KR102327023B1 - Shampoo Composition and manufacturing mehtod thereof - Google Patents

Abstract

The present invention relates to a shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function and a method for manufacturing the same, and more particularly, to a step of preparing a raw material containing green tea, gold and silver flower, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold and mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water, ultrasonically extracting the fermented raw material, plasma-treating the ultrasonically extracted extract, and the plasma-treated extract It is characterized in that it comprises the steps of distillation extraction, and filtering the distillation-extracted extract. According to the present invention, it is possible to not only cleanly clean harmful bacteria and contaminants present on the scalp, but also to remove lipid peroxide generated in the pores of the scalp and to calm the heat gathered on the scalp to prevent hair loss and scalp troubles. There is this.

Description

Shampoo composition having cooling, antibacterial and lipid peroxide removal functions, and a method for manufacturing the same

The present invention relates to a shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function and a method for manufacturing the same, and more particularly, it contains extracts of green tea, gold and silver flower, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold as active ingredients. , by fermentation, ultrasonic extraction, plasma treatment and distillation extraction of raw materials, as well as to increase the extraction efficiency, to a shampoo composition capable of maximizing the effect of cleaning heat, antibacterial and lipid peroxide removal, and a method for manufacturing the same.

In general, in modern industrialized society, where living standards have improved, shampoo is used almost every day, which causes side effects such as damage to hair. That is, shampoos sold on the market are manufactured and sold mainly for cleaning power rather than for the purpose of protecting hair, so that if you shampoo your hair every day, it will cause damage to your hair.

And, as conventional shampoos use various chemical synthetic materials, it is difficult to expect a naturally controllable soothing and purifying action of the scalp and hair, as well as abnormal stimulation of the scalp and hair.

In addition, dandruff formed on the scalp refers to the fact that the dead cells of the scalp fall off in the form of hard keratin and form a large lump with sebum and sweat secreted from the scalp, and dandruff is usually accompanied by itching in the scalp. Scratching can cause scarring and eventually inflammation, leading to eczema and hair loss.

That is, when the scalp is infected by harmful bacteria that cause scalp disease, itching and inflammation, the cell cycle of the epidermis is accelerated and keratinized abnormally, and in the case of such seborrheic dermatitis, symptoms worsen and hair loss occurs.

One of the causes of hair loss is that the pores are infected by causes such as degeneration of the sebum film and by-products, and this leads to hair loss by affecting the growth of the hair.

Therefore, it was required to develop a shampoo composition capable of alleviating scalp infection, dandruff, and itching and preventing hair loss by using natural substances rather than chemical synthetic substances.

KR 10-1292017 B1 KR 10-0839704 B1

Therefore, it is an object of the present invention to remove dandruff bacteria present on the scalp, to cleanly remove and clean various contaminants such as lipid peroxide, and to calm the heat gathered on the scalp to prevent hair loss and scalp troubles. An object of the present invention is to provide a shampoo composition having an antibacterial and lipid peroxide removal function and a method for preparing the same.

To achieve the above object, the shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function of the present invention and a method for manufacturing the same are prepared by preparing raw materials including green tea, gold leaf, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold. step, mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water, ultrasonically extracting the fermented raw material, plasma-treating the ultrasonically extracted extract, and the plasma-treated extract It is characterized in that it comprises the steps of distilling extraction, and filtering the distillation-extracted extract.

The plasma treatment is characterized in that after adding tourmaline and germanium to the ultrasonically extracted extract, plasma treatment is performed under a platinum catalyst.

The raw material is characterized in that it further comprises a hairy dew, Gabija tree and Ukriin.

The shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function according to the present invention is characterized in that it is prepared through the above-described method.

According to the present invention, it is possible to sterilize dandruff present on the scalp and clean various contaminants such as lipid peroxide, as well as to calm the heat gathered on the scalp to prevent hair loss and scalp troubles.

1 is a flow chart showing the manufacturing process of a shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function according to the present invention.

Hereinafter, the present invention will be described in detail.

First, the shampoo composition according to the present invention has an excellent cooling effect to lower the heat of the scalp, has excellent cleaning power to sufficiently remove lipid peroxide in the pores, and has an excellent antibacterial effect against various harmful bacteria such as dandruff bacteria to protect it from various contamination. The biggest feature is that it protects the scalp.

The shampoo composition according to the present invention, green tea, gold ginseng, aeyeop, gwakhyang, mint, eoseongcho, aloe and containing an extract of raw materials containing gold as an active ingredient, the extract is the raw material fermentation, ultrasonic extraction, plasma treatment, distillation extraction and filtered.

The raw materials used in the present invention will be briefly described.

The green tea (Green tea, Camellia teaceac) is known to have a function of supplying nutrients of vitamins and minerals, and a function of satisfying preferences such as taste and aroma. The main component of green tea astringent taste is catechin, which is a polyphenol component, and depending on its derivative, catechin is epicatechin, epigallocatechin, epicatechin gallate, and epigallo. It can be classified as catechin gallate (Epigallocatechin gallate) and the like. The content of catechin reaches about 8 to 20% of that of dried green tea, and it is soluble in water and eluted into water when boiled with water. On the other hand, green tea contains various physiologically active substances. In particular, catechins reduce blood LDL cholesterol, thereby inhibiting the formation of blood clots and preventing arteriosclerosis, inhibiting the formation of lipid peroxide and preventing fat oxidation. It has been found that it is used as a natural antioxidant. In addition, green tea inhibits the growth of cancer and has anti-carcinogenic functions as well as anti-aging, and it is also known to have anti-toxin action to neutralize toxins, thereby preventing food poisoning.

It was said that the gold and silver flower refers to the bud part of the honeysuckle or its variants of the Honeysuckle family, and all of the stems, stems, leaves, and flowers are used for the herbaceous tree (本草綱目). Because flowers are clinically most effective, only flowers are now mostly used. Luteolin and inositol contain about 1%. In addition, saponin, tannin, and roniseline are included. (lonicerin, = luteolinrhamnoglucoside).

The aeyeop is a perennial herbaceous plant belonging to the asteraceae (compositae), and its extract is known to have an effect of prolonging blood clotting time.

The gwakhyang refers to the above-ground portion of baechohyang (Agastache rugosa).

The peppermint (Mentha arvensis var piperascens) is a dicotyledonous perennial plant of the order Lamiaceae, which has aromaticity in the plant itself and is erected and branched at the top. The main ingredients of mint are alpha-pinene (+,-), anisaldehyde, Daucosterol, Eugenol, Linalool, Menthone, (+ )-Neomenthol ((+)-Neomenthol) and the like.

The Eoseongcho (Houttuynia cordata) is an outpost of Yakmomil, a plant of the Saururaceae family, and inhabits Southeast Asia and, in particular, Japan, Korea, and the like. The Eoseongcho is also called ten medicine because it has ten medicinal effects. Eoseongcho can be used for medicinal and edible purposes, and it is classified as an animal and plant that can use only a minimum amount as an auxiliary ingredient in the Food Ingredients Classification of the Food Standards Code. In the private sector, it is used as a cosmetic and health functional food to help detox and beauty.

The aloe (Aloe vera L) refers to all the evergreen perennials of the genus Aloe, and is also called presbytery or wood presbytery in other words. It is a succulent plant native to Africa, and the leaves are thick sword-shaped and have thorns on the edge. The main ingredients are aloin, barbaloin, p-coumarinic acid, a small amount of α-glucose, a kind of aldopentose, protein and a lot of calcium oxalate. ) contains crystals of As pharmacological action, it has a laxative action on the large intestine, a wound healing action, and an anticancer action.

The gold (黃芩) is the root of Scutellaria baicalensis, a perennial herb belonging to the family Lamiaceae, and the root of gold contains baicalein, baicalin, wogonin, wogonoside, benzoic acid, β-sitosterol, etc., and antiviral, It is known to have antifungal, sedative, and anti-inflammatory effects.

The reason for using all eight kinds of raw materials in the present invention is that while effectively removing scalp wastes and lipid peroxide through interaction between each raw material, it lowers scalp heat and removes various contaminants and dandruff bacteria through antibacterial action to remove hair loss And it is because it is possible to prevent scalp troubles, if even one of the eight kinds of raw materials is lacking, the sufficient effect required by the present invention is not expressed.

The raw materials do not limit the mixing ratio, but when considering the cooling heat, lipid peroxide removal, and antibacterial effect, 50 to 150 parts by weight of gold and silver coins, 50 to 150 parts by weight of a leaf, 50 to 150 parts by weight of gwakhyang, Most preferably, mint 50 to 150 parts by weight, eoseongcho 50 to 150 parts by weight, aloe 50 to 150 parts by weight, and gold 50 to 150 parts by weight.

On the other hand, the present invention may further include 50 to 150 parts by weight of hair mussels, 50 to 150 parts by weight of Gabija, and 50 to 150 parts by weight of Ukriin, based on 100 parts by weight of green tea as the raw material. This is because, when the hairy dew, Gabija tree, and wokniin are further included, the effect of removing wastes and dandruff bacteria is more excellent, as well as the effect of cooling and heating significantly increased.

It is recorded that the hairy dew is a perennial herb of the needleaceae family that grows in the field, and was used in oriental medicine to reduce heat by detoxification. In the present invention, the outpost of the hairy dew can be used.

The Gabija tree (Cephalotaxus koreana) is a plant distributed in China, East India, Thailand, Japan and Korea, and is also called local birch (土香榧). In the present invention, one or more of the leaves and stems of the Gabija tree may be used.

The Ukriin (郁李仁) refers to the seeds of Prunus japonica Thunb var nakaii, P triloba var truncata Kom, P tomentosa Thunb, and P ishidoyana Nakai). .

The composition of the present invention maximizes the function of removing heat, antibacterial and lipid peroxide while increasing the extraction efficiency by fermenting the raw materials, ultrasonic extraction, plasma treatment, distillation extraction and filtering.

Specific methods for fermentation of the raw materials, ultrasonic extraction, plasma treatment, distillation extraction and filtering will be described in detail through the method for preparing the composition below.

The shampoo composition according to the present invention may include the above-mentioned extract as an active ingredient in the range of 0.1 to 50% by weight, but is not limited thereto. In this case, it is natural that the shampoo composition may further include various other known additives.

Hereinafter, a method for producing a shampoo composition according to the present invention will be described.

The method for producing a shampoo composition according to the present invention, as shown in FIG. 1, includes preparing raw materials including green tea, gold leaf, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold, and EM stock solution, molasses, and sea salt in the raw materials. and mixing and fermenting water, ultrasonically extracting the fermented raw material, plasma-treating the ultrasonically extracted extract, distilling the plasma-treated extract, and distilling the extracted extract It characterized in that it comprises the step of filtering.

Green tea, gold coins, Ayeop , Kwak Hyang , preparing raw materials including mint, eosincho, aloe and gold

First, raw materials including green tea, gold leaf, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold are prepared. At this time, the mixing ratio is based on 100 parts by weight of the green tea, 50 to 150 parts by weight of gold and silver coins, 50 to 150 parts by weight of aeop, 50 to 150 parts by weight of gwakhyang, 50 to 150 parts by weight of mint, 50 to 150 parts by weight of eoseongcho, 50 parts by weight of aloe. -150 parts by weight and 50-150 parts by weight of gold are most preferred.

In addition, as described above, it may be prepared by further mixing 50 to 150 parts by weight of hairy dew as a raw material, 50 to 150 parts by weight of Gabija, and 50 to 150 parts by weight of Ukriin.

Since the present invention utilizes only natural raw materials, there is no toxicity, and there is an advantage that it can be used stably without side effects.

to the raw material EM Mixing and fermenting the stock solution, molasses, sea salt and water

Next, 2-4% by weight of EM stock solution, 2-4% by weight of molasses, 0.5-1.5% by weight of sea salt, and the remainder of water are mixed with 10-20% by weight of the raw material and fermented for 2-4 days at 37-40 ℃ do. In this case, any of commercially available products may be used as the EM stock solution.

The reason for fermenting the raw materials prior to extraction in the present invention is that the high-temperature extraction method has a risk of destruction of the active ingredient, and the cold-chilled extraction method has the disadvantage that it takes a long extraction time, but using the fermentation method does not destroy the active ingredient. This is because the extraction efficiency can be increased even without it.

Ultrasonic extraction of the fermented raw material

Next, ultrasonic extraction of the fermented raw material increases the extraction efficiency.

At this time, the wavelength at the time of the ultrasonic extraction is sufficient if about 18 ~ 21KHz, and extraction at 40 ~ 50 ℃ 40 ~ 50 hours is sufficient, but is not limited thereto.

The ultrasonically extracted extract plasma steps to process

Next, the ultrasonically extracted extract is put into the tank of the liquid plasma treatment machine, and a voltage is applied to generate plasma to plasma-treat the extract, thereby maximizing the antibacterial, cooling heat and lipid peroxide removal efficacy of the extract.

At this time, the plasma is a low-temperature plasma that is generated through the discharge of electromagnetic waves by applying a voltage between the two electrodes to form an electric field, and is an atmospheric pressure plasma that generates plasma at atmospheric pressure. The liquid plasma processor includes a tank in which to-be-treated water is stored, first and second electrodes for generating plasma, a power source, and the like, and it is natural that the conventionally disclosed liquid plasma processor can be used without limitation. Since the liquid plasma treatment device is already well known in the art to which this technology belongs, a detailed description thereof will be omitted.

More specifically, the plasma treatment is performed by adding tourmaline powder and germanium powder to the ultrasonically extracted extract in a weight ratio of 1:0.01 to 0.1:0.01 to 0.1, and then putting it into a liquid plasma processor, and applying a voltage under a platinum catalyst. By applying plasma to generate plasma, plasma ionized particles from the tourmaline powder and germanium powder are deposited on the surface of the active ingredients in the extract, thereby further activating the function of the active ingredient.

The reason for plasma-treating the extract in the present invention is that by plasma-treating the active ingredient in the extract, the plasma-treated active ingredient is transformed and acts when combined with the bio-ions of the skin, thereby activating its function and entering the cell. This is because the effect can be maximized by speeding the delivery to the

At this time, the plasma generation voltage is about 4.5 ~ 20V, the frequency is sufficient if about 1 ~ 30kHz, the processing time is enough about 3 ~ 5 hours, but is not limited thereto.

remind plasma Distilling the treated extract

Next, the plasma-treated extract is distilled and extracted at a temperature of 70 to 90° C. for 0.5 to 12 hours using a vacuum distillation extractor.

The distilled extract to filter step

Next, the distilled extract is filtered using a qualitative filter paper or the like.

In addition, it is natural that the filtered extract can be concentrated, concentrated, or dried as needed.

The extract of the present invention prepared by the above method is used as an active ingredient in a shampoo composition to effectively lower the heat of the scalp, effectively removes dandruff and various harmful bacteria, and also cleanly washes waste materials such as lipid peroxide, so that the scalp It has the advantage of preventing troubles and hair loss.

Hereinafter, the present invention will be described in detail through examples.

(Example 1)

20 g each of green tea, gold ginseng flower, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold were prepared and mixed. Next, 30 g of EM stock solution, 30 g of molasses, 10 g of sea salt, and 770 g of water were mixed, and the mixture was fermented at 38.5° C. for 3 days.

Next, the fermented product was extracted at 48° C. for 48 hours at a wavelength of 19.7 KHz using an ultrasonic extractor.

And after adding tourmaline powder and germanium powder to the ultrasonically extracted extract in a weight ratio of 1:0.05:0.05, it was put into a liquid plasma processor, and 19V under a platinum catalyst (ultrasonic extracted extract and platinum catalyst 100:1 by weight) Plasma was generated for 4 hours at a voltage of 10 kHz and a frequency of 10 kHz. At this time, the particle size of the tourmaline powder and germanium powder was 200 mesh, respectively, the electrode for plasma generation was a tungsten rod material with a diameter of 26 mm, and the distance between the electrodes was constant at 0.5 mm using a thickness gauge.

Next, the plasma-treated extract was distilled and extracted at a temperature of 80° C. for 4 hours using a vacuum distillation extractor, which was filtered and filtered three times with Whatman No. 4 filter paper. And it was vacuum-concentrated and freeze-dried.

(Example 2)

It was carried out in the same manner as in Example 1, except that 15 g each of green tea, gold and silver flower, aeyeop, gwakhyang, mint, eoseongcho, aloe, goldenrod, hairy dew sedge, gabija leaf and urchinin were used as raw materials.

(Comparative Example 1)

20g each of green tea, gold leaf, aeyeop, gwakhyang, mint, eoseongcho, aloe, and gold were prepared and mixed, 10 times by weight of water was added thereto, extracted at 90°C for 12 hours, filtered, and this was filtered by Whatman No. .4 filtration with filter paper 3 times. And it was vacuum-concentrated and freeze-dried.

(Preparation Examples 1 and 2. Comparative Preparation Example 1 and Control)

A shampoo composition was prepared in the same amount as in Table 1 below.

Ingredients and mixing ratio of shampoo composition material name Preparation Example 1 Preparation 2 Comparative Preparation Example 1 control Sodium Laureth Sulfate 10 10 10 10 acrylate copolymer 30 30 30 30 Ammonium Lauryl Sulfate 3 3 3 3 Cocamidofurophil betaine 3 3 3 3 Example 1 10 - - - Example 2 - 10 - - Comparative Example 1 - - 10 - Purified water to 100 to 100 to 100 to 100

(Test Example 1)

The samples of Examples 1, 2 and Comparative Example 1 were each diluted in purified water to a concentration of 100 μg/mL.

Using the samples of Examples 1, 2 and Comparative Example 1, the antibacterial activity against dandruff bacteria (Malassezia furfur KCTC 7743) was tested. The dandruff-inducing strain Malassezia furfur KCTC7545 stored in 10% DMSO at 70°C was smeared on an agar plate using platinum lice and cultured at 37°C for 48 hours. One produced colony was inoculated into a broth medium using a platinum ear, and pre-cultured with shaking at 200 rpm in an incubator at 37° C. for 48 hours. A pre-cultured bacterial suspension and a sterilized 8 mm paper disk were prepared. The cultured bacterial suspension was diluted to a concentration of about ^{1 × 10 6 cells/ml.} After uniformly smearing the bacterial suspension on an agar plate with a sterilized cotton seed, it was allowed to stand for about 5 minutes so that the bacteria were completely absorbed into the medium. After the bacteria were completely absorbed, the prepared sample was inoculated by lifting a paper disk by 50 μl. After standing for 10 minutes, all samples were diffused and absorbed in the medium, and then an anaerobic atmosphere was created using a gas pack system (Merck Germany). After culturing at 37° C., which is the optimum temperature for growth of bacteria, and using erythromycin as a positive control, it was cultured for 48 hours to measure the diameter of the growth inhibitory ring, and the antibacterial activity was compared, and the result is shown in Table 2 below.

Test Example 1 Results sample Growth inhibitory ring diameter (mm) Example 1 21 Example 2 25 Comparative Example 1 13 erythromycin 20

As shown in Table 2, Examples 1 and 2 of the present invention confirmed that the antibacterial activity against dandruff bacteria was significantly superior to that of Comparative Example 1.

In addition, the antibacterial activity was also tested against Escherichia coli ATCC 25922 and Staphylococcus aureus ATCC 6538. After spreading each test strain on each sample, the initial state and the state after 24 hours were evaluated by measuring the concentration of the strain, and the test environment was 37.1±0.1° C. and 30.2±0.2% RH. The results were shown in Table 3 below.

Test Example 1 Results Test Items Test result Initial concentration (CFU/mL) Concentration after 24 hours (CFU/mL) Bacteria reduction rate (%) coli Blank 1.7×10 ⁴ 6.3×10 ⁴ Example 1 1.7×10 ⁴ <10 99.9 Example 2 1.7×10 ⁴ <10 99.9 Staphylococcus aureus Blank 1.3×10 ⁴ 4.2×10 ⁴ Example 1 1.3×10 ⁴ <10 99.9 Example 2 1.3×10 ⁴ <10 99.9

As shown in Table 3, it was confirmed that Examples 1 and 2 according to the present invention exhibit excellent antibacterial properties against E. coli and Staphylococcus aureus.

(Test Example 2)

40 adult males and females were divided into four groups, and the shampoo of Preparation Example 1 was given to group 1, the shampoo of Preparation Example 2 to group 2, the shampoo of Comparative Preparation Example 1 to group 3, and the shampoo of the control group to group 4, , was used once a day for 30 days.

In addition, cleaning power, scalp itchiness, scalp trouble, scalp fever, freshness, and overall feeling of use were evaluated. The evaluation area for the previous test items was set from 0 (very poor) to 10 (very satisfied), and the results are shown in Table 3 below.

Test Example 2 Results division detergency scalp itching scalp trouble scalp fever refreshing overall feeling of use Preparation Example 1 7.8 7.5 7.6 7.5 7.9 7.8 Preparation 2 8.5 8.0 8.3 8.1 8.4 8.3 Comparative Preparation Example 1 5.6 6.1 5.7 5.6 6.0 5.9 control 4.1 2.1 3.1 2.8 2.5 3.0

As shown in Table 3 above, it was confirmed that the shampoo according to the present invention received higher evaluation than Comparative Preparation Example 1 and the control group in all of the cleansing power, scalp itching, scalp trouble, scalp heat loss, freshness and overall feeling of use.

The description of the present invention described above is for illustration, and those of ordinary skill in the art to which the present invention pertains can understand that it can be easily modified into other specific forms without changing the technical spirit or essential features of the present invention. will be. Therefore, it should be understood that the embodiments described above are illustrative in all respects and not restrictive. For example, each component described as a single type may be implemented in a dispersed form, and likewise components described as distributed may be implemented in a combined form.

The scope of the present invention is indicated by the following claims, and all changes or modifications derived from the meaning and scope of the claims and their equivalents should be construed as being included in the scope of the present invention.

Claims (4)

delete A step of preparing raw materials including green tea, gold leaf, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold;
mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water;
Ultrasonic extraction of the fermented raw material;
Plasma treatment of the ultrasonically extracted extract;
Distilling the plasma-treated extract and extracting;
Filtering the distillation-extracted extract,
The plasma treatment is
After adding tourmaline and germanium to the ultrasonically extracted extract, a method for producing a shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function, characterized in that plasma treatment is performed under a platinum catalyst.
A step of preparing raw materials including green tea, gold leaf, aeyeop, gwakhyang, mint, eoseongcho, aloe and gold;
mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water;
Ultrasonic extraction of the fermented raw material;
Plasma treatment of the ultrasonically extracted extract;
Distilling and extracting the plasma-treated extract;
Filtering the distillation-extracted extract,
The raw material is a method of producing a shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function, characterized in that it further comprises hairy dew, gabija tree and urchinin.
A shampoo composition having a cooling heat, antibacterial and lipid peroxide removal function, characterized in that it is prepared by the method of claim 2 or 3.

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