KR102327728B1 - 아크릴산의 제조 공정 및 시스템 - Google Patents

아크릴산의 제조 공정 및 시스템 Download PDF

Info

Publication number
KR102327728B1
KR102327728B1 KR1020167023211A KR20167023211A KR102327728B1 KR 102327728 B1 KR102327728 B1 KR 102327728B1 KR 1020167023211 A KR1020167023211 A KR 1020167023211A KR 20167023211 A KR20167023211 A KR 20167023211A KR 102327728 B1 KR102327728 B1 KR 102327728B1
Authority
KR
South Korea
Prior art keywords
stream
column
final column
acrylic acid
dehydration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Active
Application number
KR1020167023211A
Other languages
English (en)
Korean (ko)
Other versions
KR20160122749A (ko
Inventor
마이클 에스. 드코시
Original Assignee
알케마 인코포레이티드
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by 알케마 인코포레이티드 filed Critical 알케마 인코포레이티드
Publication of KR20160122749A publication Critical patent/KR20160122749A/ko
Application granted granted Critical
Publication of KR102327728B1 publication Critical patent/KR102327728B1/ko
Active legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020167023211A 2014-02-20 2015-02-12 아크릴산의 제조 공정 및 시스템 Active KR102327728B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201461942261P 2014-02-20 2014-02-20
US61/942,261 2014-02-20
PCT/US2015/015520 WO2015126704A1 (en) 2014-02-20 2015-02-12 Process and system for producing acrylic acid

Publications (2)

Publication Number Publication Date
KR20160122749A KR20160122749A (ko) 2016-10-24
KR102327728B1 true KR102327728B1 (ko) 2021-11-18

Family

ID=53878832

Family Applications (1)

Application Number Title Priority Date Filing Date
KR1020167023211A Active KR102327728B1 (ko) 2014-02-20 2015-02-12 아크릴산의 제조 공정 및 시스템

Country Status (11)

Country Link
US (1) US10112885B2 (enExample)
EP (1) EP3110786B1 (enExample)
JP (1) JP6703950B2 (enExample)
KR (1) KR102327728B1 (enExample)
CN (1) CN106061934B (enExample)
BR (1) BR112016019248B1 (enExample)
MX (1) MX2016010692A (enExample)
SA (1) SA516371688B1 (enExample)
SG (1) SG11201606743PA (enExample)
TW (1) TWI658035B (enExample)
WO (1) WO2015126704A1 (enExample)

Families Citing this family (17)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3041958B1 (fr) * 2015-10-06 2019-06-14 Arkema France Procede ameliore de production d’acide (meth)acrylique de grade polymere
DE202015106097U1 (de) * 2015-11-11 2016-02-01 Holger Blum Fördereinrichtung für eine Vakuumdestillationsanlage
FR3049601B1 (fr) * 2016-03-29 2018-03-09 Arkema France Procede ameliore de production d'acide (meth)acrylique
JP6522213B1 (ja) * 2018-08-03 2019-05-29 住友化学株式会社 メタクロレイン及び／又はメタクリル酸の製造方法
FR3094716B1 (fr) * 2019-04-02 2021-06-04 Arkema France Production d’acide acrylique de grade polymere
FR3108906B1 (fr) 2020-04-06 2022-03-04 Arkema France Procede de purification d’acide (meth)acrylique
KR102855127B1 (ko) * 2021-10-15 2025-09-03 주식회사 엘지화학 아크릴산 제조방법
KR102855131B1 (ko) * 2021-10-15 2025-09-03 주식회사 엘지화학 아크릴산 제조방법
CN114632343B (zh) * 2022-05-18 2022-12-02 北京化工大学 一种mvr热泵精馏系统及方法
KR20240037081A (ko) * 2022-09-14 2024-03-21 주식회사 엘지화학 아크릴산 제조방법
KR102846320B1 (ko) * 2022-09-14 2025-08-14 주식회사 엘지화학 아크릴산 제조방법
US20240093919A1 (en) * 2022-09-19 2024-03-21 Graham Corporation Process vacuum system with condenser and dual ejectors
CN115738328B (zh) * 2022-11-28 2024-07-19 东营市赫邦化工有限公司 一种节能的循环式甘油蒸馏蒸发器
KR20240152019A (ko) * 2023-04-12 2024-10-21 주식회사 엘지화학 젖산 탈수 반응을 통한 아크릴산 제조 방법 및 이의 제조 장치
KR20250087112A (ko) * 2023-12-07 2025-06-16 주식회사 엘지화학 아크릴산의 제조 방법
WO2025121919A1 (ko) * 2023-12-07 2025-06-12 주식회사 엘지화학 아크릴산의 제조 방법 및 장치
FR3162750A1 (fr) * 2024-05-30 2025-12-05 Arkema France Procede de purification d’acide (meth)acrylique

Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010027732A1 (en) 2008-09-04 2010-03-11 Dow Global Technologies Inc. Process for producing acrolein and/or acrylic acid from propane
US20110213174A1 (en) 2008-10-24 2011-09-01 Arkema France Process for manufactguring acrolein from glycerol

Family Cites Families (19)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US3168136A (en) * 1955-03-17 1965-02-02 Babcock & Wilcox Co Shell and tube-type heat exchanger
FR1357332A (fr) 1962-05-18 1964-04-03 Shell Int Research Procédé d'amélioration de la résistance au choc des pièces moulées en polypropylène
US3301871A (en) 1964-06-15 1967-01-31 Upjohn Co Novel 1, 4-dialkylprolines, derivatives thereof and process
US3314220A (en) * 1965-03-22 1967-04-18 Foster Wheeler Corp Multiannular centrifugal separator
DE69320386T2 (de) * 1992-02-28 1999-02-04 Sumitomo Chemical Co., Ltd., Tokio/Tokio Verfahren zur Herstellung von Isobutylen durch oxidative Dehydrierung von Isobutan
JP3411280B2 (ja) * 1992-09-21 2003-05-26 協和醗酵工業株式会社 血小板減少症治療剤
JPH10204030A (ja) * 1997-01-24 1998-08-04 Toagosei Co Ltd （メタ）アクリル酸エステルの精製方法及び製造方法並びにその製造装置
US6019820A (en) 1997-05-07 2000-02-01 E. I. Du Pont De Nemours And Company Liquid jet compressor
DE19740253A1 (de) 1997-09-12 1999-03-18 Basf Ag Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten
DE19837519A1 (de) * 1998-08-19 2000-02-24 Basf Ag Verfahren zur Herstellung von Acrolein und/oder Acrylsäure aus Propan
JP4698778B2 (ja) * 1999-06-03 2011-06-08 株式会社日本触媒 （メタ）アクリル酸（エステル）の精製方法
JP3948855B2 (ja) * 1999-06-10 2007-07-25 株式会社日本触媒 （メタ）アクリル酸の製造方法
JP2001131116A (ja) 1999-11-08 2001-05-15 Nippon Shokubai Co Ltd 易重合性物質含有液の蒸留方法
WO2003018162A1 (en) 2001-08-22 2003-03-06 Mitsubishi Chemical Corporation Distilling equipment for lase-of-polymerization compound
JP2005179352A (ja) * 2003-11-28 2005-07-07 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
JP5199260B2 (ja) 2006-09-15 2013-05-15 アルケマ インコーポレイティド アクリル酸の生成方法
WO2009123872A1 (en) 2008-04-01 2009-10-08 Dow Global Technologies Inc. Procedure for the startup of a (meth)acrylic acid plant
FR2935971B1 (fr) * 2008-09-16 2010-11-19 Arkema France Acide bio-acrylique de grade polymere et son procede de fabrication a partir de glycerol.
MX2011003411A (es) 2008-10-01 2011-04-21 Arkema Inc Control de un proceso para la purificacion de acido (met) acrilico usando analisis de ir cercano en linea.

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2010027732A1 (en) 2008-09-04 2010-03-11 Dow Global Technologies Inc. Process for producing acrolein and/or acrylic acid from propane
US20110213174A1 (en) 2008-10-24 2011-09-01 Arkema France Process for manufactguring acrolein from glycerol

Also Published As

Publication number Publication date
SG11201606743PA (en) 2016-09-29
US10112885B2 (en) 2018-10-30
KR20160122749A (ko) 2016-10-24
CN106061934B (zh) 2019-05-03
TWI658035B (zh) 2019-05-01
BR112016019248B1 (pt) 2022-03-15
EP3110786A4 (en) 2017-09-06
EP3110786B1 (en) 2021-08-25
WO2015126704A1 (en) 2015-08-27
BR112016019248A2 (enExample) 2017-08-15
CN106061934A (zh) 2016-10-26
JP2017509613A (ja) 2017-04-06
EP3110786A1 (en) 2017-01-04
SA516371688B1 (ar) 2019-04-16
MX2016010692A (es) 2017-05-09
US20170174604A1 (en) 2017-06-22
TW201534581A (zh) 2015-09-16
JP6703950B2 (ja) 2020-06-03

Similar Documents

Publication Publication Date Title
KR102327728B1 (ko) 아크릴산의 제조 공정 및 시스템
CN101516820B (zh) 制备丙烯酸的方法
JP6894255B2 (ja) 改良された（メタ）アクリル酸製造プロセス
US7799946B2 (en) Process for separating methacrolein from methacrylic acid in a gas phase product from the partial oxidation of isobutene
JP6716597B2 (ja) （メタ）アクリル酸の改良された製造方法
US10343969B2 (en) Process and plant for recovering acrylic acid
JP2002509902A (ja) アクリル酸及びアクリル酸エステルの製造法
US12116339B2 (en) Method for purifying (meth)acrylic acid

Legal Events

Date Code Title Description
PA0105 International application

Patent event date: 20160824

Patent event code: PA01051R01D

Comment text: International Patent Application

PG1501 Laying open of application
PA0201 Request for examination

Patent event code: PA02012R01D

Patent event date: 20200207

Comment text: Request for Examination of Application

E902 Notification of reason for refusal
PE0902 Notice of grounds for rejection

Comment text: Notification of reason for refusal

Patent event date: 20210226

Patent event code: PE09021S01D

E701 Decision to grant or registration of patent right
PE0701 Decision of registration

Patent event code: PE07011S01D

Comment text: Decision to Grant Registration

Patent event date: 20210826

PR0701 Registration of establishment

Comment text: Registration of Establishment

Patent event date: 20211112

Patent event code: PR07011E01D

PR1002 Payment of registration fee

Payment date: 20211115

End annual number: 3

Start annual number: 1

PG1601 Publication of registration