KR102299413B1 - Scalp composition and manufacturing mehtod thereof - Google Patents

Abstract

The present invention relates to a composition for the scalp having a deodorizing and antibacterial effect, and a method for manufacturing the same, and more particularly, to preparing a raw material containing cypress, arborvitae, Eugeunpi, mint, cinnamon, quince, yellow lily, and mulberry bark; , mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water, ultrasonically extracting the fermented raw material, plasma-treating the ultrasonically extracted extract, and distilling the plasma-treated extract It is characterized in that it comprises the step of extracting, and filtering the distillation-extracted extract. According to the present invention, there is an advantage in that the condition of the scalp can be improved by sterilizing dandruff bacteria and contaminants present on the scalp and providing a deodorizing effect.

Description

A composition for scalp having a deodorizing and antibacterial effect, and a method for manufacturing the same

The present invention relates to a composition for scalp having an odor removal and antibacterial effect and a method for manufacturing the same, and more particularly, it contains cypress, arborvitae, Eugeunpi, peppermint, cinnamon, quincea, yellow lily, and mulberry bark as active ingredients. Fermentation, ultrasonic extraction, plasma treatment and distillation extraction, as well as increasing the extraction efficiency, and relates to a composition for the scalp that can maximize the odor removal and antibacterial effect, and a method for producing the same.

In general, when washing your hair, shampoo or soap is used to wash away accumulated or attached sebum, sweat, dead skin cells, wastes, and dust on the scalp. are doing

However, conventional shampoos and rinses mainly use chemicals, so there is a risk of irritation to the skin, and there is a disadvantage that a sterilizing effect against dandruff bacteria and contaminants cannot be expected.

In addition, no matter how much shampoo or soap is used to wash the hair, there is no antibacterial effect, and after a certain period of time has elapsed, the scalp is contaminated again, causing itching and odor caused by various bacteria.

In order to solve this problem, the use of scented shampoo, various hair mists, antibacterial shampoo, etc. has been proposed, but these scented shampoos or mists are only temporary and have no antibacterial and deodorizing effects, so there is a problem of generating bad odors over time. Shampoo also used chemicals to increase cleaning power, but had the disadvantage that the antibacterial effect was insignificant.

Therefore, it has been required to develop a composition for the scalp that can sterilize various contaminants and dandruff bacteria on the scalp, impart a deodorizing effect, and prevent itchiness by using a natural material rather than a chemical synthetic material.

KR 10-2009-0092899 A

Accordingly, an object of the present invention is to provide a composition for the scalp and a method for producing the same, which effectively sterilizes dandruff and contaminants present on the scalp, and has a deodorizing and antibacterial effect capable of improving the scalp condition with an excellent deodorizing action.

The composition for scalp having a deodorizing and antibacterial effect of the present invention for achieving the above object, and a method for producing the same, are prepared by preparing a raw material comprising cypress, arborvitae, Eugeunpi, peppermint, cinnamon, quince, yellow lily and mulberry bark. and mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water, ultrasonically extracting the fermented raw material, plasma-treating the ultrasonically extracted extract, and the plasma-treated extract It is characterized in that it comprises the steps of distillation extraction, and filtering the distillation-extracted extract.

The plasma treatment is characterized in that after adding tourmaline and germanium to the ultrasonically extracted extract, plasma treatment is performed under a platinum catalyst.

The raw material is characterized in that it further comprises a hairy dew, Gabija tree and Ukriin.

The composition for scalp having a deodorizing and antibacterial effect according to the present invention is characterized in that it is prepared through the above-described method.

According to the present invention, there is an advantage in that the condition of the scalp can be improved by sterilizing dandruff bacteria and contaminants present on the scalp and providing a deodorizing effect.

1 is a flow chart showing the manufacturing process of a composition for scalp having an odor removal and antibacterial effect according to the present invention.

Hereinafter, the present invention will be described in detail.

First, the composition for scalp according to the present invention has the greatest characteristic in that it has excellent odor removal and antibacterial effects as an external composition, thereby improving the scalp condition, that is, improving dandruff, itchiness, and preventing troubles and hair loss.

The composition for scalp according to the present invention includes, as an active ingredient, an extract of raw materials including cypress, arborvitae, Eugeunpi, mint, cinnamon, quince, yellow lily and mulberry, wherein the extract is fermented by raw materials, ultrasonic extraction, plasma treatment , characterized in that it is distilled and filtered.

The raw materials used in the present invention will be briefly described.

The cypress (Chamaecyparis obtusa) is a coniferous tree that has been successfully grown and settled in the southern regions of Korea after being planted in the southern regions of Korea, called cypress (檜木), hinoki, and cypress, which are native to Japan. The amount of phytoncide from cypress is superior to that of other hardwoods, so you can keep your scalp healthy and clean with its natural antibacterial effect. In the present invention, one or more of the leaves and roots of the cypress tree may be used.

The lateral leaf is a leaf of an evergreen tree of the coniferous arboraceae family, an evergreen, obovate or ovate, scaly, and both sides are green or light yellow-green with some white spots. Arborvitae leaf is known to contain a lot of phytoncide, a natural antibacterial component.

The eugeunpi refers to the root bark of the so-called elm tree, and the bark of the elm stem is called yubaekpi (楡白皮). The scientific name is Ulmus davidiana. It has been used medicinally by peeling the root bark in early spring or autumn. In Donguibogam, it is recorded that the elm tree has a flat nature, sweet taste, and is soft without poison. .

The peppermint (Mentha arvensis var piperascens) is a dicotyledonous perennial plant of the order Lamiaceae, which has aromaticity in the plant itself and is erected and branched at the top. The main ingredients of mint are alpha-pinene (+,-), anisaldehyde, Daucosterol, Eugenol, Linalool, Menthone, (+ )-Neomenthol ((+)-Neomenthol) and the like.

The cinnamon is a medicinal herb made from the bark of cassia belonging to the camphoraceae (Cinnamomum aromaticum Nees, Cinnamomum cassia auct, Cinnamomum cassia J Presl, Cinnamomum zeylanicum Blume var cassia Nees, Cinnamomum japonicum SIEB, Cinnamomum cassia BLUME). Cinnamon is called broiler chicken in oriental medicine and is mainly used for the treatment of anorexia and indigestion as a stomach acid.

The Galla Rhois refers to a nest formed by a stab wound of a rhus javanica L or a member of the family Rhus javanica L. They are called saphenous lobster, red buoyancy, anastomosis, and white chungchang. Obaeja is an irregular pouch shape, resembling the shape of a human ear, and is empty inside and has a very sour taste. Obaeja mainly contains 50-60% of tannins, so it is used as a raw material for tannins, hair dyes and inks.

The yellow lily (黃連) is an evergreen perennial plant of the Dicotyledonous Hemiptera, Heteroptera, which is native to China, but is also cultivated in Korea, Japan, and China for medicinal purposes, and is distributed in Russia and North America, and various species around the world. exist. In oriental medicine, the roots of 5 to 6 years old yellow lotus planted in November are collected and dried in the sun.

The Moutan Cortex Radicis refers to the root bark of the Paeoniaceae family, and the ingredients include paeonoside, paeonolide and paeonol, and paeonoside decomposes during storage to form sugars and phaeonols. As pharmacological action, antipyretic, anti-inflammatory, antithrombotic, anti-allergic, etc. have been reported.

The reason for using all of the eight kinds of raw materials in the present invention is to improve the scalp condition by significantly increasing the antibacterial and deodorizing effects through the interaction between the respective raw materials. This is because the sufficient effect required for this is not expressed.

The raw materials do not limit the mixing ratio, but when considering the antibacterial and deodorant effects, based on 100 parts by weight of the cypress, 50 to 150 parts by weight of arborvitae, 50 to 150 parts by weight of Eugeun skin, 50 to 150 parts by weight of mint, 50 parts by weight of cinnamon Most preferably, it is 150 parts by weight, 50 to 150 parts by weight of quince, 50 to 150 parts by weight of hwangryeon, and 50 to 150 parts by weight of mulberry skin.

On the other hand, the present invention may further comprise 50 to 150 parts by weight of hairy dew, 50 to 150 parts by weight of cypress tree, and 50 to 150 parts by weight of Ukriin, as the raw material, based on 100 parts by weight of cypress. This is because it has a more excellent antibacterial and deodorizing effect when it further includes the hairy dew, Gabija tree, and Ukriin.

It is recorded that the hairy dew is a perennial herb of the needleaceae family that grows in the field, and was used in oriental medicine to reduce heat by detoxification. In the present invention, the outpost of the hairy dew can be used.

The Gabija tree (Cephalotaxus koreana) is a plant distributed in China, East India, Thailand, Japan and Korea, and is also called local birch (土香榧). In the present invention, one or more of the leaves and stems of the Gabija tree may be used.

The Ukriin (郁李仁) refers to the seeds of Prunus japonica Thunb var nakaii, P triloba var truncata Kom, P tomentosa Thunb, and P ishidoyana Nakai). .

The composition of the present invention maximizes the antibacterial and deodorizing functions while increasing the extraction efficiency by fermenting the raw materials, ultrasonic extraction, plasma treatment, distillation extraction and filtering.

Specific methods for fermentation of the raw materials, ultrasonic extraction, plasma treatment, distillation extraction and filtering will be described in detail through the method for preparing the composition below.

The composition for scalp according to the present invention may include the above extract as an active ingredient in the range of 0.1 to 50% by weight, but is not limited thereto. In this case, it is natural that the composition for the scalp may further include various other known additives as an external preparation for skin.

Hereinafter, a method for producing the composition for scalp according to the present invention will be described.

The manufacturing method of the shampoo composition according to the present invention includes the steps of preparing a raw material including cypress, arborvitae, Eugeunpi, peppermint, cinnamon, quince, fenugreek, and mulberry bark, as shown in FIG. 1, and EM stock solution, molasses, Mixing and fermenting sea salt and water; ultrasonically extracting the fermented raw material; plasma-treating the ultrasonically extracted extract; distilling the plasma-treated extract; It is characterized in that it comprises the step of filtering the extract.

cypress, arborvitae , You Geun-Pi , mint, cinnamon, pear, goldthread And preparing a raw material comprising a wood dandelion skin

First, prepare raw materials including cypress, arborvitae, eugeunpi, mint, cinnamon, quince, hwangryeon and mulberry. At this time, the mixing ratio is based on 100 parts by weight of the cypress, 50 to 150 parts by weight of arborvitae, 50 to 150 parts by weight of Eugeunpi, 50 to 150 parts by weight of mint, 50 to 150 parts by weight of cinnamon, 50 to 150 parts by weight of quince Most preferably, it is 50 to 150 parts by weight and 50 to 150 parts by weight of mulberry skin.

In addition, as described above, it may be prepared by further mixing 50-150 parts by weight of hair dew as a raw material, 50-150 parts by weight of Gabija, and 50-150 parts by weight of Ukriin.

Since the present invention utilizes only natural raw materials, there is no toxicity, and there is an advantage that it can be used stably without side effects.

to the raw material EM Mixing and fermenting the stock solution, molasses, sea salt and water

Next, 2-4% by weight of EM stock solution, 2-4% by weight of molasses, 0.5-1.5% by weight of sea salt, and the remainder of water are mixed with 10-20% by weight of the raw material and fermented for 2-4 days at 37-40 ℃ do. In this case, any of commercially available products may be used as the EM stock solution.

The reason for fermenting the raw materials prior to extraction in the present invention is that the high-temperature extraction method has a risk of destruction of the active ingredient, and the cold-chilled extraction method has the disadvantage that it takes a long extraction time, but using the fermentation method does not destroy the active ingredient. This is because the extraction efficiency can be increased even without it.

Ultrasonic extraction of the fermented raw material

Next, ultrasonic extraction of the fermented raw material increases the extraction efficiency.

At this time, the wavelength at the time of the ultrasonic extraction is sufficient if about 18 ~ 21KHz, and extraction at 40 ~ 50 ℃ 40 ~ 50 hours is sufficient, but is not limited thereto.

The ultrasonically extracted extract plasma steps to process

Next, by injecting the ultrasonically extracted extract into the water tank of the liquid plasma treatment machine, and applying a voltage to generate plasma to plasma-treat the extract, the antibacterial and deodorant efficacy of the extract is maximized.

At this time, the plasma is a low-temperature plasma that is generated through the discharge of electromagnetic waves by applying a voltage between the two electrodes to form an electric field, and is an atmospheric pressure plasma that generates plasma at atmospheric pressure. The liquid plasma processor includes a tank in which to-be-treated water is stored, first and second electrodes for generating plasma, a power source, and the like, and it is natural that the conventionally disclosed liquid plasma processor can be used without limitation. Since the liquid plasma treatment device is already well known in the art to which this technology belongs, a detailed description thereof will be omitted.

More specifically, the plasma treatment is performed by adding tourmaline powder and germanium powder to the ultrasonically extracted extract in a weight ratio of 1:0.01 to 0.1:0.01 to 0.1, and then putting it into a liquid plasma processor, and applying a voltage under a platinum catalyst. By applying plasma to generate plasma, plasma ionized particles from the tourmaline powder and germanium powder are deposited on the surface of the active ingredients in the extract, thereby further activating the function of the active ingredient.

The reason for plasma-treating the extract in the present invention is that by plasma-treating the active ingredient in the extract, the plasma-treated active ingredient is transformed and acts when combined with the bio-ions of the skin, thereby activating its function and entering the cell. This is because the effect can be maximized by speeding the delivery to the

At this time, the plasma generation voltage is about 4.5 ~ 20V, the frequency is sufficient if about 1 ~ 30kHz, the processing time is enough about 3 ~ 5 hours, but is not limited thereto.

remind plasma Distilling the treated extract

Next, the plasma-treated extract is distilled and extracted at a temperature of 70 to 90° C. for 0.5 to 12 hours using a vacuum distillation extractor.

The distilled extract to filter step

Next, the distilled extract is filtered using a qualitative filter paper or the like.

In addition, it is natural that the filtered extract can be concentrated, concentrated, or dried as needed.

The extract of the present invention prepared by the above method has the advantage that it is used as an active ingredient in the composition for the scalp and significantly improves the condition of the scalp due to its antibacterial and deodorizing functions.

Hereinafter, the present invention will be described in detail through examples.

(Example 1)

20 g each of cypress leaves, arborvitae leaf, eugeunpi, mint, cinnamon, quince, and mulberry bark were prepared and mixed. Next, 30 g of EM stock solution, 30 g of molasses, 10 g of sea salt, and 770 g of water were mixed, and the mixture was fermented at 38.5° C. for 3 days.

Next, the fermented product was extracted at 48° C. for 48 hours at a wavelength of 19.7 KHz using an ultrasonic extractor.

And after adding tourmaline powder and germanium powder to the ultrasonically extracted extract in a weight ratio of 1:0.05:0.05, it was put into a liquid plasma processor, and 19V under a platinum catalyst (ultrasonic extracted extract and platinum catalyst 100:1 by weight) Plasma was generated for 4 hours at a voltage of 10 kHz and a frequency of 10 kHz. At this time, the particle size of the tourmaline powder and germanium powder was 200 mesh, respectively, the electrode for plasma generation was a tungsten rod material with a diameter of 26 mm, and the distance between the electrodes was constant at 0.5 mm using a thickness gauge.

Next, the plasma-treated extract was distilled and extracted at a temperature of 80° C. for 4 hours using a vacuum distillation extractor, which was filtered and filtered three times with Whatman No. 4 filter paper. And it was vacuum-concentrated and freeze-dried.

(Example 2)

It was carried out in the same manner as in Example 1, except that 15 g each of cypress leaves, arborvitae leaf, eugeunpi, mint, cinnamon, quince, yellow rhubarb, mulberry bark, hairy dew outpost, gabija leaf, and ukniin were used as raw materials.

(Comparative Example 1)

20 g each of cypress leaf, arborvitae leaf, Eugeun skin, mint, cinnamon, quince leaf, yellow rhubarb, and mulberry bark were prepared and mixed, 10 times by weight of water was added thereto, extracted at 90° C. for 12 hours, filtered, and the resultant Filtered by filtration three times with No.4 filter paper. And it was vacuum-concentrated and freeze-dried.

(Test Example 1)

The samples of Examples 1, 2 and Comparative Example 1 were each diluted in purified water to a concentration of 100 μg/mL.

Using the samples of Examples 1, 2 and Comparative Example 1, the antibacterial activity against dandruff bacteria (Malassezia furfur KCTC 7743) was tested. The dandruff-inducing strain Malassezia furfur KCTC7545 stored in 10% DMSO at 70°C was smeared on an agar plate using platinum lice and cultured at 37°C for 48 hours. One produced colony was inoculated into a broth medium using a platinum ear, and pre-cultured with shaking at 200 rpm in an incubator at 37° C. for 48 hours. A pre-cultured bacterial suspension and a sterilized 8 mm paper disk were prepared. The cultured bacterial suspension was diluted to a concentration of about ^{1 × 10 6 cells/ml.} After uniformly smearing the bacterial suspension on an agar plate with a sterilized cotton seed, it was allowed to stand for about 5 minutes so that the bacteria were completely absorbed into the medium. After the bacteria were completely absorbed, the prepared sample was inoculated by lifting a paper disk by 50 μl. After standing for 10 minutes, all samples were diffused and absorbed in the medium, and then an anaerobic atmosphere was created using a gas pack system (Merck Germany). After culturing at 37° C., which is the optimum temperature for growth of bacteria, and using erythromycin as a positive control, it was cultured for 48 hours to measure the diameter of the growth inhibitory ring, and the antibacterial activity was compared, and the result is shown in Table 1 below.

Test Example 1 Results sample Growth inhibitory ring diameter (mm) Example 1 21 Example 2 25 Comparative Example 1 13 erythromycin 20

As shown in Table 1, it was confirmed that Examples 1 and 2 of the present invention had significantly superior antibacterial activity against dandruff bacteria compared to Comparative Example 1.

In addition, the antibacterial activity was also tested against Escherichia coli ATCC 25922 and Staphylococcus aureus ATCC 6538. After spreading each test strain on each sample, the initial state and the state after 24 hours were evaluated by measuring the concentration of the strain, and the test environment was 37.1±0.1° C. and 30.2±0.2% RH. The results are shown in Table 2 below.

Test Example 1 Results Test Items Test result Initial concentration (CFU/mL) Concentration after 24 hours (CFU/mL) Bacteria reduction rate (%) coli Blank 1.7×10 ⁴ 6.3×10 ⁴ Example 1 1.7×10 ⁴ <10 99.9 Example 2 1.7×10 ⁴ <10 99.9 Staphylococcus aureus Blank 1.3×10 ⁴ 4.2×10 ⁴ Example 1 1.3×10 ⁴ <10 99.9 Example 2 1.3×10 ⁴ <10 99.9

As shown in Table 2, it was confirmed that Examples 1 and 2 according to the present invention exhibit excellent antibacterial properties against E. coli and Staphylococcus aureus.

(Test Example 2)

The samples of Examples 1, 2 and Comparative Example 1 were each diluted in purified water to a concentration of 100 μg/mL.

The method as follows for 5-androst-16-en-3-one (5-androst-16-en-3-one, Aldrich, USA), which is a representative substance of a body odor source among substances that have been identified so far to compare the degree of deodorization.

After putting 1 ml of sample and 1 ml of 5-alpha-androst-16-en-3-one (1% dilution in ethanol) into the flask and sealing it, 30 minutes later, three sensory evaluation specialists make the judgment as shown in Table 3 below. After smelling according to the criteria, the evaluation scores were averaged. And the results are shown in Table 4 below.

Criteria for Test Example 2 score Evaluation standard 0 No smell at all. One very weak odor 2 weak odor 3 odor is normal 4 strong smell 5 Very strong smell (Blank)

Results of Test Example 2 division Example 1 Example 2 Comparative Example 1 Blank score 2.5 1.6 3.1 5.0

As shown in Table 4, it was confirmed that Examples 1 and 2 according to the present invention had an excellent deodorizing effect on 5-androst-16-en-3-one, which is a odor source.

(Test Example 3)

The samples of Examples 1, 2 and Comparative Example 1 were each diluted in purified water to a concentration of 100 μg/mL.

100ppm and 30ppm of ammonia and trimethylamine, respectively, were injected into each Tedlabag, which is a test container of 10L capacity, and then 10ml of the sample was injected into the Tedlarbag. Thereafter, the concentrations of ammonia and trimethylamine at 0.5 hours, 1 hour, 2 hours, 4 hours and 6 hours were measured. It was tested in the same way without adding a sample, and it was set as a blank test. And the results are shown in Tables 5 and 6 below.

Deodorizing effect on ammonia according to Test Example 3 (unit: ppm) hour blank test Example 1 Example 2 Comparative Example 1 initial concentration 100 100 100 100 0.5 hours 100 13 5 42 1 hours 100 8 3 25 2 hours 100 5 2 15 4 hours 100 4 less than 1 8 6 hours 100 3 less than 1 5

Deodorizing effect on trimethylamine according to Test Example 3 (unit: ppm) hour blank test Example 1 Example 2 Comparative Example 1 initial concentration 30 30 30 30 0.5 hours 30 8 5 14 1 hours 29 5 2 10 2 hours 28 3 less than 1 5 4 hours 28 less than 1 less than 1 3 6 hours 28 less than 1 less than 1 3

As shown in Tables 5 and 6, it was confirmed that Examples 1 and 2 according to the present invention had excellent deodorizing effects on ammonia and trimethylamine compared to Comparative Example 1.

(Test Example 4)

The samples of Examples 1, 2 and Comparative Example 1 were each diluted in purified water to a concentration of 100 μg/mL.

60 adult males and females were divided into three groups, Example 1 was given to group 1, Example 2 to group 2, and Example 3 to group 3, and 10 ml of the provided composition was sufficiently applied to the scalp and hair. After 3 months of use, the results were observed.

To determine the effect, the improvement of scalp odor, scalp itchiness, scalp trouble, dandruff, and hair loss was evaluated in 9 steps as an evaluation scale and the overall improvement was evaluated. was given. The results were shown in Table 7 below.

Test Example 4 Results division scalp smell scalp itching scalp trouble dandruff hair loss overall improvement Example 1 7.8 7.5 7.6 7.5 7.9 7.8 Example 2 8.5 8.0 8.3 8.1 8.4 8.3 Comparative Example 1 5.6 6.1 5.7 5.6 6.0 5.9

As shown in Table 7, it was confirmed that Examples 1 and 2 according to the present invention received higher evaluation than Comparative Example 1 in all of the scalp odor, scalp itchiness, scalp trouble, dandruff, hair loss, and overall improvement.

The description of the present invention described above is for illustration, and those of ordinary skill in the art to which the present invention pertains can understand that it can be easily modified into other specific forms without changing the technical spirit or essential features of the present invention. will be. Therefore, it should be understood that the embodiments described above are illustrative in all respects and not restrictive. For example, each component described as a single type may be implemented in a distributed manner, and likewise components described as distributed may be implemented in a combined form.

The scope of the present invention is indicated by the following claims, and all changes or modifications derived from the meaning and scope of the claims and their equivalents should be construed as being included in the scope of the present invention.

Claims (4)

A step of preparing raw materials including cypress, arborvitae, eugeunpi, mint, cinnamon, quince, yellow rhubarb and mulberry bark;
mixing and fermenting the raw material with EM stock solution, molasses, sea salt and water;
Ultrasonic extraction of the fermented raw material;
Plasma treatment of the ultrasonically extracted extract;
Distilling the plasma-treated extract and extracting;
Method for producing a composition for scalp having a deodorizing and antibacterial effect, characterized in that it comprises the step of filtering the distilled extract.
According to claim 1,
The plasma treatment is
After adding tourmaline stone and germanium to the ultrasonically extracted extract, a method for producing a composition for scalp having a deodorizing and antibacterial effect, characterized in that the plasma treatment is performed under a platinum catalyst.
According to claim 1,
The raw material is a method for producing a composition for the scalp having a deodorizing and antibacterial effect, characterized in that it further comprises a hairy dew, a birch tree, and an urchin.
[Claim 4] A composition for scalp having a deodorizing and antibacterial effect, characterized in that it is prepared by the method of any one of claims 1 to 3.

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