KR20000070888A - 헥사메틸렌디아민 및 2-아미노메틸시클로펜틸아민 함유 혼합물로부터 2-아미노메틸시클로펜틸아민의 분리 방법 - Google Patents
헥사메틸렌디아민 및 2-아미노메틸시클로펜틸아민 함유 혼합물로부터 2-아미노메틸시클로펜틸아민의 분리 방법 Download PDFInfo
- Publication number
- KR20000070888A KR20000070888A KR1019997007153A KR19997007153A KR20000070888A KR 20000070888 A KR20000070888 A KR 20000070888A KR 1019997007153 A KR1019997007153 A KR 1019997007153A KR 19997007153 A KR19997007153 A KR 19997007153A KR 20000070888 A KR20000070888 A KR 20000070888A
- Authority
- KR
- South Korea
- Prior art keywords
- aminomethylcyclopentylamine
- hexamethylenediamine
- distillation
- amcpa
- separating
- Prior art date
Links
- NAQMVNRVTILPCV-UHFFFAOYSA-N hexane-1,6-diamine Chemical compound NCCCCCCN NAQMVNRVTILPCV-UHFFFAOYSA-N 0.000 title claims abstract description 36
- 238000000034 method Methods 0.000 title claims abstract description 16
- 239000000203 mixture Substances 0.000 title claims abstract description 16
- SRGQQZYVZFJYHJ-UHFFFAOYSA-N 2-(aminomethyl)cyclopentan-1-amine Chemical compound NCC1CCCC1N SRGQQZYVZFJYHJ-UHFFFAOYSA-N 0.000 title claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 6
- 238000004821 distillation Methods 0.000 claims description 15
- 238000000926 separation method Methods 0.000 claims description 6
- 238000005984 hydrogenation reaction Methods 0.000 description 6
- 239000003054 catalyst Substances 0.000 description 5
- SSJXIUAHEKJCMH-UHFFFAOYSA-N cyclohexane-1,2-diamine Chemical compound NC1CCCCC1N SSJXIUAHEKJCMH-UHFFFAOYSA-N 0.000 description 5
- 102100028735 Dachshund homolog 1 Human genes 0.000 description 4
- 101000915055 Homo sapiens Dachshund homolog 1 Proteins 0.000 description 4
- PXHVJJICTQNCMI-UHFFFAOYSA-N Nickel Chemical compound [Ni] PXHVJJICTQNCMI-UHFFFAOYSA-N 0.000 description 4
- BTGRAWJCKBQKAO-UHFFFAOYSA-N adiponitrile Chemical compound N#CCCCCC#N BTGRAWJCKBQKAO-UHFFFAOYSA-N 0.000 description 3
- 238000009835 boiling Methods 0.000 description 3
- 238000012856 packing Methods 0.000 description 3
- KBMSFJFLSXLIDJ-UHFFFAOYSA-N 6-aminohexanenitrile Chemical compound NCCCCCC#N KBMSFJFLSXLIDJ-UHFFFAOYSA-N 0.000 description 2
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- KJTLSVCANCCWHF-UHFFFAOYSA-N Ruthenium Chemical compound [Ru] KJTLSVCANCCWHF-UHFFFAOYSA-N 0.000 description 2
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 2
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 description 2
- WNLRTRBMVRJNCN-UHFFFAOYSA-N adipic acid Chemical compound OC(=O)CCCCC(O)=O WNLRTRBMVRJNCN-UHFFFAOYSA-N 0.000 description 2
- ZSIQJIWKELUFRJ-UHFFFAOYSA-N azepane Chemical compound C1CCCNCC1 ZSIQJIWKELUFRJ-UHFFFAOYSA-N 0.000 description 2
- 239000006227 byproduct Substances 0.000 description 2
- 229910017052 cobalt Inorganic materials 0.000 description 2
- 239000010941 cobalt Substances 0.000 description 2
- GUTLYIVDDKVIGB-UHFFFAOYSA-N cobalt atom Chemical compound [Co] GUTLYIVDDKVIGB-UHFFFAOYSA-N 0.000 description 2
- 238000009833 condensation Methods 0.000 description 2
- 230000005494 condensation Effects 0.000 description 2
- 229910052751 metal Inorganic materials 0.000 description 2
- 239000002184 metal Substances 0.000 description 2
- 229910052707 ruthenium Inorganic materials 0.000 description 2
- 239000007868 Raney catalyst Substances 0.000 description 1
- 229910000564 Raney nickel Inorganic materials 0.000 description 1
- 239000001361 adipic acid Substances 0.000 description 1
- 235000011037 adipic acid Nutrition 0.000 description 1
- 238000007796 conventional method Methods 0.000 description 1
- 150000001991 dicarboxylic acids Chemical class 0.000 description 1
- 229910052742 iron Inorganic materials 0.000 description 1
- 239000000395 magnesium oxide Substances 0.000 description 1
- CPLXHLVBOLITMK-UHFFFAOYSA-N magnesium oxide Inorganic materials [Mg]=O CPLXHLVBOLITMK-UHFFFAOYSA-N 0.000 description 1
- AXZKOIWUVFPNLO-UHFFFAOYSA-N magnesium;oxygen(2-) Chemical compound [O-2].[Mg+2] AXZKOIWUVFPNLO-UHFFFAOYSA-N 0.000 description 1
- 239000000463 material Substances 0.000 description 1
- 229910052759 nickel Inorganic materials 0.000 description 1
- TWNQGVIAIRXVLR-UHFFFAOYSA-N oxo(oxoalumanyloxy)alumane Chemical compound O=[Al]O[Al]=O TWNQGVIAIRXVLR-UHFFFAOYSA-N 0.000 description 1
- 238000005192 partition Methods 0.000 description 1
- 229920000642 polymer Polymers 0.000 description 1
- 239000000047 product Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 229910052703 rhodium Inorganic materials 0.000 description 1
- 239000010948 rhodium Substances 0.000 description 1
- MHOVAHRLVXNVSD-UHFFFAOYSA-N rhodium atom Chemical compound [Rh] MHOVAHRLVXNVSD-UHFFFAOYSA-N 0.000 description 1
- 239000000377 silicon dioxide Substances 0.000 description 1
- 235000012239 silicon dioxide Nutrition 0.000 description 1
- 239000011029 spinel Substances 0.000 description 1
- 229910052596 spinel Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 239000004408 titanium dioxide Substances 0.000 description 1
Classifications
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
- C07C209/82—Purification; Separation; Stabilisation; Use of additives
- C07C209/84—Purification
-
- C—CHEMISTRY; METALLURGY
- C07—ORGANIC CHEMISTRY
- C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
- C07C2601/00—Systems containing only non-condensed rings
- C07C2601/06—Systems containing only non-condensed rings with a five-membered ring
- C07C2601/08—Systems containing only non-condensed rings with a five-membered ring the ring being saturated
Landscapes
- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| DE19704618.5 | 1997-02-07 | ||
| DE19704618A DE19704618A1 (de) | 1997-02-07 | 1997-02-07 | Verfahren zur Abtrennung von 2-Aminomethylcyclopentylamin aus einer Mischung enthaltend Hexamethylendiamin und 2-Aminomethylcyclopentylamin |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| KR20000070888A true KR20000070888A (ko) | 2000-11-25 |
Family
ID=7819570
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| KR1019997007153A KR20000070888A (ko) | 1997-02-07 | 1998-01-17 | 헥사메틸렌디아민 및 2-아미노메틸시클로펜틸아민 함유 혼합물로부터 2-아미노메틸시클로펜틸아민의 분리 방법 |
Country Status (10)
| Country | Link |
|---|---|
| EP (1) | EP0960094A1 (ja) |
| JP (1) | JP2001511163A (ja) |
| KR (1) | KR20000070888A (ja) |
| CN (1) | CN1251567A (ja) |
| AR (1) | AR011636A1 (ja) |
| AU (1) | AU6094798A (ja) |
| BR (1) | BR9807188A (ja) |
| CA (1) | CA2280830A1 (ja) |
| DE (1) | DE19704618A1 (ja) |
| WO (1) | WO1998034901A1 (ja) |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| GB731819A (en) * | 1951-04-11 | 1955-06-15 | Du Pont | Improvements in or relating to the production of hexamethylene diamine and salts thereof |
| GB1125706A (en) * | 1965-01-20 | 1968-08-28 | Ici Ltd | Process for the production of hexamethylene diamine |
| DE1543973A1 (de) * | 1966-06-08 | 1970-02-05 | Vickers Zimmer Ag | Verfahren zur Reinigung von Hexamethylendiamin |
| CA915707A (en) * | 1969-07-11 | 1972-11-28 | J. Kershaw Bernard | Hydrogenation of adiponitrile |
| SU810669A1 (ru) * | 1978-12-06 | 1981-03-07 | Предприятие П/Я В-2609 | Способ очистки гексаметилендиа-МиНА |
-
1997
- 1997-02-07 DE DE19704618A patent/DE19704618A1/de not_active Withdrawn
-
1998
- 1998-01-17 WO PCT/EP1998/000241 patent/WO1998034901A1/de not_active Application Discontinuation
- 1998-01-17 EP EP98905307A patent/EP0960094A1/de not_active Withdrawn
- 1998-01-17 JP JP53367398A patent/JP2001511163A/ja active Pending
- 1998-01-17 CA CA002280830A patent/CA2280830A1/en not_active Abandoned
- 1998-01-17 AU AU60947/98A patent/AU6094798A/en not_active Abandoned
- 1998-01-17 BR BR9807188-2A patent/BR9807188A/pt not_active Application Discontinuation
- 1998-01-17 KR KR1019997007153A patent/KR20000070888A/ko not_active Application Discontinuation
- 1998-01-17 CN CN98803807A patent/CN1251567A/zh active Pending
- 1998-02-05 AR ARP980100510A patent/AR011636A1/es unknown
Also Published As
| Publication number | Publication date |
|---|---|
| CA2280830A1 (en) | 1998-08-13 |
| AR011636A1 (es) | 2000-08-30 |
| JP2001511163A (ja) | 2001-08-07 |
| CN1251567A (zh) | 2000-04-26 |
| WO1998034901A1 (de) | 1998-08-13 |
| BR9807188A (pt) | 2000-01-25 |
| DE19704618A1 (de) | 1998-08-13 |
| AU6094798A (en) | 1998-08-26 |
| EP0960094A1 (de) | 1999-12-01 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| WITN | Application deemed withdrawn, e.g. because no request for examination was filed or no examination fee was paid |