TWI658035B - 用於生產丙烯酸之方法和系統 - Google Patents

用於生產丙烯酸之方法和系統 Download PDF

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Publication number
TWI658035B
TWI658035B TW104105708A TW104105708A TWI658035B TW I658035 B TWI658035 B TW I658035B TW 104105708 A TW104105708 A TW 104105708A TW 104105708 A TW104105708 A TW 104105708A TW I658035 B TWI658035 B TW I658035B
Authority
TW
Taiwan
Prior art keywords
column
stream
final treatment
acrylic acid
treatment column
Prior art date
Application number
TW104105708A
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English (en)
Chinese (zh)
Other versions
TW201534581A (zh
Inventor
麥克Ｓ 狄克爾西
Original Assignee
美商愛克瑪公司
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Filing date
Publication date
Application filed by 美商愛克瑪公司 filed Critical 美商愛克瑪公司
Publication of TW201534581A publication Critical patent/TW201534581A/zh
Application granted granted Critical
Publication of TWI658035B publication Critical patent/TWI658035B/zh

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Classifications

    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/43—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation
    • C07C51/44—Separation; Purification; Stabilisation; Use of additives by change of the physical state, e.g. crystallisation by distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/10—Vacuum distillation
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D3/00—Distillation or related exchange processes in which liquids are contacted with gaseous media, e.g. stripping
    • B01D3/14—Fractional distillation or use of a fractionation or rectification column
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0027—Condensation of vapours; Recovering volatile solvents by condensation by direct contact between vapours or gases and the cooling medium
    • B—PERFORMING OPERATIONS; TRANSPORTING
    • B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
    • B01D—SEPARATION
    • B01D5/00—Condensation of vapours; Recovering volatile solvents by condensation
    • B01D5/0057—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes
    • B01D5/006—Condensation of vapours; Recovering volatile solvents by condensation in combination with other processes with evaporation or distillation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C51/00—Preparation of carboxylic acids or their salts, halides or anhydrides
    • C07C51/42—Separation; Purification; Stabilisation; Use of additives
    • C07C51/50—Use of additives, e.g. for stabilisation
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C57/00—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms
    • C07C57/02—Unsaturated compounds having carboxyl groups bound to acyclic carbon atoms with only carbon-to-carbon double bonds as unsaturation
    • C07C57/03—Monocarboxylic acids
    • C07C57/04—Acrylic acid; Methacrylic acid
    • Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
    • Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
    • Y02P—CLIMATE CHANGE MITIGATION TECHNOLOGIES IN THE PRODUCTION OR PROCESSING OF GOODS
    • Y02P20/00—Technologies relating to chemical industry
    • Y02P20/50—Improvements relating to the production of bulk chemicals
    • Y02P20/582—Recycling of unreacted starting or intermediate materials

Landscapes

  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Crystallography & Structural Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
TW104105708A 2014-02-20 2015-02-17 用於生產丙烯酸之方法和系統 TWI658035B (zh)

Applications Claiming Priority (2)

Application Number Priority Date Filing Date Title
US201461942261P 2014-02-20 2014-02-20
US61/942,261 2014-02-20

Publications (2)

Publication Number Publication Date
TW201534581A TW201534581A (zh) 2015-09-16
TWI658035B true TWI658035B (zh) 2019-05-01

Family

ID=53878832

Family Applications (1)

Application Number Title Priority Date Filing Date
TW104105708A TWI658035B (zh) 2014-02-20 2015-02-17 用於生產丙烯酸之方法和系統

Country Status (11)

Country Link
US (1) US10112885B2 (enExample)
EP (1) EP3110786B1 (enExample)
JP (1) JP6703950B2 (enExample)
KR (1) KR102327728B1 (enExample)
CN (1) CN106061934B (enExample)
BR (1) BR112016019248B1 (enExample)
MX (1) MX2016010692A (enExample)
SA (1) SA516371688B1 (enExample)
SG (1) SG11201606743PA (enExample)
TW (1) TWI658035B (enExample)
WO (1) WO2015126704A1 (enExample)

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* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
FR3041958B1 (fr) * 2015-10-06 2019-06-14 Arkema France Procede ameliore de production d’acide (meth)acrylique de grade polymere
DE202015106097U1 (de) * 2015-11-11 2016-02-01 Holger Blum Fördereinrichtung für eine Vakuumdestillationsanlage
FR3049601B1 (fr) * 2016-03-29 2018-03-09 Arkema France Procede ameliore de production d'acide (meth)acrylique
JP6522213B1 (ja) * 2018-08-03 2019-05-29 住友化学株式会社 メタクロレイン及び／又はメタクリル酸の製造方法
FR3094716B1 (fr) * 2019-04-02 2021-06-04 Arkema France Production d’acide acrylique de grade polymere
FR3108906B1 (fr) 2020-04-06 2022-03-04 Arkema France Procede de purification d’acide (meth)acrylique
KR102855127B1 (ko) * 2021-10-15 2025-09-03 주식회사 엘지화학 아크릴산 제조방법
KR102855131B1 (ko) * 2021-10-15 2025-09-03 주식회사 엘지화학 아크릴산 제조방법
CN114632343B (zh) * 2022-05-18 2022-12-02 北京化工大学 一种mvr热泵精馏系统及方法
KR20240037081A (ko) * 2022-09-14 2024-03-21 주식회사 엘지화학 아크릴산 제조방법
KR102846320B1 (ko) * 2022-09-14 2025-08-14 주식회사 엘지화학 아크릴산 제조방법
US20240093919A1 (en) * 2022-09-19 2024-03-21 Graham Corporation Process vacuum system with condenser and dual ejectors
CN115738328B (zh) * 2022-11-28 2024-07-19 东营市赫邦化工有限公司 一种节能的循环式甘油蒸馏蒸发器
KR20240152019A (ko) * 2023-04-12 2024-10-21 주식회사 엘지화학 젖산 탈수 반응을 통한 아크릴산 제조 방법 및 이의 제조 장치
KR20250087112A (ko) * 2023-12-07 2025-06-16 주식회사 엘지화학 아크릴산의 제조 방법
WO2025121919A1 (ko) * 2023-12-07 2025-06-12 주식회사 엘지화학 아크릴산의 제조 방법 및 장치
FR3162750A1 (fr) * 2024-05-30 2025-12-05 Arkema France Procede de purification d’acide (meth)acrylique

Citations (2)

* Cited by examiner, † Cited by third party
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CN1277183A (zh) * 1999-06-10 2000-12-20 株式会社日本触媒 (甲基)丙烯酸的制造方法
TW200825047A (en) * 2006-09-15 2008-06-16 Dow Global Technologies Inc Process for producing acrylic acid

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FR1357332A (fr) 1962-05-18 1964-04-03 Shell Int Research Procédé d'amélioration de la résistance au choc des pièces moulées en polypropylène
US3301871A (en) 1964-06-15 1967-01-31 Upjohn Co Novel 1, 4-dialkylprolines, derivatives thereof and process
US3314220A (en) * 1965-03-22 1967-04-18 Foster Wheeler Corp Multiannular centrifugal separator
DE69320386T2 (de) * 1992-02-28 1999-02-04 Sumitomo Chemical Co., Ltd., Tokio/Tokio Verfahren zur Herstellung von Isobutylen durch oxidative Dehydrierung von Isobutan
JP3411280B2 (ja) * 1992-09-21 2003-05-26 協和醗酵工業株式会社 血小板減少症治療剤
JPH10204030A (ja) * 1997-01-24 1998-08-04 Toagosei Co Ltd （メタ）アクリル酸エステルの精製方法及び製造方法並びにその製造装置
US6019820A (en) 1997-05-07 2000-02-01 E. I. Du Pont De Nemours And Company Liquid jet compressor
DE19740253A1 (de) 1997-09-12 1999-03-18 Basf Ag Verfahren zur fraktionierten Kondensation eines heißen Gasgemisches mit einem hohen Anteil nicht kondensierbarer Komponenten
DE19837519A1 (de) * 1998-08-19 2000-02-24 Basf Ag Verfahren zur Herstellung von Acrolein und/oder Acrylsäure aus Propan
JP4698778B2 (ja) * 1999-06-03 2011-06-08 株式会社日本触媒 （メタ）アクリル酸（エステル）の精製方法
JP2001131116A (ja) 1999-11-08 2001-05-15 Nippon Shokubai Co Ltd 易重合性物質含有液の蒸留方法
WO2003018162A1 (en) 2001-08-22 2003-03-06 Mitsubishi Chemical Corporation Distilling equipment for lase-of-polymerization compound
JP2005179352A (ja) * 2003-11-28 2005-07-07 Mitsubishi Chemicals Corp （メタ）アクリル酸の精製方法
WO2009123872A1 (en) 2008-04-01 2009-10-08 Dow Global Technologies Inc. Procedure for the startup of a (meth)acrylic acid plant
WO2010027732A1 (en) 2008-09-04 2010-03-11 Dow Global Technologies Inc. Process for producing acrolein and/or acrylic acid from propane
FR2935971B1 (fr) * 2008-09-16 2010-11-19 Arkema France Acide bio-acrylique de grade polymere et son procede de fabrication a partir de glycerol.
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EP2179981A1 (en) * 2008-10-24 2010-04-28 Arkema France Process for manufacturing acrolein from glycerol

Patent Citations (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1277183A (zh) * 1999-06-10 2000-12-20 株式会社日本触媒 (甲基)丙烯酸的制造方法
TW200825047A (en) * 2006-09-15 2008-06-16 Dow Global Technologies Inc Process for producing acrylic acid

Also Published As

Publication number Publication date
SG11201606743PA (en) 2016-09-29
US10112885B2 (en) 2018-10-30
KR20160122749A (ko) 2016-10-24
CN106061934B (zh) 2019-05-03
BR112016019248B1 (pt) 2022-03-15
EP3110786A4 (en) 2017-09-06
EP3110786B1 (en) 2021-08-25
WO2015126704A1 (en) 2015-08-27
BR112016019248A2 (enExample) 2017-08-15
CN106061934A (zh) 2016-10-26
JP2017509613A (ja) 2017-04-06
KR102327728B1 (ko) 2021-11-18
EP3110786A1 (en) 2017-01-04
SA516371688B1 (ar) 2019-04-16
MX2016010692A (es) 2017-05-09
US20170174604A1 (en) 2017-06-22
TW201534581A (zh) 2015-09-16
JP6703950B2 (ja) 2020-06-03

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