메틸 환상 탄산에스테르의 제조방법 |
Also Published As
Publication number | Publication date |
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CN101066965A (zh) | 2007-11-07 |
JP4789892B2 (ja) | 2011-10-12 |
JP2008297299A (ja) | 2008-12-11 |
CN100558721C (zh) | 2009-11-11 |
KR100942901B1 (ko) | 2010-02-16 |
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