KR102629781B1 - A method of manufacturing eco-friendly plant nutritional supplements to prevent cold and cold damage - Google Patents
A method of manufacturing eco-friendly plant nutritional supplements to prevent cold and cold damage Download PDFInfo
- Publication number
- KR102629781B1 KR102629781B1 KR1020230079795A KR20230079795A KR102629781B1 KR 102629781 B1 KR102629781 B1 KR 102629781B1 KR 1020230079795 A KR1020230079795 A KR 1020230079795A KR 20230079795 A KR20230079795 A KR 20230079795A KR 102629781 B1 KR102629781 B1 KR 102629781B1
- Authority
- KR
- South Korea
- Prior art keywords
- extract
- mixture
- wax
- soybean oil
- plant
- Prior art date
Links
- 230000002595 cold damage Effects 0.000 title claims description 24
- 238000004519 manufacturing process Methods 0.000 title claims description 14
- 235000015872 dietary supplement Nutrition 0.000 title 1
- 241000196324 Embryophyta Species 0.000 claims abstract description 36
- 239000003549 soybean oil Substances 0.000 claims abstract description 33
- 235000012424 soybean oil Nutrition 0.000 claims abstract description 33
- 235000015097 nutrients Nutrition 0.000 claims abstract description 21
- WQZGKKKJIJFFOK-GASJEMHNSA-N Glucose Natural products OC[C@H]1OC(O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-GASJEMHNSA-N 0.000 claims abstract description 15
- 239000008103 glucose Substances 0.000 claims abstract description 15
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 15
- ZOXJGFHDIHLPTG-UHFFFAOYSA-N Boron Chemical compound [B] ZOXJGFHDIHLPTG-UHFFFAOYSA-N 0.000 claims abstract description 4
- HCHKCACWOHOZIP-UHFFFAOYSA-N Zinc Chemical compound [Zn] HCHKCACWOHOZIP-UHFFFAOYSA-N 0.000 claims abstract description 4
- 229910052796 boron Inorganic materials 0.000 claims abstract description 4
- 239000011701 zinc Substances 0.000 claims abstract description 4
- 229910052725 zinc Inorganic materials 0.000 claims abstract description 4
- 239000000203 mixture Substances 0.000 claims description 47
- 239000000284 extract Substances 0.000 claims description 24
- 239000000077 insect repellent Substances 0.000 claims description 23
- 239000000419 plant extract Substances 0.000 claims description 21
- 230000002708 enhancing effect Effects 0.000 claims description 18
- 230000009746 freeze damage Effects 0.000 claims description 16
- 239000001993 wax Substances 0.000 claims description 16
- 244000068988 Glycine max Species 0.000 claims description 15
- 235000010469 Glycine max Nutrition 0.000 claims description 15
- 239000003995 emulsifying agent Substances 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 13
- 239000008213 purified water Substances 0.000 claims description 13
- 238000002156 mixing Methods 0.000 claims description 11
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 10
- 238000003756 stirring Methods 0.000 claims description 10
- 230000008569 process Effects 0.000 claims description 9
- NBIIXXVUZAFLBC-UHFFFAOYSA-N Phosphoric acid Chemical compound OP(O)(O)=O NBIIXXVUZAFLBC-UHFFFAOYSA-N 0.000 claims description 8
- WQZGKKKJIJFFOK-VFUOTHLCSA-N beta-D-glucose Chemical compound OC[C@H]1O[C@@H](O)[C@H](O)[C@@H](O)[C@@H]1O WQZGKKKJIJFFOK-VFUOTHLCSA-N 0.000 claims description 7
- 238000005516 engineering process Methods 0.000 claims description 7
- 238000000605 extraction Methods 0.000 claims description 7
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 claims description 6
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims description 6
- YMWUJEATGCHHMB-UHFFFAOYSA-N Dichloromethane Chemical compound ClCCl YMWUJEATGCHHMB-UHFFFAOYSA-N 0.000 claims description 6
- XEKOWRVHYACXOJ-UHFFFAOYSA-N Ethyl acetate Chemical compound CCOC(C)=O XEKOWRVHYACXOJ-UHFFFAOYSA-N 0.000 claims description 6
- OKKJLVBELUTLKV-UHFFFAOYSA-N Methanol Chemical compound OC OKKJLVBELUTLKV-UHFFFAOYSA-N 0.000 claims description 6
- 239000000843 powder Substances 0.000 claims description 6
- 239000011550 stock solution Substances 0.000 claims description 6
- 238000000194 supercritical-fluid extraction Methods 0.000 claims description 6
- 239000001569 carbon dioxide Substances 0.000 claims description 5
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 5
- 239000000243 solution Substances 0.000 claims description 5
- HEDRZPFGACZZDS-UHFFFAOYSA-N Chloroform Chemical compound ClC(Cl)Cl HEDRZPFGACZZDS-UHFFFAOYSA-N 0.000 claims description 4
- 244000223760 Cinnamomum zeylanicum Species 0.000 claims description 4
- RTZKZFJDLAIYFH-UHFFFAOYSA-N Diethyl ether Chemical compound CCOCC RTZKZFJDLAIYFH-UHFFFAOYSA-N 0.000 claims description 4
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims description 4
- 240000001549 Ipomoea eriocarpa Species 0.000 claims description 4
- 235000005146 Ipomoea eriocarpa Nutrition 0.000 claims description 4
- KFZMGEQAYNKOFK-UHFFFAOYSA-N Isopropanol Chemical compound CC(C)O KFZMGEQAYNKOFK-UHFFFAOYSA-N 0.000 claims description 4
- LRHPLDYGYMQRHN-UHFFFAOYSA-N N-Butanol Chemical compound CCCCO LRHPLDYGYMQRHN-UHFFFAOYSA-N 0.000 claims description 4
- 235000005035 Panax pseudoginseng ssp. pseudoginseng Nutrition 0.000 claims description 4
- 235000003140 Panax quinquefolius Nutrition 0.000 claims description 4
- 229910000147 aluminium phosphate Inorganic materials 0.000 claims description 4
- 235000017803 cinnamon Nutrition 0.000 claims description 4
- 235000014113 dietary fatty acids Nutrition 0.000 claims description 4
- 239000000194 fatty acid Substances 0.000 claims description 4
- 229930195729 fatty acid Natural products 0.000 claims description 4
- 150000004665 fatty acids Chemical class 0.000 claims description 4
- 235000008434 ginseng Nutrition 0.000 claims description 4
- 239000004922 lacquer Substances 0.000 claims description 4
- VLKZOEOYAKHREP-UHFFFAOYSA-N n-Hexane Chemical compound CCCCCC VLKZOEOYAKHREP-UHFFFAOYSA-N 0.000 claims description 4
- 244000236658 Paeonia lactiflora Species 0.000 claims description 3
- 235000008598 Paeonia lactiflora Nutrition 0.000 claims description 3
- ZLMJMSJWJFRBEC-UHFFFAOYSA-N Potassium Chemical compound [K] ZLMJMSJWJFRBEC-UHFFFAOYSA-N 0.000 claims description 3
- 244000018633 Prunus armeniaca Species 0.000 claims description 3
- 235000009827 Prunus armeniaca Nutrition 0.000 claims description 3
- 240000001417 Vigna umbellata Species 0.000 claims description 3
- 235000011453 Vigna umbellata Nutrition 0.000 claims description 3
- 239000011591 potassium Substances 0.000 claims description 3
- 229910052700 potassium Inorganic materials 0.000 claims description 3
- 239000002904 solvent Substances 0.000 claims description 3
- 244000060011 Cocos nucifera Species 0.000 claims description 2
- 235000013162 Cocos nucifera Nutrition 0.000 claims description 2
- XDTMQSROBMDMFD-UHFFFAOYSA-N Cyclohexane Chemical compound C1CCCCC1 XDTMQSROBMDMFD-UHFFFAOYSA-N 0.000 claims description 2
- 235000021307 Triticum Nutrition 0.000 claims description 2
- 244000098338 Triticum aestivum Species 0.000 claims description 2
- 244000273928 Zingiber officinale Species 0.000 claims description 2
- 235000006886 Zingiber officinale Nutrition 0.000 claims description 2
- 239000012164 animal wax Substances 0.000 claims description 2
- 229940069765 bean extract Drugs 0.000 claims description 2
- 235000020230 cinnamon extract Nutrition 0.000 claims description 2
- 229940007062 eucalyptus extract Drugs 0.000 claims description 2
- 235000008397 ginger Nutrition 0.000 claims description 2
- 229940002508 ginger extract Drugs 0.000 claims description 2
- 235000020708 ginger extract Nutrition 0.000 claims description 2
- 235000020710 ginseng extract Nutrition 0.000 claims description 2
- 238000010438 heat treatment Methods 0.000 claims description 2
- ZGEGCLOFRBLKSE-UHFFFAOYSA-N methylene hexane Natural products CCCCCC=C ZGEGCLOFRBLKSE-UHFFFAOYSA-N 0.000 claims description 2
- WPHGSKGZRAQSGP-UHFFFAOYSA-N methylenecyclohexane Natural products C1CCCC2CC21 WPHGSKGZRAQSGP-UHFFFAOYSA-N 0.000 claims description 2
- 239000012169 petroleum derived wax Substances 0.000 claims description 2
- 235000019381 petroleum wax Nutrition 0.000 claims description 2
- BDERNNFJNOPAEC-UHFFFAOYSA-N propan-1-ol Chemical compound CCCO BDERNNFJNOPAEC-UHFFFAOYSA-N 0.000 claims description 2
- 239000002994 raw material Substances 0.000 claims description 2
- 239000012178 vegetable wax Substances 0.000 claims description 2
- 238000005728 strengthening Methods 0.000 claims 3
- 240000001822 Ilex glabra Species 0.000 claims 2
- 235000001932 Ilex glabra Nutrition 0.000 claims 2
- 241001107116 Castanospermum australe Species 0.000 claims 1
- 240000007817 Olea europaea Species 0.000 claims 1
- 240000001439 Opuntia Species 0.000 claims 1
- 235000013389 Opuntia humifusa var. humifusa Nutrition 0.000 claims 1
- 244000131316 Panax pseudoginseng Species 0.000 claims 1
- 235000021279 black bean Nutrition 0.000 claims 1
- 238000005868 electrolysis reaction Methods 0.000 claims 1
- 235000001459 whitebark Nutrition 0.000 claims 1
- 235000013399 edible fruits Nutrition 0.000 abstract description 12
- 230000000694 effects Effects 0.000 abstract description 11
- 241000607479 Yersinia pestis Species 0.000 abstract description 10
- 230000006378 damage Effects 0.000 abstract description 8
- 230000012010 growth Effects 0.000 abstract description 7
- 238000007710 freezing Methods 0.000 abstract description 4
- 230000001737 promoting effect Effects 0.000 abstract description 4
- 230000020477 pH reduction Effects 0.000 abstract description 3
- 239000012188 paraffin wax Substances 0.000 abstract description 3
- 239000002689 soil Substances 0.000 abstract description 3
- 230000008014 freezing Effects 0.000 abstract description 2
- LWIHDJKSTIGBAC-UHFFFAOYSA-K tripotassium phosphate Chemical compound [K+].[K+].[K+].[O-]P([O-])([O-])=O LWIHDJKSTIGBAC-UHFFFAOYSA-K 0.000 abstract 2
- 229910000160 potassium phosphate Inorganic materials 0.000 abstract 1
- 235000011009 potassium phosphates Nutrition 0.000 abstract 1
- 229910001868 water Inorganic materials 0.000 abstract 1
- 244000052769 pathogen Species 0.000 description 4
- 240000004371 Panax ginseng Species 0.000 description 3
- 230000005094 fruit set Effects 0.000 description 3
- 239000007788 liquid Substances 0.000 description 3
- 239000003921 oil Substances 0.000 description 3
- 235000019198 oils Nutrition 0.000 description 3
- 230000008635 plant growth Effects 0.000 description 3
- IIZPXYDJLKNOIY-JXPKJXOSSA-N 1-palmitoyl-2-arachidonoyl-sn-glycero-3-phosphocholine Chemical compound CCCCCCCCCCCCCCCC(=O)OC[C@H](COP([O-])(=O)OCC[N+](C)(C)C)OC(=O)CCC\C=C/C\C=C/C\C=C/C\C=C/CCCCC IIZPXYDJLKNOIY-JXPKJXOSSA-N 0.000 description 2
- 241000238631 Hexapoda Species 0.000 description 2
- 244000046052 Phaseolus vulgaris Species 0.000 description 2
- 235000010627 Phaseolus vulgaris Nutrition 0.000 description 2
- 235000006040 Prunus persica var persica Nutrition 0.000 description 2
- 240000004460 Tanacetum coccineum Species 0.000 description 2
- ROVGZAWFACYCSP-MQBLHHJJSA-N [2-methyl-4-oxo-3-[(2z)-penta-2,4-dienyl]cyclopent-2-en-1-yl] (1r,3r)-2,2-dimethyl-3-(2-methylprop-1-enyl)cyclopropane-1-carboxylate Chemical compound CC1(C)[C@H](C=C(C)C)[C@H]1C(=O)OC1C(C)=C(C\C=C/C=C)C(=O)C1 ROVGZAWFACYCSP-MQBLHHJJSA-N 0.000 description 2
- 230000000895 acaricidal effect Effects 0.000 description 2
- 239000002671 adjuvant Substances 0.000 description 2
- 230000000903 blocking effect Effects 0.000 description 2
- 230000000749 insecticidal effect Effects 0.000 description 2
- 239000000787 lecithin Substances 0.000 description 2
- 229940067606 lecithin Drugs 0.000 description 2
- 235000010445 lecithin Nutrition 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- 230000007721 medicinal effect Effects 0.000 description 2
- 238000009931 pascalization Methods 0.000 description 2
- 102000004169 proteins and genes Human genes 0.000 description 2
- 108090000623 proteins and genes Proteins 0.000 description 2
- 229940015367 pyrethrum Drugs 0.000 description 2
- 238000003860 storage Methods 0.000 description 2
- 241000238876 Acari Species 0.000 description 1
- 229920001817 Agar Polymers 0.000 description 1
- 240000002234 Allium sativum Species 0.000 description 1
- 244000144730 Amygdalus persica Species 0.000 description 1
- 235000003261 Artemisia vulgaris Nutrition 0.000 description 1
- 240000006891 Artemisia vulgaris Species 0.000 description 1
- 241000233866 Fungi Species 0.000 description 1
- 244000194101 Ginkgo biloba Species 0.000 description 1
- 235000008100 Ginkgo biloba Nutrition 0.000 description 1
- 244000299452 Gouania lupuloides Species 0.000 description 1
- 235000000292 Gouania lupuloides Nutrition 0.000 description 1
- 244000070406 Malus silvestris Species 0.000 description 1
- 241000207836 Olea <angiosperm> Species 0.000 description 1
- 241000736199 Paeonia Species 0.000 description 1
- 235000006484 Paeonia officinalis Nutrition 0.000 description 1
- 240000005809 Prunus persica Species 0.000 description 1
- 241000220324 Pyrus Species 0.000 description 1
- 241000219784 Sophora Species 0.000 description 1
- 241000700605 Viruses Species 0.000 description 1
- 230000002159 abnormal effect Effects 0.000 description 1
- 238000009825 accumulation Methods 0.000 description 1
- 239000000654 additive Substances 0.000 description 1
- 239000008272 agar Substances 0.000 description 1
- 239000003963 antioxidant agent Substances 0.000 description 1
- 235000021016 apples Nutrition 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 230000005779 cell damage Effects 0.000 description 1
- 239000012141 concentrate Substances 0.000 description 1
- 230000001276 controlling effect Effects 0.000 description 1
- 238000001816 cooling Methods 0.000 description 1
- 238000012272 crop production Methods 0.000 description 1
- 239000013078 crystal Substances 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000018044 dehydration Effects 0.000 description 1
- 238000006297 dehydration reaction Methods 0.000 description 1
- 238000004925 denaturation Methods 0.000 description 1
- 230000036425 denaturation Effects 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000009826 distribution Methods 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000004064 dysfunction Effects 0.000 description 1
- 235000013601 eggs Nutrition 0.000 description 1
- 239000000839 emulsion Substances 0.000 description 1
- 238000003912 environmental pollution Methods 0.000 description 1
- 230000004720 fertilization Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 239000000417 fungicide Substances 0.000 description 1
- 235000004611 garlic Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 230000007774 longterm Effects 0.000 description 1
- 239000012528 membrane Substances 0.000 description 1
- 230000004060 metabolic process Effects 0.000 description 1
- 230000037323 metabolic rate Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- OAQWWRSICWQQSE-UHFFFAOYSA-N octan-2-yl 16-methylheptadecanoate Chemical compound CCCCCCC(C)OC(=O)CCCCCCCCCCCCCCC(C)C OAQWWRSICWQQSE-UHFFFAOYSA-N 0.000 description 1
- 210000000056 organ Anatomy 0.000 description 1
- 235000021017 pears Nutrition 0.000 description 1
- 230000000149 penetrating effect Effects 0.000 description 1
- 239000000575 pesticide Substances 0.000 description 1
- 230000001766 physiological effect Effects 0.000 description 1
- 238000007670 refining Methods 0.000 description 1
- 239000005871 repellent Substances 0.000 description 1
- 230000002940 repellent Effects 0.000 description 1
- 230000000241 respiratory effect Effects 0.000 description 1
- 230000004044 response Effects 0.000 description 1
- 239000000779 smoke Substances 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 230000009466 transformation Effects 0.000 description 1
- 235000015112 vegetable and seed oil Nutrition 0.000 description 1
- 239000008158 vegetable oil Substances 0.000 description 1
- 230000017260 vegetative to reproductive phase transition of meristem Effects 0.000 description 1
- 235000021419 vinegar Nutrition 0.000 description 1
- 239000000052 vinegar Substances 0.000 description 1
Classifications
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/20—Fabaceae or Leguminosae [Pea or Legume family], e.g. pea, lentil, soybean, clover, acacia, honey locust, derris or millettia
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/02—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests containing liquids as carriers, diluents or solvents
- A01N25/04—Dispersions, emulsions, suspoemulsions, suspension concentrates or gels
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N25/00—Biocides, pest repellants or attractants, or plant growth regulators, characterised by their forms, or by their non-active ingredients or by their methods of application, e.g. seed treatment or sequential application; Substances for reducing the noxious effect of the active ingredients to organisms other than pests
- A01N25/12—Powders or granules
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/12—Asteraceae or Compositae [Aster or Sunflower family], e.g. daisy, pyrethrum, artichoke, lettuce, sunflower, wormwood or tarragon
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/24—Lauraceae [Laurel family], e.g. laurel, avocado, sassafras, cinnamon or camphor
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/08—Magnoliopsida [dicotyledons]
- A01N65/34—Rosaceae [Rose family], e.g. strawberry, hawthorn, plum, cherry, peach, apricot or almond
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N65/00—Biocides, pest repellants or attractants, or plant growth regulators containing material from algae, lichens, bryophyta, multi-cellular fungi or plants, or extracts thereof
- A01N65/40—Liliopsida [monocotyledons]
- A01N65/48—Zingiberaceae [Ginger family], e.g. ginger or galangal
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01P—BIOCIDAL, PEST REPELLANT, PEST ATTRACTANT OR PLANT GROWTH REGULATORY ACTIVITY OF CHEMICAL COMPOUNDS OR PREPARATIONS
- A01P21/00—Plant growth regulators
-
- A—HUMAN NECESSITIES
- A01—AGRICULTURE; FORESTRY; ANIMAL HUSBANDRY; HUNTING; TRAPPING; FISHING
- A01N—PRESERVATION OF BODIES OF HUMANS OR ANIMALS OR PLANTS OR PARTS THEREOF; BIOCIDES, e.g. AS DISINFECTANTS, AS PESTICIDES OR AS HERBICIDES; PEST REPELLANTS OR ATTRACTANTS; PLANT GROWTH REGULATORS
- A01N2300/00—Combinations or mixtures of active ingredients covered by classes A01N27/00 - A01N65/48 with other active or formulation relevant ingredients, e.g. specific carrier materials or surfactants, covered by classes A01N25/00 - A01N65/48
Landscapes
- Life Sciences & Earth Sciences (AREA)
- Health & Medical Sciences (AREA)
- General Health & Medical Sciences (AREA)
- Engineering & Computer Science (AREA)
- Natural Medicines & Medicinal Plants (AREA)
- Wood Science & Technology (AREA)
- Environmental Sciences (AREA)
- Zoology (AREA)
- Plant Pathology (AREA)
- Agronomy & Crop Science (AREA)
- Dentistry (AREA)
- Biotechnology (AREA)
- Mycology (AREA)
- Microbiology (AREA)
- Pest Control & Pesticides (AREA)
- Chemical & Material Sciences (AREA)
- Toxicology (AREA)
- Botany (AREA)
- Dispersion Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
본 발명은 냉동해 방지용 식물 영양제에 관한 것으로서, 대두유와 파라핀 왁스, 포도당, 물, 인산가리, 붕소 및 아연을 포함하는 것을 기술적 특징으로 하며, 냉동해 방지 효과 뿐만 아니라 생육촉진, 과실의 당도 증가, 과실의 경도 증가, 과실의 저장성 증가 및 토양 산성화를 예방하는 동시에 해충 방제 효과를 제공한다.The present invention relates to a plant nutrient for preventing freezing damage, and has the technical characteristics of containing soybean oil, paraffin wax, glucose, water, potassium phosphate, boron and zinc, and has not only an anti-freezing effect, but also promoting growth, increasing the sugar content of fruit, It increases fruit hardness, increases fruit storability, and prevents soil acidification while providing pest control effects.
Description
본 발명은 냉해 및 동해 예방용 친환경 식물 영양제 제조방법에 관한 것으로, 더욱 상세하게는 식물 과실 및 착과율 증대에 중대한 역할을 하는 꽃봉우리의 냉해를 보다 적극적이고 효율적으로 방지하여 주고, 식물세포가 더욱 완벽하게 보호되며, 여기에 식물에 각종 영양소를 공급하여 줌으로써 식물생장을 촉진시키는 동시에, 해충 방제시 보조제로 사용 가능한 여러가지 기능이 동시에 발휘되는 냉해 및 동해 예방용 친환경 식물 영양제 제조방법에 관한 것이다.The present invention relates to a method for manufacturing an eco-friendly plant nutrient for preventing cold and freeze damage. More specifically, it more actively and efficiently prevents cold damage to plant fruits and flower buds, which play a significant role in increasing the fruit set rate, and makes plant cells more perfect. It relates to a method of manufacturing an eco-friendly plant nutrient for preventing cold damage and freeze damage, which promotes plant growth by supplying various nutrients to plants and simultaneously exerts various functions that can be used as an adjuvant for pest control.
최근 우리나라는 이른 봄 개화기의 급격한 기온하강으로 인해 일교차가 크고, 여름철 장마기의 불규칙적인 강우와 폭염 등 이상기후로 인하여 농작물 재배시 예측할 수 없는 환경들이 자주 생기게 된다.Recently, in Korea, the daily temperature difference is large due to a rapid drop in temperature during the flowering season in early spring, and abnormal climates such as irregular rainfall and heat waves during the summer rainy season often create unpredictable environments when growing crops.
일반적으로 작물은 일시적인 저온이라도 생육이 거의 멈추게 되기 때문에 작물 생육에 피해가 발생하게 된다. In general, damage to crop growth occurs because crop growth almost stops even at temporarily low temperatures.
사과, 배, 복숭아 등 과수는 봄에 꽃이 핀 후 수정이 이루어져 열매가 생기게 되는데 이 시기에 아침 온도가 급격히 하락하거나 낮의 온도가 급격히 올라갈 경우 암술이 온도 차이에 의한 스트레스를 받아 기능을 나타내지 못하여 인공으로 꽃가루 접종을 하여도 수정이 되지 않아 착과율이 급격히 저하된다.Fruit trees such as apples, pears, and peaches flower in the spring and then fertilize to produce fruit. If the morning temperature drops sharply or the daytime temperature rises sharply during this period, the pistil is stressed by the temperature difference and cannot function. Even if pollen is artificially inoculated, fertilization does not occur and the fruit set rate decreases sharply.
냉해 조건은 잠재적으로 성장기를 제한하고 생산량과 생산율에 영향을 주는 작물 생산의 영향인자 중의 하나이며, 냉해조건에서 세포는 삼투현상에 의하여 세포의 얼음 결정체가 형성되어 수분을 잃게 되며, 이러한 냉각-유도 탈수는 단백질 변성, 항산화제의 축적 및 막 기능장애를 포함하는 세포 손상을 초래한다.Cold conditions are one of the influencing factors in crop production that potentially limit the growing season and affect production and production rates. Under cold conditions, cells lose moisture through osmosis through the formation of ice crystals in the cells, and this cooling-induced Dehydration results in cellular damage, including protein denaturation, accumulation of antioxidants, and membrane dysfunction.
식물들은 저온에 서 생존하는 능력이 크게 변화되고, 따라서 식물의 지리적 분포에 있어 성장에 제한을 받게 된다.Plants' ability to survive at low temperatures is greatly altered, thus limiting their growth and geographical distribution.
또한, 봄철 꽃샘 추위에 의한 냉해 및 동해는 대부분 밤에 -1℃ 내지 -5℃에서 심하게 일어나는데, 산간지역과 같이 지역에 따라 갑작스럽게 온도가 떨어지면 피할 수 있는 대책이 없어 작물의 냉해 및 동해로 인한 손해가 매우 큰 상태이다.In addition, cold and freeze damage caused by the cold in the spring most often occur at -1℃ to -5℃ at night, and there are no measures to avoid sudden temperature drops depending on the region, such as mountainous areas, resulting in cold and freeze damage to crops. The damage is very serious.
따라서, 이와 같은 냉해를 방지하기 위해서 여러개의 특허들이 안출된 것들이 있으나 이 들은 그 제조방법이 매우 복잡하고, 제조단가가 매우 비싼 등의 여러가지 문제점이 있었다.Accordingly, several patents have been developed to prevent such cold damage, but these have various problems such as the manufacturing method is very complicated and the manufacturing cost is very expensive.
본 발명은 상기와 같은 제반 문제점을 해소하기 위해 안출된 것으로서,The present invention was devised to solve the above-mentioned problems,
농작물의 착과율 증대에 중대한 역할을 하는 꽃봉우리의 냉해를 보다 적극적일고 효율적으로 방지하여 주고, 식물세포가 더욱 완벽하게 보호되며, 여기에 식물에 각종 영양소를 공급하여 줌으로써 식물생장을 촉진시켜 주는 등의 여러 가지 기능이 동시에 발휘되는 냉해 및 동해 예방용 친환경 식물 영양제를 제공함으로써, 결과적으로 농가수익을 촉진시켜 줄 수 있다.It more actively and efficiently prevents cold damage to flower buds, which plays a significant role in increasing the fruit set rate of crops, protects plant cells more completely, and promotes plant growth by supplying various nutrients to plants. By providing eco-friendly plant nutrients to prevent cold and freeze damage that perform multiple functions at the same time, it can ultimately promote farm profits.
본 발명의 바람직한 실시예에 따른 냉해 및 동해 예방용 친환경 식물 영양제의 제조방법은 대두유, 천연 유화제, 정제수, 방충기능 강화용 식물추출물, 포도당 및 왁스를 준비하는 단계(A), 상기 (A)단계에서 준비한 대두유, 천연유화제, 정제수, 포도당 및 왁스를 혼합하여 혼합물을 제조하는 단계(B), 상기 (B)단계에서 제조한 혼합물에 방충기능 강화용 식물 추출물 원액을 첨가하고 혼합 후 교반하여 혼합물을 제조하는 단계(C) 및 (C)단계에서 제조된 혼합물을 농축기에 넣어 농축하는 단계(D)가 포함된다.The method for producing an eco-friendly plant nutrient for preventing cold damage and freeze damage according to a preferred embodiment of the present invention includes preparing soybean oil, natural emulsifier, purified water, plant extract for enhancing insect repellent function, glucose, and wax, step (A). Step (B) of preparing a mixture by mixing soybean oil, natural emulsifier, purified water, glucose, and wax prepared in step (B), adding the plant extract stock solution for enhancing insect repellent function to the mixture prepared in step (B), mixing, and stirring to form the mixture. It includes a step (D) of concentrating the mixture prepared in steps (C) and (C) in a concentrator.
본 발명에서의 방충대상은 병해충, 병원균 또는 곰팡이 중 적어도 어느 하나가 포함되도록 하는 것을 특징으로 한다. The insect control target in the present invention is characterized in that it includes at least one of pests, pathogens, or mold.
또한, 본 발명의 방제대상이 병해충인 살충제에는 제충국, 고삼 및 자리공의 추출물을 첨가하고, 그 방제대상이 병원균인 방충제에는 자리공, 계피, 은행잎의 추출물을 첨가하며, 상기 방충대상이 곰팡이인 곰팡이제거제에는 인진쑥, 계피, 마늘의 추출물과 식초를 첨가하는 것을 특징으로 한다. In addition, extracts of pyrethrum, sophora ginseng, and ginseng are added to the insecticide whose control target is pests of the present invention, and extracts of pyrethrum, cinnamon, and ginkgo biloba are added to the insect repellent whose control target is pathogens, and fungicides whose target is fungi. It is characterized by adding extracts of mugwort, cinnamon, garlic, and vinegar.
아울러, 본 발명의 액성 조성물은 동해 및 냉해 효과를 제공하기 위해 대두유, 수용성 파라핀 왁스, 포도당, 인산, 가리, 붕소, 아연 및 식물추출물을 포함한다. In addition, the liquid composition of the present invention contains soybean oil, water-soluble paraffin wax, glucose, phosphoric acid, potassium, boron, zinc, and plant extracts to provide anti-freezing and freezing effects.
상기 대두유의 경우 초고압 가공를 통해 대두 내부의 지방 추출 수율을 효율적으로 증가시켜 냉해 및 동해 예방용 친환경 액성 조성물의 유막이 수분차단 효과를 증가시키고 있으며, In the case of soybean oil, ultra-high pressure processing efficiently increases the yield of fat extraction inside soybeans, and the oil film of the eco-friendly liquid composition for preventing cold damage and freeze damage increases the moisture blocking effect,
상기 파라핀 왁스는 냉해 및 동해 예방용 친환경 액성 조성물의 피막 강도를 증가시켜 외부 냉기를 차단하는 효과를 제공한다. The paraffin wax provides the effect of blocking external cold air by increasing the film strength of the eco-friendly liquid composition for preventing cold damage and freeze damage.
아울러 상기 포도당, 인산, 가리의 경우 생리 활성도 및 기초 대사량을 증가시켜 식물의 성장을 촉진하는 효과를 제공한다. In addition, the glucose, phosphoric acid, and garri increase physiological activity and basal metabolic rate, thereby promoting plant growth.
본 발명에 의하면,고난도의 숙련기술을 필요로 하지 않으면서도 동해 및 냉해 예방 효과를 제공할 수 있다.According to the present invention, it is possible to provide the effect of preventing frost damage and cold damage without requiring advanced skills.
또한, 본 발명에 따른 냉해 및 동해 예방용 친환경 식물 영양제는 냉해방지 효과 뿐만 아니라 생육촉진, 과실의 당도 증가, 과실의 경도 증가, 과실의 저장성 증가 및 토양산성화를 예방할 수 있는 효과가 있다.In addition, the eco-friendly plant nutrient for preventing cold damage and freeze damage according to the present invention has the effect of not only preventing cold damage, but also promoting growth, increasing the sugar content of fruit, increasing fruit hardness, increasing fruit storage, and preventing soil acidification.
도 1은 본 발명의 냉해 및 동해 예방용 친환경 식물 영양제 제조방법의 공정 단계를 도시한 도시도이다.
Figure 1 is a diagram showing the process steps of the method of manufacturing an eco-friendly plant nutrient for preventing cold damage and frost damage of the present invention.
이하, 첨부된 도면을 참조하여 본 발명을 상세히 설명한다.Hereinafter, the present invention will be described in detail with reference to the attached drawings.
하기에서 본 발명을 설명함에 있어서 공지 기능 또는 구성에 대한 구체적인 설명이 본 발명의 요지를 불필요하게 흐릴 수 있다고 판단되는 경우에는 그 상세한 설명을 생략할 것이다.In the following description of the present invention, if a detailed description of a known function or configuration is judged to unnecessarily obscure the gist of the present invention, the detailed description will be omitted.
그리고 후술되는 용어들은 본 발명에서의 기능을 고려하여 정의된 용어들로서 이는 사용자, 운용자의 의도 또는 관례 등에 따라 달라질 수 있다.The terms described below are defined in consideration of the functions in the present invention, and may vary depending on the intention or custom of the user or operator.
그러므로 그 정의는 본 명세서 전반에 걸친 내용을 토대로 내려져야 할 것이다.Therefore, the definition should be made based on the contents throughout this specification.
본 발명의 기술적 사상의 일 실시예에 따른 냉해 및 동해 예방용 친환경 식물 영양제의 제조방법은 대두유, 천연 유화제, 정제수, 방충기능 강화용 식물추출물, 포도당 및 왁스를 준비하는 단계(A), 상기 (A)단계에서 준비한 대두유, 천연유화제, 정제수, 포도당 및 왁스를 혼합하여 혼합물을 제조하는 단계(B), 상기 (B)단계에서 제조한 혼합물에 방충기능 강화용 식물 추출물 원액을 첨가하고 혼합 후 교반하여 혼합물을 제조하는 단계(C) 및 (C)단계에서 제조된 혼합물을 농축기에 넣어 농축하는 단계(D)가 포함된다.The method for producing an eco-friendly plant nutrient for preventing cold and freeze damage according to an embodiment of the technical idea of the present invention includes preparing soybean oil, natural emulsifier, purified water, plant extract for enhancing insect repellent function, glucose and wax, (A), the ( Step (B) of preparing a mixture by mixing soybean oil, natural emulsifier, purified water, glucose and wax prepared in step A), adding the plant extract stock solution for enhancing insect repellent function to the mixture prepared in step (B), mixing and stirring Step (C) of preparing a mixture and step (D) of concentrating the mixture prepared in step (C) by placing it in a concentrator.
통상적으로 친환경 식물 영양제는 자연계에 존재하는 생물체의 추출물을 이용하여 농작물의 성장에 해를 끼치는 바이러스나 병원균 및 해충 등을 방제할 수 있도록 제조한 약재이다.Typically, eco-friendly plant nutrients are medicines manufactured using extracts of organisms existing in the natural world to control viruses, pathogens, and pests that harm the growth of crops.
이러한 친환경 식물 영양제은 환경오염에 대해서 영향이 거의 없다는 장점 때문에 점차 그 사용량이 증가하고 있다.The use of these eco-friendly plant nutrients is gradually increasing due to the advantage that they have little effect on environmental pollution.
아직까지는 친환경 식물 영양제가 약효를 발휘하는데 시간이 걸리고, 대량생산과 장기보관이 어렵다는 단점 때문에 사용량이 화학 식물 영양제에 비해 낮은 수준이지만, 최근에는 그러한 단점을 극복하기 위한 다방면의 기술개발이 이루어지고 있다.Until now, the amount of use of eco-friendly plant nutrients is lower than that of chemical plant nutrients due to the disadvantages that it takes time to exert medicinal effects and that mass production and long-term storage are difficult. However, in recent years, various technologies have been developed to overcome such disadvantages. .
그 중에서도 식물성 오일인 대두유는 대량생산이 가능하여 물량확보가 용이하며, 발연점이 240℃로 높고 지방산과 단백질 성분을 많이 함유하고 있다는 장점 때문에 친환경 식물 영양제의 소재로 각광을 받고 있다.Among them, soybean oil, a vegetable oil, is attracting attention as a material for eco-friendly plant nutrients because it can be mass-produced, making it easy to secure quantities, has a high smoke point of 240℃, and contains a lot of fatty acids and proteins.
특히 대두유를 정제하는 과정에서 얻을 수 있는 레시틴(Lecithin)은 천연유화제로서 그 활용도가 높기 때문에 효율적인 자원이용 측면에서도 주목을 받고 있다.In particular, lecithin, which can be obtained in the process of refining soybean oil, is attracting attention in terms of efficient resource use due to its high utility as a natural emulsifier.
대두유의 성분은 식물의 유막을 형성하여 냉해와 동해로부터 식물의 잎과 과육을 보호할 수 있고, 유막이 해충의 몸체를 덮어 호흡기관의 무력화하여 질식사하게 만들 수 있다.The components of soybean oil can form an oil film on plants, protecting the leaves and flesh of plants from cold and frost damage, and the oil film can cover the bodies of pests, disabling their respiratory organs and causing them to suffocate.
또한, 대두유의 지방산 성분을 통해 응애류 등의 대사과정을 교란하여 직접적인 살충·살비 효과를 발휘할 수 있다.In addition, the fatty acid component of soybean oil can exert a direct insecticidal and acaricidal effect by disrupting the metabolic process of mites and other insects.
아울러, 몸체에 대두유가 도포된 작물은 해충의 기피반응으로 먹이활동이나 산란활동을 예방할 수 있고, 대두유의 끈적이는 성질로 인해 해충의 움직임이 봉쇄되어 생존활동을 못하게 하는 방식으로 살충·살비 효과가 구현할 수 있다.In addition, crops with soybean oil applied to their bodies can prevent pests from feeding or laying eggs due to their repellent response, and the sticky nature of soybean oil blocks the movement of pests and prevents them from surviving, thereby providing an insecticidal and acaricidal effect. You can.
이 때문에 대두유를 이용한 친환경 농약은 식물체 내부로 직접 침투하여 약효를 발휘하는 것이 아니라 잎사귀나 줄기 등의 식물몸체 외부에 접촉하여 병원균이나 해충을 방제하는 훌륭한 자재라 할 수 있다.For this reason, eco-friendly pesticides using soybean oil can be said to be an excellent material for controlling pathogens and pests by contacting the outside of the plant body, such as leaves and stems, rather than penetrating directly into the plant body to exert medicinal effects.
상기 대두유, 천연 유화제, 정제수, 왁스, 포도당 및 식물추출물을 준비하는 단계(A)에서 대두유는 초고압의 가공을 통해 대두 내부의 지방을 추출하는 단계를 거치며, 대두유를 추출하는 공정은 다음과 같다.In the step (A) of preparing the soybean oil, natural emulsifier, purified water, wax, glucose, and plant extract, the soybean oil goes through a step of extracting the fat inside the soybean through ultra-high pressure processing, and the process of extracting the soybean oil is as follows.
먼저 대두유를 준비하기 위해, 초고압 전처리 공정을 거친 대두 또는 대두분말과 초임계 유체 추출기술을 사용한다.First, to prepare soybean oil, soybeans or soybean powder that has undergone an ultra-high pressure pretreatment process and supercritical fluid extraction technology are used.
먼저, 대두 또는 대두분말을 500MPa의 압력에서 1시간 동안 초고압 처리를 통해 전처리를 진행한다.First, soybeans or soybean powder are pretreated through ultra-high pressure treatment at a pressure of 500 MPa for 1 hour.
그 후, 초고압 처리된 대두 또는 대두분말을 초임계 유체 추출기술을 통해 대두유를 생산한다.Afterwards, soybean oil is produced from ultra-high pressure treated soybeans or soybean powder using supercritical fluid extraction technology.
상기 초임계 유체 추출기술에서 사용되는 초임계 이산화탄소의 조건은 40 내지 90도의 온도, 400 내지 900 bar 및 40 내지 60g/min의 유동율로 설정하는 것이 적정하다.The conditions for the supercritical carbon dioxide used in the supercritical fluid extraction technology are appropriately set to a temperature of 40 to 90 degrees, 400 to 900 bar, and a flow rate of 40 to 60 g/min.
또한, 초임계 이산화탄소를 투입하여 추출하는 추출 시간은 4시간 내외로 추출한다.In addition, the extraction time for extraction by adding supercritical carbon dioxide is approximately 4 hours.
이 과정에서 추출을 위해 메탄올, 에탄올, 프로판올, 이소프로판올, 부탄올, 아세톤, 에테르, 벤젠, 클로로폴흠, 에틸아세테이트, 메틸렌클로라이드, 헥산 및 시클로헥산으로 이루어진 용매 중 선택된 한 종 이상의 용매를 사용한다.In this process, one or more solvents selected from methanol, ethanol, propanol, isopropanol, butanol, acetone, ether, benzene, chloroform, ethyl acetate, methylene chloride, hexane, and cyclohexane are used for extraction.
상기 천연 유화제는 밀, 코코넛, 올리브, 콩 등 중 선택된 한 종이상의 원료를 사용하여 추출하여 제조된다.The natural emulsifier is manufactured by extraction using one or more raw materials selected from wheat, coconut, olives, soybeans, etc.
상기 왁스는 석유계 왁스, 동물성 왁스, 식물성 왁스 중 선택된 한 종 이상의 왁스이다.The wax is one or more types of wax selected from petroleum wax, animal wax, and vegetable wax.
다음으로, 상기 (A)단계에서 준비한 대두유, 천연유화제, 정제수, 포도당 및 왁스를 혼합하여 혼합물을 제조하는 단계(B)에서는 대두유에 지방산을 넣고 24시간 동안 30 내지 35℃의 저온에 숙성하여 대두유 특유의 냄새를 제거하고 유화안전성을 향상시킨다.Next, in step (B) of preparing a mixture by mixing soybean oil, natural emulsifier, purified water, glucose, and wax prepared in step (A), fatty acid is added to soybean oil and aged at a low temperature of 30 to 35° C. for 24 hours to produce soybean oil. Removes unique odor and improves emulsion safety.
상기 대두유와 왁스를 7:3 내지 6:4 질량 비율로 혼합 후 교반하여 제1 혼합물을 제조한다.The soybean oil and wax are mixed at a mass ratio of 7:3 to 6:4 and then stirred to prepare a first mixture.
제조된 제1 혼합물 100중량%에 3중량%의 포도당과 제1 혼합물 100중량%에 1중량%의 천연유화제를 첨가하여 교반과정을 통해 제2 혼합물을 제조한다.A second mixture is prepared by adding 3% by weight of glucose to 100% by weight of the first mixture and 1% by weight of a natural emulsifier to 100% by weight of the first mixture through a stirring process.
제2 혼합물 100중량%에 정제수 2중량%와 인산과 가리를 각 0.3중량% 첨가하여 교반하고, 붕소와 아연을 각 0.2중량% 첨가하여 교반하여 제3 혼합물을 제조한다.To 100% by weight of the second mixture, 2% by weight of purified water and 0.3% by weight of phosphoric acid and potassium were added and stirred, and 0.2% by weight of boron and zinc were added and stirred to prepare the third mixture.
다음으로, 상기 제3 혼합물에 방충기능 강화용 식물 추출물 원액을 첨가하고 혼합 후 교반하여 혼합물을 제조하는 단계(C)에서 방충기능 강화용 식물 추출물은 인삼 추출물, 옻 추출물, 행인 추출물, 계피 추출물, 저근백피 추출물, 백작약 추출물, 오배자 추출물, 사군자 추출물, 작두콩 추출물, 팥꽃나무 추출물, 생강 추출물, 도꼬마리 추출물, 나팔꽃 추출물 등 다양한 식물들을 활용하여 추출물을 제조할 수 있으며, 본 발명에서는 방충기능 강화용 식물 추출물을 한정하지 않는다.Next, in the step (C) of preparing the mixture by adding the plant extract solution for enhancing insect repellent function to the third mixture, mixing, and stirring, the plant extract for enhancing insect repellent function is ginseng extract, lacquer extract, agar root extract, cinnamon extract, Extracts can be prepared using a variety of plants such as root bark extract, peony extract, shipwreck extract, Sagunja extract, small bean extract, red bean tree extract, ginger extract, eucalyptus extract, and morning glory extract. In the present invention, plants for enhancing insect repellent function are used. The extract is not limited.
상기 제3 혼합물에 첨가되는 방충기능 강화용 식물 추출물의 추출방법은 다음과 같다.The extraction method of the plant extract for enhancing insect repellent function added to the third mixture is as follows.
인삼, 옻, 행인, 계피, 저근백피, 백작약, 오배자, 사군자, 작두콩, 팥꽃나무, 생강, 도꼬마리, 나팔꽃 등 선택된 한 종의 식물을 부직포 주머니에 넣어서 가마솥에 넣은 후 100℃에서 10 내지 12시간 동안 가열하여 식물의 성분을 추출한다.Put one selected plant species such as ginseng, lacquer, apricot, cinnamon, white root bark, white peony, chinensis chinensis, four bean sprouts, bean sprouts, ginger, peach blossom, morning glory, etc. in a non-woven bag and place in a cauldron at 100°C for 10 to 12 hours. The ingredients of the plant are extracted by heating for a while.
추출이 완료된 부직포 주머니를 가마솥에서 빼내어 제거하여 방충기능 강화용 식물 추출물 원액을 제조한다.The extracted non-woven bag is removed from the cauldron and removed to prepare a plant extract solution for enhancing insect repellent function.
상기 제3 혼합물에 상기 방충기능 강화용 식물 추출물 원액을 특정 비율로 첨가하고 혼합 후 교반 과정을 통해서 제4 혼합물을 제조한다.The plant extract stock solution for enhancing the insect repellent function is added to the third mixture at a specific ratio, mixed, and then stirred to prepare the fourth mixture.
상기 제4 혼합물은 기존 대두유의 레시틴에 의한 방충 효과를 한층 더 강화된다.The fourth mixture further enhances the insect repellent effect of lecithin in existing soybean oil.
상기 방충기능 강화용 식물 추출물의 종류에 따라 상기 제3 혼합물에 첨가하는 비율은 상이하다.The ratio added to the third mixture varies depending on the type of plant extract for enhancing the insect repellent function.
본 발명에서는 제3 혼합물 100중량% 에 3 내지 10중량%의 방충기능 강화용 식물 첨가물 원액을 첨가하고 혼합 후 교반하여 제4 혼합물을 제조한다.In the present invention, 3 to 10% by weight of a stock solution of plant additives for enhancing insect repellent function is added to 100% by weight of the third mixture, mixed, and then stirred to prepare the fourth mixture.
마지막으로 상기 단계(C)를 통해 제조된 제4 혼합물을 농축기에 넣어서 농축하는 단계(D)를 거쳐 냉해 및 동해 예방용 친환경 식물 영양제를 제조한다.Finally, the fourth mixture prepared through step (C) is placed in a concentrator to concentrate (D) to produce an eco-friendly plant nutrient for preventing cold damage and frost damage.
상기 단계(D)에서 제조된 제4 혼합물을 농축기에 넣고 3분의 1 내지 4분의 1에 분량으로 농축하여 최종 생산물인 냉해 및 동해 예방용 친환경 식물 영양제를 제조한다.The fourth mixture prepared in step (D) is placed in a concentrator and concentrated to one-third to one-fourth to produce the final product, an eco-friendly plant nutrient for preventing cold damage and freeze damage.
본 발명의 실시에 따른 냉해 및 동해 예방용 친환경 식물 영양제는 250배로 희석하여 사용한다.The eco-friendly plant nutrient for preventing cold and freeze damage according to the practice of the present invention is diluted 250 times and used.
이러한 상기 과정을 통해 냉해 및 동해 예방용 친환경 식물 영양제를 제조할 수 있으며, 본 발명의 기술적 사상에 의한 다양한 실시예를 통해 냉해 및 동해 방지 효과와 해충 방제 보조제로서 활용이 가능하고, 생육촉진, 과실의 당도 증가, 과실의 경도 증가, 과실의 저장성 증가 및 토양산성화를 예방할 수 있는 효과를 제공할 수 있다.Through this process, an eco-friendly plant nutrient for preventing cold damage and freeze damage can be manufactured, and through various embodiments based on the technical idea of the present invention, it can be used as an adjuvant for preventing cold damage and freeze damage and controlling pests, promoting growth and fruit. It can provide the effect of increasing the sugar content, increasing the hardness of the fruit, increasing the storability of the fruit, and preventing soil acidification.
이상과 같이 본 발명에 대해서 예시한 도면을 참조로 하여 설명하였으나, 본 명세서에 개시된 실시 예와 도면에 의해 본 발명이 한정되는 것은 아니며, 본 발명의 기술사상의 범위 내에서 통상의 기술자에 의해 다양한 변형이 이루어질 수 있음은 자명하다. 아울러 앞서 본 발명의 실시 예를 설명하면서 본 발명의 구성에 따른 작용 효과를 명시적으로 기재하여 설명하지 않았을 지라도, 해당 구성에 의해 예측 가능한 효과 또한 인정되어야 함은 당연하다.As described above, the present invention has been described with reference to the illustrative drawings, but the present invention is not limited to the embodiments and drawings disclosed herein, and various modifications may be made by those skilled in the art within the scope of the technical idea of the present invention. It is obvious that transformation can occur. In addition, although the operational effects according to the configuration of the present invention were not explicitly described and explained while explaining the embodiments of the present invention above, it is natural that the predictable effects due to the configuration should also be recognized.
Claims (8)
상기 (A)단계에서 준비한 대두유, 천연유화제, 정제수, 포도당 및 왁스를 혼합하여 혼합물을 제조하는 단계(B);
상기 상기 (B)단계에서 제조한 혼합물에 방충기능 강화용 식물 추출물 원액을 첨가하고 혼합 후 교반하여 혼합물을 제조하는 단계(C); 및
(C)단계에서 제조된 혼합물을 농축기에 넣어 농축하는 단계(D)를 포함하며,
상기 대두유, 천연 유화제, 정제수, 방충기능 강화용 식물추출물, 포도당 및 왁스를 준비하는 단계(A)에서 대두유를 준비하는 공정은 초고압 처리 공정을 거친 대두 또는 대두분말과 이산화탄소 초임계 유체 추출기술을 사용하고,
상기 천연 유화제는 밀, 코코넛, 올리브 중 선택된 한 종이상의 원료를 사용하여 추출하여 제조하며,
상기 왁스는 석유계 왁스, 동물성 왁스, 식물성 왁스 중 선택된 한 종 이상의 왁스인 것을 특징으로 하고,
대두유를 준비하는 공정은 대두 또는 대두분말을 500MPa의 압력에서 1시간 내지 1시간 30분 동안 초고압 전저리를 통해 전처리 된 대두 또는 대두분말를 준비하며,
상기 전처리된 대두 또는 대두분말을 40 내지 90℃의 온도, 400 내지 900 bar의 압력 및 40 내지 60g/min의 유동율로 설정된 이산화탄소 초임계 유체 추출기술을 통해 4시간 동안 추출하여 대두유를 제조를 제조하는 것을 특징으로 하고,
상기 이산화탄소 초임계 유체 추출기술에 사용하는 용매는 메탄올, 에탄올, 프로판올, 이소프로판올, 부탄올, 아세톤, 에테르, 벤젠, 클로로폴흠, 에틸아세테이트, 메틸렌클로라이드, 헥산 및 시클로헥산으로 이루어진 용매 중 선택된 한 종 이상의 용매인 것을 특징으로 하며,
상기 (A)단계에서 준비한 대두유, 천연유화제, 정제수, 포도당 및 왁스를 혼합하여 혼합물을 제조하는 단계(B)는 대두유에 지방산을 넣어 24시간 동안 30 내지 35℃에서 저온 숙성하며,
대두유와 왁스를 7:3 내지 6:4 질량 비율로 혼합 후 교반하여 제1 혼합물을 제조하고,
상기 제1 혼합물 100중량%에 3중량%의 포도당과 제1 혼합물 100중량%에 1중량%의 천연유화제를 첨가 후 교반하여 제2 혼합물을 제조하며,
상기 제2 혼합물 100중량%에 정제수 2중량%와 인산과 가리를 각 0.3중량% 첨가하여 교반 후, 붕소와 아연을 각 0.2중량% 첨가 후 교반하여 제3 혼합물을 제조하는 것을 특징으로 하고,
상기 상기 (B)단계에서 제조한 혼합물에 방충기능 강화용 식물 추출물 원액을 첨가하고 혼합 후 교반하여 혼합물을 제조하는 단계(C)는 제3 혼합물에 방충기능 강화용 식물 추출물 원액을 첨가하여 혼합하며,
상기 방충기능 강화용 식물 추출물은 인삼 추출물, 옻 추출물, 행인 추출물, 계피 추출물, 저근백피 추출물, 백작약 추출물, 오배자 추출물, 사군자 추출물, 작두콩 추출물, 팥꽃나무 추출물, 생강 추출물, 도꼬마리 추출물, 나팔꽃 추출물 중 선택된 한 종 이상의 식물 추출물이며,
상기 방충 기능강화용 식물 추출물을 추출하는 방법은 인삼, 옻, 행인, 계피, 저근백피, 백작약, 오배자, 사군자, 작두콩, 팥꽃나무, 생강, 도꼬마리, 나팔꽃 등 선택된 한 종의 식물을 부직포 주머니에 넣어서 가마솥에 넣은 후 정제수를 넣고 100℃에서 10 내지 12시간 동안 가열하여 추출하며,
추출이 완료된 부직포 주머니를 가마솥에서 제거 후 방충기능 강화용 식물 추출물 원액을 제조하고,
상기 제3 혼합물 100중량%에 3 내지 10중량%의 방충기능 강화용 식물 추출물 원액을 혼합 후 교반하여 제4 혼합물을 제조하는 것을 특징으로 하고,
제조된 혼합물을 농축기에 넣어 농축하는 단계(D)는 단계(C)로부터 제조된 제4 혼합물을 농축기에 넣고 4 분의 1 내지 3 분의 1의 분량으로 농축하여 냉해 및 동해 예방용 친환경 식물 영양제를 제조하는 것을 특징으로 하는 냉해 및 동해 예방용 친환경 식물 영양제 제조방법. Step (A) of preparing soybean oil, natural emulsifier, purified water, plant extract for enhancing insect repellent function, glucose, and wax;
Step (B) of preparing a mixture by mixing soybean oil, natural emulsifier, purified water, glucose, and wax prepared in step (A);
Step (C) of preparing a mixture by adding a stock solution of plant extract for enhancing insect repellent function to the mixture prepared in step (B), mixing, and then stirring; and
It includes a step (D) of concentrating the mixture prepared in step (C) by placing it in a concentrator,
The process of preparing soybean oil in step (A) of preparing soybean oil, natural emulsifier, purified water, plant extract for enhancing insect repellent function, glucose, and wax uses soybeans or soybean powder that have undergone an ultra-high pressure treatment process and carbon dioxide supercritical fluid extraction technology. do,
The natural emulsifier is manufactured by extraction using one or more raw materials selected from wheat, coconut, and olive,
The wax is characterized in that it is one or more types of wax selected from petroleum wax, animal wax, and vegetable wax,
The process of preparing soybean oil involves preparing soybeans or soybean powder that has been pretreated by ultra-high pressure electrolysis for 1 hour to 1 hour and 30 minutes at a pressure of 500 MPa.
Manufacturing soybean oil by extracting the pretreated soybeans or soybean powder for 4 hours through carbon dioxide supercritical fluid extraction technology set at a temperature of 40 to 90°C, a pressure of 400 to 900 bar, and a flow rate of 40 to 60 g/min. Characterized by,
The solvent used in the carbon dioxide supercritical fluid extraction technology is one or more solvents selected from the group consisting of methanol, ethanol, propanol, isopropanol, butanol, acetone, ether, benzene, chloroform, ethyl acetate, methylene chloride, hexane, and cyclohexane. Characterized by
In the step (B) of preparing a mixture by mixing the soybean oil, natural emulsifier, purified water, glucose, and wax prepared in step (A), fatty acid is added to soybean oil and aged at a low temperature of 30 to 35°C for 24 hours,
Soybean oil and wax were mixed at a mass ratio of 7:3 to 6:4 and stirred to prepare a first mixture,
A second mixture is prepared by adding 3% by weight of glucose to 100% by weight of the first mixture and 1% by weight of a natural emulsifier to 100% by weight of the first mixture and stirring,
A third mixture is prepared by adding 2% by weight of purified water and 0.3% by weight of phosphoric acid and potassium each to 100% by weight of the second mixture and stirring, then adding 0.2% by weight of boron and zinc and stirring,
The step (C) of preparing a mixture by adding the plant extract solution for enhancing insect repellent function to the mixture prepared in step (B), mixing, and then stirring, adds and mixes the plant extract solution for enhancing insect repellent function to the third mixture. ,
The plant extracts for strengthening the insect repellent function include ginseng extract, lacquer extract, apricot root extract, cinnamon extract, root bark extract, white peony extract, gallberry extract, Sagundro chinensis extract, pea extract, red bean extract, ginger extract, eucalyptus extract, and morning glory extract. It is an extract of one or more selected plant species,
The method of extracting the plant extract for strengthening the insect repellent function is by placing one selected plant species such as ginseng, lacquer, apricot, cinnamon, white-rooted white bark, white peony, gallnut, gallberry, black bean, red bean, ginger, prickly pear, and morning glory in a non-woven bag. Put it in a cauldron, add purified water, and extract by heating at 100°C for 10 to 12 hours.
After removing the extracted non-woven bag from the cauldron, a plant extract solution for strengthening insect repellent function is prepared,
Characterized in that the fourth mixture is prepared by mixing 3 to 10% by weight of a plant extract stock solution for enhancing insect repellent function with 100% by weight of the third mixture and then stirring,
In the step (D) of concentrating the prepared mixture in a concentrator, the fourth mixture prepared in step (C) is placed in a concentrator and concentrated to one-quarter to one-third of the amount to produce an eco-friendly plant nutrient for preventing cold damage and freeze damage. A method for manufacturing an eco-friendly plant nutrient for preventing cold damage and freeze damage, characterized in that the manufacturing method.
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