KR102497069B1 - 금속 나노와이어의 연속 흐름 제조 - Google Patents

금속 나노와이어의 연속 흐름 제조 Download PDF

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KR102497069B1
KR102497069B1 KR1020207009426A KR20207009426A KR102497069B1 KR 102497069 B1 KR102497069 B1 KR 102497069B1 KR 1020207009426 A KR1020207009426 A KR 1020207009426A KR 20207009426 A KR20207009426 A KR 20207009426A KR 102497069 B1 KR102497069 B1 KR 102497069B1
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nanowires
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metal
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아몰 아르빈드 쿨카르니
제이딥 비핀 데쉬판데
프라치 아쇼크 케이트
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카운슬 오브 사이언티픽 앤드 인더스트리얼 리서치
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    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1806—Stationary reactors having moving elements inside resulting in a turbulent flow of the reactants, such as in centrifugal-type reactors, or having a high Reynolds-number
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J19/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J19/18—Stationary reactors having moving elements inside
    • B01J19/1862—Stationary reactors having moving elements inside placed in series
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F1/00—Metallic powder; Treatment of metallic powder, e.g. to facilitate working or to improve properties
    • B22F1/05—Metallic powder characterised by the size or surface area of the particles
    • B22F1/054—Nanosized particles
    • B22F1/0547—Nanofibres or nanotubes
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F9/00—Making metallic powder or suspensions thereof
    • B22F9/16—Making metallic powder or suspensions thereof using chemical processes
    • B22F9/18—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds
    • B22F9/24—Making metallic powder or suspensions thereof using chemical processes with reduction of metal compounds starting from liquid metal compounds, e.g. solutions
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B82—NANOTECHNOLOGY
    • B82Y—SPECIFIC USES OR APPLICATIONS OF NANOSTRUCTURES; MEASUREMENT OR ANALYSIS OF NANOSTRUCTURES; MANUFACTURE OR TREATMENT OF NANOSTRUCTURES
    • B82Y40/00—Manufacture or treatment of nanostructures
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00002—Chemical plants
    • B01J2219/00018—Construction aspects
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00051—Controlling the temperature
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/00049—Controlling or regulating processes
    • B01J2219/00164—Controlling or regulating processes controlling the flow
    • B01J2219/00166—Controlling or regulating processes controlling the flow controlling the residence time inside the reactor vessel
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2418—Feeding means
    • B01J2219/2419—Feeding means for the reactants
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01J—CHEMICAL OR PHYSICAL PROCESSES, e.g. CATALYSIS OR COLLOID CHEMISTRY; THEIR RELEVANT APPARATUS
    • B01J2219/00—Chemical, physical or physico-chemical processes in general; Their relevant apparatus
    • B01J2219/24—Stationary reactors without moving elements inside
    • B01J2219/2401—Reactors comprising multiple separate flow channels
    • B01J2219/2402—Monolithic-type reactors
    • B01J2219/2423—Separation means, e.g. membrane inside the reactor
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2201/00—Treatment under specific atmosphere
    • B22F2201/40—Metal compounds
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2202/00—Treatment under specific physical conditions
    • B22F2202/17—Treatment under specific physical conditions use of centrifugal or vortex forces
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2203/00—Controlling
    • B22F2203/11—Controlling temperature, temperature profile
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2301/00—Metallic composition of the powder or its coating
    • B22F2301/25—Noble metals, i.e. Ag Au, Ir, Os, Pd, Pt, Rh, Ru
    • B22F2301/255—Silver or gold
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B22—CASTING; POWDER METALLURGY
    • B22F—WORKING METALLIC POWDER; MANUFACTURE OF ARTICLES FROM METALLIC POWDER; MAKING METALLIC POWDER; APPARATUS OR DEVICES SPECIALLY ADAPTED FOR METALLIC POWDER
    • B22F2304/00—Physical aspects of the powder
    • B22F2304/05—Submicron size particles
    • B22F2304/056—Particle size above 100 nm up to 300 nm
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Engineering & Computer Science (AREA)
  • Nanotechnology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Inorganic Chemistry (AREA)
  • Manufacturing & Machinery (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • General Physics & Mathematics (AREA)
  • Condensed Matter Physics & Semiconductors (AREA)
  • Physics & Mathematics (AREA)
  • Manufacture Of Metal Powder And Suspensions Thereof (AREA)
KR1020207009426A 2017-09-06 2018-09-06 금속 나노와이어의 연속 흐름 제조 Active KR102497069B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
IN201711031533 2017-09-06
PCT/IN2018/050576 WO2019049172A1 (en) 2017-09-06 2018-09-06 CONTINUOUS FLOW PRODUCTION OF METALLIC NANOWELS
IN201711031533A IN201711031533A (https=) 2017-09-06 2018-09-06

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KR20200051682A KR20200051682A (ko) 2020-05-13
KR102497069B1 true KR102497069B1 (ko) 2023-02-06

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US (1) US20210060656A1 (https=)
EP (1) EP3678804B1 (https=)
JP (1) JP7225217B2 (https=)
KR (1) KR102497069B1 (https=)
CN (1) CN111225755A (https=)
ES (1) ES2927254T3 (https=)
IN (1) IN201711031533A (https=)
WO (1) WO2019049172A1 (https=)

Families Citing this family (7)

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Publication number Priority date Publication date Assignee Title
JP7438348B2 (ja) * 2019-11-15 2024-02-26 カウンシル オブ サイエンティフィック アンド インダストリアル リサーチ 気泡塔型反応器を使用した、金属ナノワイヤの合成のための連続流動法
CN112024905A (zh) * 2020-07-08 2020-12-04 南京大学 一种基于连续流技术规模化合成纳米银线的方法
KR102537063B1 (ko) * 2021-11-02 2023-05-26 경희대학교 산학협력단 금속계 나노소재의 제조방법, 이로부터 제조된 금속계 나노소재, 촉매 및 검출장치
CN114833334B (zh) * 2022-04-02 2023-08-15 有研工程技术研究院有限公司 可连续制备微米级球形金粉的方法
DE102023101927A1 (de) * 2023-01-26 2024-08-01 Karlsruher Institut für Technologie, Körperschaft des öffentlichen Rechts Verfahren zur kontinuierlichen Cluster- und Nanopartikelsynthese
CN116698671B (zh) * 2023-06-05 2023-11-21 南京工业大学 一种磁纳米毛刷及其制备方法
CN118905237B (zh) * 2024-07-24 2025-09-23 泉州师范学院 一种超长银纳米线的制备方法

Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080034921A1 (en) 2005-01-14 2008-02-14 Cabot Corporation Production of metal nanoparticles
US20120207644A1 (en) 2011-02-15 2012-08-16 Ollmann Richard R Nanowire preparation methods, compositions, and articles
US20130298732A1 (en) 2009-08-25 2013-11-14 Cambrios Technologies Corporation Methods for controlling metal nanostructures morphology
US20150107413A1 (en) 2012-01-30 2015-04-23 Nthdegree Technologies Worldwide Inc. Methods for fabrication of nanostructures
JP2015526836A (ja) 2012-06-05 2015-09-10 コミサリア ア レネルジィ アトミーク エ オ ゼネ ルジイ アルテアナティーフＣｏｍｍｉｓｓａｒｉａｔａ Ｌ’Ｅｎｅｒｇｉｅ Ａｔｏｍｉｑｕｅ Ｅｔ Ａｕｘ Ｅｎｅｒｇｉｅｓ Ａｌｔｅｒｎａｔｉｖｅｓ 銀ナノワイヤをベースとする透明導体材料の電気的および光学的性能を改善する方法
JP2015180772A (ja) 2014-03-07 2015-10-15 Ｄｏｗａホールディングス株式会社 銀ナノワイヤの製造方法並びに銀ナノワイヤおよびそれを用いたインク

Family Cites Families (10)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US8048192B2 (en) * 2005-12-30 2011-11-01 General Electric Company Method of manufacturing nanoparticles
KR100877522B1 (ko) * 2007-05-15 2009-01-09 삼성전기주식회사 금속 나노입자의 제조장치 및 제조방법
TWI379908B (en) * 2008-12-02 2012-12-21 Chung Shan Inst Of Science Method for continuously fabricating silver nanowire
DE102009015470A1 (de) * 2008-12-12 2010-06-17 Byk-Chemie Gmbh Verfahren zur Herstellung von Metallnanopartikeln und auf diese Weise erhaltene Metallnanopartikel und ihre Verwendung
US20100242679A1 (en) 2009-03-29 2010-09-30 Yi-Hsiuan Yu Method for continuously fabricating silver nanowire
JP2013007070A (ja) 2011-06-22 2013-01-10 Nippon Steel & Sumikin Chemical Co Ltd ニッケルナノ粒子の連続製造装置及び連続製造方法
JP5785001B2 (ja) 2011-06-23 2015-09-24 新日鉄住金化学株式会社 金属ナノ粒子の連続製造装置及び連続製造方法
KR20130014279A (ko) * 2011-07-29 2013-02-07 엘지이노텍 주식회사 나노 와이어 및 이의 제조방법
CN104511596B (zh) * 2013-09-30 2017-01-18 中科院广州化学有限公司 一种纳米银线的连续制备方法及其装置
DE102015013219A1 (de) 2014-10-28 2016-04-28 Dow Global Technologies Llc Verfahren zur Herstellung von Silber-Nanodrähten

Patent Citations (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US20080034921A1 (en) 2005-01-14 2008-02-14 Cabot Corporation Production of metal nanoparticles
US20130298732A1 (en) 2009-08-25 2013-11-14 Cambrios Technologies Corporation Methods for controlling metal nanostructures morphology
US20120207644A1 (en) 2011-02-15 2012-08-16 Ollmann Richard R Nanowire preparation methods, compositions, and articles
US20150107413A1 (en) 2012-01-30 2015-04-23 Nthdegree Technologies Worldwide Inc. Methods for fabrication of nanostructures
JP2015526836A (ja) 2012-06-05 2015-09-10 コミサリア ア レネルジィ アトミーク エ オ ゼネ ルジイ アルテアナティーフＣｏｍｍｉｓｓａｒｉａｔａ Ｌ’Ｅｎｅｒｇｉｅ Ａｔｏｍｉｑｕｅ Ｅｔ Ａｕｘ Ｅｎｅｒｇｉｅｓ Ａｌｔｅｒｎａｔｉｖｅｓ 銀ナノワイヤをベースとする透明導体材料の電気的および光学的性能を改善する方法
JP2015180772A (ja) 2014-03-07 2015-10-15 Ｄｏｗａホールディングス株式会社 銀ナノワイヤの製造方法並びに銀ナノワイヤおよびそれを用いたインク

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ES2927254T3 (es) 2022-11-03
JP7225217B2 (ja) 2023-02-20
IN201711031533A (https=) 2024-02-23
WO2019049172A1 (en) 2019-03-14
WO2019049172A4 (en) 2019-05-09
EP3678804A1 (en) 2020-07-15
CN111225755A (zh) 2020-06-02
KR20200051682A (ko) 2020-05-13
JP2021503039A (ja) 2021-02-04
US20210060656A1 (en) 2021-03-04
EP3678804B1 (en) 2022-06-15

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