KR102115384B1 - 테트라부틸암모늄 비스(플루오로술포닐)이미드 및 관련 염의 합성 - Google Patents

테트라부틸암모늄 비스(플루오로술포닐)이미드 및 관련 염의 합성 Download PDF

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KR102115384B1
KR102115384B1 KR1020157012939A KR20157012939A KR102115384B1 KR 102115384 B1 KR102115384 B1 KR 102115384B1 KR 1020157012939 A KR1020157012939 A KR 1020157012939A KR 20157012939 A KR20157012939 A KR 20157012939A KR 102115384 B1 KR102115384 B1 KR 102115384B1
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solvent
reactor
salt
fluoride
base
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KR20150082321A (ko
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마틴 알. 존슨
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트리나프코 인크.
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    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C311/00—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups
    • C07C311/48—Amides of sulfonic acids, i.e. compounds having singly-bound oxygen atoms of sulfo groups replaced by nitrogen atoms, not being part of nitro or nitroso groups having nitrogen atoms of sulfonamide groups further bound to another hetero atom
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C—CHEMISTRY; METALLURGY
    • C01—INORGANIC CHEMISTRY
    • C01B—NON-METALLIC ELEMENTS; COMPOUNDS THEREOF; METALLOIDS OR COMPOUNDS THEREOF NOT COVERED BY SUBCLASS C01C
    • C01B21/00—Nitrogen; Compounds thereof
    • C01B21/082—Compounds containing nitrogen and non-metals and optionally metals
    • C01B21/086—Compounds containing nitrogen and non-metals and optionally metals containing one or more sulfur atoms
    • C—CHEMISTRY; METALLURGY
    • C07—ORGANIC CHEMISTRY
    • C07C—ACYCLIC OR CARBOCYCLIC COMPOUNDS
    • C07C209/00—Preparation of compounds containing amino groups bound to a carbon skeleton
    • C07C209/68—Preparation of compounds containing amino groups bound to a carbon skeleton from amines, by reactions not involving amino groups, e.g. reduction of unsaturated amines, aromatisation, or substitution of the carbon skeleton

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  • Chemical & Material Sciences (AREA)
  • Organic Chemistry (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Inorganic Chemistry (AREA)
  • Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
KR1020157012939A 2012-11-16 2013-11-15 테트라부틸암모늄 비스(플루오로술포닐)이미드 및 관련 염의 합성 Expired - Fee Related KR102115384B1 (ko)

Applications Claiming Priority (3)

Application Number Priority Date Filing Date Title
US201261727616P 2012-11-16 2012-11-16
US61/727,616 2012-11-16
PCT/US2013/070410 WO2014078725A1 (en) 2012-11-16 2013-11-15 Synthesis of tetrabutylammonium bis(fluorosulfonyl)imide and related salts

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KR20150082321A KR20150082321A (ko) 2015-07-15
KR102115384B1 true KR102115384B1 (ko) 2020-05-26

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US (2) US9181173B2 (OSRAM)
EP (1) EP2920147B1 (OSRAM)
JP (1) JP6276778B2 (OSRAM)
KR (1) KR102115384B1 (OSRAM)
CN (1) CN104918913B (OSRAM)
WO (1) WO2014078725A1 (OSRAM)

Families Citing this family (22)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
JP6276778B2 (ja) * 2012-11-16 2018-02-07 トリナプコ インコーポレイテッド ビス（フルオロスルホニル）イミドアニオンの塩を生成する方法
US10214419B2 (en) * 2013-11-18 2019-02-26 Nippon Soda Co., Ltd. Granules or powder of disulfonylamide salt and method for producing same
ES2956953T3 (es) * 2014-06-06 2024-01-05 Scripps Research Inst Compuestos de fluoruro de azufre (VI) y su uso en reacción click
CN104477861B (zh) * 2014-11-24 2017-02-22 中国船舶重工集团公司第七一八研究所 一种双氟磺酰亚胺盐的制备方法
US10020538B2 (en) 2015-11-13 2018-07-10 Uchicago Argonne, Llc Salts for multivalent ion batteries
JP2019089663A (ja) * 2016-03-31 2019-06-13 セントラル硝子株式会社 ビス（ハロゲン化スルホニル）イミド酸金属塩の製造方法
US11094208B2 (en) 2016-09-30 2021-08-17 The Boeing Company Stereo camera system for collision avoidance during aircraft surface operations
MX2019005823A (es) * 2016-11-19 2019-07-10 Trinapco Inc Metodo de elaboracion de n-(fluorosulfonil) dimetilamina.
CN107986248B (zh) * 2017-11-17 2021-11-26 南京红太阳生物化学有限责任公司 一种双氟磺酰亚胺的制备方法
CN110217764B (zh) * 2018-03-02 2022-08-09 中国科学院上海有机化学研究所 一种双氟磺酰亚胺的有机碱盐的制备方法
KR102729560B1 (ko) * 2019-04-08 2024-11-14 가부시기가이샤 닛뽕쇼꾸바이 알칼리 금속 비스(플루오로술포닐)이미드 수용액, 수용액이 든 용기, 및 당해 수용액의 보관 또는 수송 방법
US11267707B2 (en) 2019-04-16 2022-03-08 Honeywell International Inc Purification of bis(fluorosulfonyl) imide
US11591218B2 (en) 2019-12-17 2023-02-28 Honeywell International Inc. Integrated processes for producing bis(fluorosulfonyl) imide
CN110935286B (zh) * 2020-01-16 2022-03-01 浙江工业大学 一种利用离子液体复合生物基溶剂吸收残留熏蒸剂硫酰氟的方法
US11772967B2 (en) 2021-01-07 2023-10-03 Honeywell International Inc. Integrated processes for treatment of an ammonium fluorosulfate byproduct of the production of bis (fluorosulfonyl) imide
US12421114B2 (en) 2021-01-29 2025-09-23 Honeywell International Inc. Sulfamyl fluoride compositions and processes for making sulfamyl fluoride compositions
CA3267325A1 (en) 2022-09-22 2024-03-28 Specialty Operations France PROCESS FOR MANUFACTURING BIS(HALOGENO SULFONYL)IMIDE
CN115535974B (zh) * 2022-11-03 2023-09-26 昆山美淼新材料科技有限公司 一种高选择性合成双氟磺酰亚胺的方法及用途
CN116281895B (zh) * 2023-02-06 2025-06-20 杭州弗思创新材料有限公司 一种高选择性合成双氟磺酰亚胺三乙胺盐的方法
CN116283601A (zh) * 2023-03-16 2023-06-23 浙江中欣氟材股份有限公司 一种双氟磺酰亚胺有机铵盐的制备方法
CN116119766B (zh) * 2023-04-07 2024-07-09 福州大学 一种高效处理LiFSI生产废水的方法
CN116789090B (zh) * 2023-04-27 2025-10-31 福州大学 一种捕捉反应中间体fso2nh2的方法

Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012129322A1 (en) * 2011-03-21 2012-09-27 Trinapco, Inc. Improved synthesis of tetrabutylammonium bis(fluorosulfonyl)imide and related salts

Family Cites Families (31)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
US2130038A (en) 1938-09-13 Sulphamic acid fluorides
DE1143495B (de) 1961-12-09 1963-02-14 Dr Rolf Appel Verfahren zur Herstellung von Imidobisschwefelsaeurefluorid
DE1199244B (de) 1963-10-29 1965-08-26 Olin Mathieson Verfahren zur Herstellung von Imidobisschwefelsaeurefluorid
US3411889A (en) 1966-03-07 1968-11-19 Allied Chem Sulfamide
US3418088A (en) 1966-03-21 1968-12-24 Du Pont Sulfuryl halides and process
US5256821A (en) 1988-10-05 1993-10-26 Societe Nationale Elf Aquitaine Method of synthesis of sulphonylimides
FR2645533B1 (fr) 1989-04-06 1991-07-12 Centre Nat Rech Scient Procede de synthese de sulfonylimidures
JP3878206B2 (ja) 1994-03-21 2007-02-07 サントル・ナショナル・ドゥ・ラ・ルシェルシュ・シャンティフィク 良好な耐食性を示すイオン性伝導材料
JP3117369B2 (ja) 1994-09-12 2000-12-11 セントラル硝子株式会社 スルホンイミドの製造方法
US5874616A (en) 1995-03-06 1999-02-23 Minnesota Mining And Manufacturing Company Preparation of bis (fluoroalkylenesulfonyl) imides and (fluoroalkysulfony) (fluorosulfonyl) imides
WO1998029399A1 (fr) 1996-12-30 1998-07-09 Hydro-Quebec Sels d'anions pentacycliques ou derives de tetrazapentalene, et leurs utilisations comme materiaux a conduction ionique
DE69934170T2 (de) 1998-02-03 2007-09-27 Acep Inc., Montreal Neue als elektrolytische solubilisate geeignete werkstoffe
US6252111B1 (en) 1999-02-16 2001-06-26 Central Glass Company, Limited Method for producing sulfonimide or its salt
JP3623452B2 (ja) 2000-01-31 2005-02-23 森田化学工業株式会社 スルホニルイミド化合物の製造方法
KR20010078204A (ko) * 2000-01-31 2001-08-20 모리타 시게루 설포닐이미드 화합물의 제조방법
CA2322099A1 (en) 2000-01-31 2001-07-31 Yoshitaka Sakamoto Process for producing sulfonylimide compound
FR2818972B1 (fr) 2000-12-29 2003-03-21 Rhodia Chimie Sa Procede de fluoration d'un compose halogene
CN1306959C (zh) * 2004-09-21 2007-03-28 中国科学院武汉病毒研究所 草鱼呼肠孤病毒抗原亚单位疫苗制备方法
JP2009504790A (ja) 2005-08-22 2009-02-05 トランスファート プラス エスイーシー スルホニルイミド及びその誘導体を調製するための方法
JP5374895B2 (ja) 2008-03-21 2013-12-25 セントラル硝子株式会社 光学活性フルオロアミン類の製造方法
CN101980955B (zh) 2008-03-31 2013-07-03 株式会社日本触媒 磺酰亚胺盐及其制备方法
JP5443118B2 (ja) 2009-03-31 2014-03-19 三菱マテリアル株式会社 ビス（フルオロスルホニル）イミド塩の製造方法、ビス（フルオロスルホニル）イミド塩及びフルオロ硫酸塩の製造方法、並びにビス（フルオロスルホニル）イミド・オニウム塩の製造方法
JP5527993B2 (ja) 2009-03-31 2014-06-25 三菱マテリアル株式会社 ビス（フルオロスルホニル）イミドの製造方法
JP5630048B2 (ja) 2009-03-31 2014-11-26 セントラル硝子株式会社 イミド酸化合物の製造方法
JP5471045B2 (ja) 2009-06-03 2014-04-16 セントラル硝子株式会社 イミド酸塩の製造方法
JP5730513B2 (ja) 2009-08-13 2015-06-10 三菱マテリアル株式会社 含フッ素スルホニルイミド化合物の製造方法
JP5401336B2 (ja) 2010-01-15 2014-01-29 株式会社日本触媒 フルオロスルホニルイミド塩の製造方法
EP3705453B1 (en) 2010-05-28 2021-06-23 Nippon Shokubai Co., Ltd. Alkali metal salt of fluorosulfonyl imide
CN103391896A (zh) * 2011-03-03 2013-11-13 日本曹达株式会社 氟磺酰亚胺铵盐的制造方法
US8377406B1 (en) 2012-08-29 2013-02-19 Boulder Ionics Corporation Synthesis of bis(fluorosulfonyl)imide
JP6276778B2 (ja) * 2012-11-16 2018-02-07 トリナプコ インコーポレイテッド ビス（フルオロスルホニル）イミドアニオンの塩を生成する方法

Patent Citations (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
WO2012129322A1 (en) * 2011-03-21 2012-09-27 Trinapco, Inc. Improved synthesis of tetrabutylammonium bis(fluorosulfonyl)imide and related salts

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JP6276778B2 (ja) 2018-02-07
EP2920147A4 (en) 2016-06-22
US9181173B2 (en) 2015-11-10
WO2014078725A1 (en) 2014-05-22
CN104918913A (zh) 2015-09-16
US9475764B2 (en) 2016-10-25
US20160031806A1 (en) 2016-02-04
US20140142338A1 (en) 2014-05-22
HK1215019A1 (zh) 2016-08-12
EP2920147B1 (en) 2019-02-13
EP2920147A1 (en) 2015-09-23
KR20150082321A (ko) 2015-07-15
CN104918913B (zh) 2018-02-09
JP2015536296A (ja) 2015-12-21

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