KR102221867B1 - Cosmetic composition having extracts of fresh and entrails of avalone, and manufacturing method thereof - Google Patents

Abstract

The present invention relates to a method for manufacturing a cosmetic composition containing flesh and entrails of abalone comprising the following steps: (a) preparing flesh and entrails of abalone; (b) based on 100 parts by weight of the abalone flesh, mixing 0.1 to 30 parts by weight of abalone entrails, 0.1 to 5 parts by weight of a green plum fermented solution, and 30 to 150 parts by weight of sugar, fermenting the same at 30 to 37°C for 1 to 6 months, and then filtering the same to manufacture a primary fermentation solution; (c) based on 100 parts by weight of the first fermentation solution, mixing and stirring 10 to 150 parts by weight of purified water, and 1 to 5 parts by weight of a Nipa palm extract to manufacture a secondary fermentation solution; (d) standing the secondary fermentation solution at 2 to 5°C for 12 to 24 hours; (e) based on 100 parts by weight of the second fermentation solution that has been left standing, mixing 30 to 250 parts by weight of ethyl alcohol, and 1 to 3 parts by weight of vitamin C, heating the same at 35 to 40°C for 10 to 12 hours, followed by filtering the same. Therefore, the present invention has an effect of mass-producing a cosmetic composition having high whitening and anti-oxidation effects.

Description

Cosmetic composition having extracts of fresh and entrails of avalone, and manufacturing method thereof

The present invention relates to a cosmetic composition containing abalone meat and abalone intestine extract, and a method for producing the same.

Republic of Korea Patent Publication No. 10-2016-0079979 (published date: 2016.07.07., title of invention: skin wrinkle improvement or whitening cosmetic composition containing abalone mucus as an active ingredient) is separated from abalone mucus or abalone mucus Comprising the obtained glycoprotein as an active ingredient, wherein the abalone mucous fluid secretes the mucous fluid from the abalone and then filtering; And dialysis of the filtered mucous solution and centrifugation to obtain a supernatant.

This prior art has an effect of improving wrinkles through inhibitory activities of hyaluronic acid degrading enzyme and elastin degrading enzyme; At the same time, since it has a skin whitening effect through tyrosinase inhibitory activity, the composition of the present invention containing it as an active ingredient can effectively improve the wrinkles of the skin, and also claims that it can be usefully used as a whitening functional cosmetic composition. On the other hand, the abalone mucus liquid, which is a portion of the supernatant obtained by centrifuging the dialysis process, has a disadvantage in that the yield is low because abalone cannot be used as a whole.

In addition, Republic of Korea Patent Registration No. 1982510 (registration date: May 21, 2019, title of the invention: a cosmetic composition containing a complex consisting of a seaweed mixture extract and a mixture of dogtail and violet extract) is a mixture of hepatitis, agara, maternal, seaweed and Ecklonia. Contains 0.001 to 30% by weight of a composite consisting of a mixed extract of dogtail and violet, prepared by mixing the extract, dogtail, and violet in a weight ratio of 3:1, and mixing the tot, walnut agar, hatban, seaweed and Ecklonia cava The extract is prepared by supercritical extraction by mixing tot, agaric, mackerel, seaweed, and Ecklonia in a weight ratio of 1-4:1-4:1-4:1-4:1-4, respectively, and the complex is A cosmetic composition for skin moisturizing, skin barrier protection and skin elasticity improvement, characterized in that it consists of a ratio of 90 to 99% by weight of a mixed extract of agaric agar, mother and child, seaweed and Ecklonia cava, and 1 to 10% by weight of a mixed extract of dogtail and violets is disclosed. have.

This prior art, while being safe for the human body, exhibits excellent skin moisturizing, skin barrier protection, and anti-aging effects due to its synergistic effect, so that it can be usefully used as a cosmetic, but there is a fundamental problem with a complex composition.

An object of the present invention created to solve the above problems is to provide a cosmetic composition containing abalone meat and abalone visceral extract, which can maximize the yield of active ingredients by using abalone and intestines as a whole, and a method for manufacturing the same Have.

The object of the present invention, (a) and the steps of preparing abalone and abalone intestines; (b) With respect to 100 parts by weight of the abalone meat, 0.1 to 30 parts by weight of abalone intestines, 0.1 to 5 parts by weight of fermented green plum, and 30 to 150 parts by weight of sugar are mixed, fermented at 30 to 37°C for 1 to 6 months, and then filtered. Preparing a primary fermentation broth; (c) mixing and stirring 10 to 150 parts by weight of purified water and 3 to 5 parts by weight of Hwangchil tree extract based on 100 parts by weight of the first fermentation broth to prepare a secondary fermentation broth; (d) allowing the secondary fermentation broth to stand at 2 to 5° C. for 12 to 24 hours; (e) mixing 30 to 250 parts by weight of ethyl alcohol and 1 to 3 parts by weight of vitamin C based on 100 parts by weight of the secondary fermentation broth, followed by heating at 35 to 40°C for 10 to 12 hours, followed by filtering. It can be achieved by a method for producing a cosmetic composition containing abalone meat and abalone intestine extract.

Preferably, the abalone of the step (a) of the present invention is 5 to 30 parts by weight of healthy abalone, with respect to 100 parts by weight of live abalone, and the abalone intestine is characterized in that the gallbladder part is removed.

Preferably, the green plum extract of the present invention is (a) 50 to 250 parts by weight of purified water, 1 to 30 parts by weight of oligosaccharide or sugar, and 0.01 to 3 parts by weight of kimchi lactic acid bacteria based on 100 parts by weight of chopped green plums. Fermenting at 35 to 39° C. for 14 to 21 days to prepare a first fermented green plum fermentation broth; (B) mixing and stirring 3 to 5 parts by weight of grapefruit seed powder, 200 to 500 parts by weight of purified water, and 0.1 to 0.3 parts by weight of sea salt with respect to 100 parts by weight of the first fermentation broth; (C) With respect to 100 parts by weight of the secondary green plum fermentation broth, 500 to 1,000 parts by weight of purified water is added, heated at 80 to 95°C for 100 to 120 minutes, and then filtered.

Preferably, the Hwangchil wood extract of the present invention is (a) mixed with 5,000 to 10,000 parts by weight of purified water based on 100 parts by weight of hwangchil wood powder and heated at 85 to 120°C for 18 to 22 hours to obtain the first Hwangchil wood extract. Manufacturing; (B) mixing 150 to 200 parts by weight of ethyl alcohol with respect to 100 parts by weight of the first Hwangchil tree extract, followed by stirring for 24 to 36 hours, followed by filtering to prepare a second Hwangchil tree extract; (C) It is characterized in that it is prepared by mixing 30 to 50 parts by weight of purified water with respect to 100 parts by weight of the second Hwangchil tree extract, heating at 50 to 65°C for 10 to 12 hours, and then filtering.

Another object of the present invention can be achieved by a cosmetic composition prepared by any one of the above methods.

The present invention as described above has the effect of mass-producing a cosmetic composition having high whitening and antioxidant effects.

Hereinafter, it will be described with reference to an embodiment of the present invention.

-Manufacture of cosmetic composition containing abalone meat and abalone intestine extract

1. Preparation of abalone meat and abalone intestines

In this embodiment, live abalone and healthy abalone can be used together.

In addition, the abalone meat is 5 to 30 parts by weight of healthy abalone, and the abalone intestines are preferably removed from the gallbladder. The reason is that the gallbladder is concentrated in parasites, and a cosmetic to be produced later This is because it adversely affects the turbidity and aroma of the composition.

2. Manufacture of primary fermentation broth

The primary fermentation broth is mixed with 0.1 to 30 parts by weight of abalone intestines, 0.1 to 5 parts by weight of green plum fermentation broth, and 30 to 150 parts by weight of sugar based on 100 parts by weight of abalone, then fermented at 30 to 37°C for 1 to 6 months and then filtered. It is manufactured by

The green plum fermentation broth of this embodiment is to help prevent the growth of spoilage bacteria and to help whitening effect.

Green plum contains a large amount of picric acid and citric acid, so it has the effect of making the intestines comfortable by removing harmful bacteria in the large intestine and decomposing toxic substances. In addition to relieving fatigue and relieving hangovers, pyruvic acid and picric acid reduce the toxicity accumulated in the liver. It is known to have the effect of improving liver function by loosening. In addition, Cheongmaesil has the effect of improving anorexia and digestive function, and citric acid contained in a large amount removes lactic acid, which is a muscle fatigue substance that occurs after excessive exercise, and aids in rapid supply of nutrients to the muscles. When used as such, the green plum is toxic, so it is heated or fermented as in this example.

The green plum fermentation broth of this example is, with respect to 100 parts by weight of chopped green plums, 50 to 250 parts by weight of purified water, 1 to 30 parts by weight of oligosaccharide or sugar, and 0.01 to 3 parts by weight of kimchi lactic acid bacteria are mixed, and then 14 to 21 at 35 to 39°C. Fermenting for a day to prepare a first fermented green plum; Mixing and stirring 3 to 5 parts by weight of grapefruit seed powder, 200 to 500 parts by weight of purified water, and 0.1 to 0.3 parts by weight of sea salt based on 100 parts by weight of the first green plum fermentation broth to prepare a second fermentation broth; It is prepared by adding 500 to 1,000 parts by weight of purified water to 100 parts by weight of the secondary green plum fermentation broth, heating it at 80 to 95°C for 100 to 120 minutes, and then filtering it, and kimchi lactic acid bacteria are provided to prevent spoilage from spoiling the fermentation broth. . In addition, it has been verified that the fermented liquid of Cheongmaesil has a whitening effect as disclosed in Patent No. 1491463.

3. Second fermentation broth manufacturing

The secondary fermentation broth is prepared by mixing and stirring 10 to 150 parts by weight of purified water and 3 to 5 parts by weight of Hwangchil tree extract based on 100 parts by weight of the primary fermentation broth.

Here, Hwangchil tree improves liver function, anticancer effect, improves cholesterol levels and improves adult diseases, which helps in blood sugar management, improves immunity, and stabilizes nerves because it contains a large amount of sesquiterpene to relieve depression, insomnia, and stress. It is known to be effective.

Hwangchil tree extract of this example was used as a natural preservative to prevent the growth of putrefactive bacteria. The hwangchil tree extract is mixed with 5,000 to 10,000 parts by weight of purified water based on 100 parts by weight of hwangchil tree powder and heated at 85 to 120°C for 18 to 22 hours to prepare a first hwangchil tree extract; Mixing 150 to 200 parts by weight of ethyl alcohol with respect to 100 parts by weight of the first Hwangchil tree extract, followed by stirring for 24 to 36 hours, followed by filtration to prepare a second Hwangchil tree extract; It is prepared by mixing 30 to 50 parts by weight of purified water with respect to 100 parts by weight of the second Hwangchil tree extract, heating at 50 to 65°C for 10 to 12 hours, and then filtering.

4. Politics

The second fermentation broth is allowed to stand at 2 to 5°C for 12 to 24 hours.

5. Preparation of final cosmetic composition

Finally, the cosmetic composition is prepared by mixing 30 to 250 parts by weight of ethyl alcohol and 1 to 3 parts by weight of vitamin C based on 100 parts by weight of the secondary fermentation broth, which is then heated at 35 to 40°C for 10 to 12 hours and then filtered. .

end. Making cosmetics (cream formulation)

This cosmetic composition is described as being limited to manufacturing a general cosmetic product of a cream formulation as shown in Table 1 below, but is not limited thereto and can be modified into a spray formulation, a liquid formulation, etc., as well as soap, shampoo, rinse, It should be noted in advance that it can be widely applied to detergents, etc.

Here, the components of numbers 1 to 9 are the composition of a general cosmetic of a cream formulation as described above, and the unit is weight%, and the unit of the cosmetic composition containing the abalone meat and abalone intestine extract is 100 parts by weight of the cosmetic of Comparative Example 1. Is about parts by weight.

I. Antioxidant effect experiment

For the antioxidant effect, a TBA assay kit was used, and the absorbance of the butanol layer after centrifugation was measured at 535 nm and the average value of the antioxidant effect (%) was calculated 10 times. It was confirmed that there is an antioxidant effect of more than %. In addition, as for the antioxidant effect of the examples, it was found that the higher the content of the cosmetic composition containing abalone meat and abalone intestine extract, the higher the antioxidant effect.

All. Whitening effect experiment

The subjects were selected from 10 women in their 20s to 50s without chronic diseases.

As a result of measuring the skin brightness of the test subject before and after 4 weeks of use of cosmetics using a spectrophotometer, Comparative Example 1 did not improve skin brightness, but in Examples, ΔL (Lightness Value) was improved from 0.95 to 2.75, resulting in a whitening effect. Has been verified.

The present invention as described above has been described limited to one embodiment, but the embodiments are not limited thereto and modified based on the technical idea of the present invention, it is clear that all of the embodiments belong to the scope of the present invention.

Claims (5)

(a) preparing abalone meat and abalone intestines;
(b) With respect to 100 parts by weight of the abalone meat, 0.1 to 30 parts by weight of abalone intestines, 0.1 to 5 parts by weight of fermented green plum, and 30 to 150 parts by weight of sugar are mixed, fermented at 30 to 37°C for 1 to 6 months, and then filtered Preparing a primary fermentation broth;
(c) mixing and stirring 10 to 150 parts by weight of purified water and 3 to 5 parts by weight of Hwangchil tree extract based on 100 parts by weight of the first fermentation broth to prepare a secondary fermentation broth;
(d) allowing the secondary fermentation broth to stand at 2 to 5° C. for 12 to 24 hours;
(e) mixing 30 to 250 parts by weight of ethyl alcohol and 1 to 3 parts by weight of vitamin C based on 100 parts by weight of the secondary fermentation broth, followed by heating at 35 to 40°C for 10 to 12 hours, followed by filtering. Method for producing a cosmetic composition containing abalone meat and abalone intestine extract.
The method of claim 1,
The abalone of the step (a) is 5 to 30 parts by weight of healthy abalone, with respect to 100 parts by weight of live abalone, and the abalone intestine is a cosmetic containing abalone and abalone intestine extract, characterized in that the gallbladder part is removed. Method of making the composition.
The method of claim 1,
The green plum fermentation broth,
(A) For 100 parts by weight of chopped green plum, 50 to 250 parts by weight of purified water, 1 to 30 parts by weight of oligosaccharide or sugar, and 0.01 to 3 parts by weight of kimchi lactic acid bacteria were mixed, and then fermented at 35 to 39°C for 14 to 21 days. Preparing a fermented green plum tea;
(B) mixing and stirring 3 to 5 parts by weight of grapefruit seed powder, 200 to 500 parts by weight of purified water, and 0.1 to 0.3 parts by weight of sea salt with respect to 100 parts by weight of the first fermentation broth;
(C) Containing abalone meat and abalone intestine extract, characterized in that it is prepared by adding 500 to 1,000 parts by weight of purified water to 100 parts by weight of the second green plum fermentation broth, heating at 80 to 95°C for 100 to 120 minutes, and filtering Method for producing a cosmetic composition.
The method of claim 1,
The hwangchil tree extract,
(A) mixing 5,000 to 10,000 parts by weight of purified water based on 100 parts by weight of Hwangchil wood powder and heating at 85 to 120°C for 18 to 22 hours to prepare a first Hwangchil wood extract;
(B) mixing 150 to 200 parts by weight of ethyl alcohol with respect to 100 parts by weight of the first Hwangchil tree extract, followed by stirring for 24 to 36 hours, followed by filtering to prepare a second Hwangchil tree extract;
(C) Abalone meat and abalone intestines, characterized in that it is prepared by mixing 30 to 50 parts by weight of purified water for 100 parts by weight of the second Hwangchil tree extract, heating at 50 to 65°C for 10 to 12 hours, and then filtering Method for producing a cosmetic composition containing the extract.
A cosmetic composition prepared by any one of the methods of claims 1 to 4.