KR102066261B1 - Manufacturing Method Of Cosmetic Composition Containing Chojeong Carbonated Water And Scutellaria Baicalensis Extract For Hair Damage Prevention And Improvement - Google Patents

Abstract

The present invention is to provide a cosmetic composition for improving skin moisture by using ultra-fine mineral water and golden extract to improve the moisture content of the skin, thereby improving wrinkles, skin elasticity and anti-aging of the skin, Ultra-fine mineral water 50 to 60 parts by weight, characterized in that it comprises 1 to 10 parts by weight of golden extract.

Description

Manufacturing Method Of Cosmetic Composition Containing Chojeong Carbonated Water And Scutellaria Baicalensis Extract For Hair Damage Prevention And Improvement}

The present invention relates to a cosmetic composition for improving skin moisture, and more particularly, to a cosmetic composition for improving skin moisture, including ultrafine mineral water and a golden extract.

The skin is divided into three layers of epidermis, dermis, and subcutaneous fat tissue in order from the outside, and protects the body from physical and chemical stimuli from the external environment. It controls the evaporation of ~ 70% of moisture out of the body. Among them, the epidermis is divided into the stratum corneum, granule layer, polar layer, and basal layer from the outside. The stratum corneum of the epidermis contains about 10-20% of moisture and exists at the outermost part of the human body to suppress evaporation of moisture from the body. Blocks material infiltration from the outside. The cells constituting the stratum corneum have a high concentration of natural moisturizing factor (NMF), which is a water-soluble ingredient, which helps the skin to show flexibility and maintain proper moisture.

However, due to changes in the environment or changes in life patterns, various stresses and environmental pollution caused by social life, frequent face washing due to makeup habits, and natural skin aging due to age increase, moisture in the stratum corneum decreases and the skin dries. As the skin becomes rough and the surface becomes rough and the skin loses shine and dull appearance occurs, there is a growing interest in improving skin moisture content. The improvement of skin moisture content is not only moisturizing the skin but also improving the wrinkles of the skin, It is also closely related to skin elasticity and anti-aging.

Therefore, various attempts have been made to improve skin moisture content. For example, Korean Patent Application Publication No. 10-2014-0073837 (hereinafter referred to as "Patent Document 1") is effective for "fur protein hydrolyzate." Cosmetic moisturizing composition for improving skin moisturizing and elasticity comprising as a component ", and Korean Patent No. 10-1351185 (hereinafter referred to as" Patent Document 2 ") contains" lactic acid extract of the red crab shell as an active ingredient The skin moisturizing cosmetic composition "is disclosed.

The patent document 1 shows a moisturizing effect through the antioxidant activity of the pollack oil protein hydrolyzate, the patent document 2 is excellent in water retention and moisture adsorption power to keep the lactic acid extract of the red crab shell retaining water, It has an excellent effect of oil and fat stability, indicating a skin moisturizing function.

These conventional techniques are mainly for improving the moisture content of the skin using only functional ingredients, and the effector is often temporary or insignificant.

On the other hand, when you soak in a carbonated hot spring (炭 酸 溫泉), the skin feels supple and refreshing from the body. This is because carbonated bubbles generated in carbonated water move finely on the skin to easily discharge the waste accumulated in the pores, In addition, as carbon dioxide is absorbed into the body, capillaries expand and blood volume increases, which speeds up oxygen delivery.

Such carbonated water is slightly acidic by the carbonic acid gas contained therein, and as the carbonic acid gas is absorbed into the body over the skin barrier layer, the capillaries expand to facilitate oxygen supply and to easily discharge the waste accumulated in the pores of the skin. There is a characteristic.

In other words, the present inventors expect to be able to more effectively improve the water content of the skin when using a functional natural extract having a moisturizing effect after removing the skin waste by the carbonic acid contained in the natural carbonated water using natural carbonated water. It came to invention.

Korean Patent Publication No. 10-2014-0073837 Korean Patent Registration No. 10-1351185

The present invention, in view of the above-described conventional problems, by using ultra-fine mineral water and golden extract, to improve the moisture content of the skin, thereby improving skin moisture, such as skin wrinkles, skin elasticity and anti-aging It is to provide a cosmetic composition for improvement.

The skin composition for improving skin moisture comprising the ultra mineral water and the golden extract of the present invention is characterized in that it comprises 50 to 60 parts by weight of the ultra mineral water and 1 to 10 parts by weight of the golden extract.

In addition, the cosmetic composition for improving skin moisture containing ultra-fine mineral water and golden extract of the present invention further comprises natural oils, the natural oils, soybean oil 0.1 to 3 parts by weight, sunflower seed oil 1 to 10 parts by weight and mountain plant It is characterized by including the seed oil 0.01 to 3 parts by weight.

In addition, the cosmetic composition for improving skin moisture comprising ultra-fine mineral water and golden extract of the present invention, further comprising a natural extract, the natural extract is 0.01 ~ 3 parts by weight of Centella asiatica extract, 0.1 ~ 5 parts by weight, sea grapes 0.1 to 5 parts by weight of the extract and 0.01 to 3 parts by weight of golden cocoon extract.

In addition, the cosmetic composition for improving skin moisture containing ultra-fine mineral water and golden extract of the present invention, characterized in that it further comprises 0.1-3 parts by weight of dimethicone, 0.1-3 parts by weight of collagen and 0.1-3 parts by weight of tocopheryl acetate. do.

In addition, in the cosmetic composition for improving skin moisture comprising the ultra mineral water and golden extract of the present invention, the golden cocoon extract is sericin, the collagen is characterized in that the fish collagen.

According to the present invention, after removing the wastes of the skin by the carbonic acid contained in the ultra mineral mineral water, it is possible to improve the moisture content of the skin in the functional natural extracts having a moisturizing effect, further improve the wrinkles of the skin, skin elasticity and anti-aging, etc. You can expect the effect of.

Cosmetic composition for skin moisture improvement (hereinafter referred to as "cosmetics composition") containing ultra-fine mineral water and golden extract according to the present invention includes ultra-fine mineral water and golden extract as an active ingredient, the ultra-fine mineral water in the cosmetic composition About 50 ~ 60 parts by weight. The golden extract is preferably included 1 to 10 parts by weight based on the cosmetic composition.

In addition, the cosmetic composition further comprises a natural extract consisting of Centella asiatica extract, Root Extract, Sea Grape Extract and Golden Cocoon Extract, The Centella asiatica extract comprises 0.01 to 3 parts by weight relative to the cosmetic composition, the root extract Contains 0.1 to 5 parts by weight based on the cosmetic composition, the sea grape extract comprises 0.1 to 5 parts by weight based on the cosmetic composition, and the golden cocoon extract comprises 0.01 to 3 parts by weight based on the cosmetic composition. It is preferable.

In addition, the cosmetic composition further comprises natural oils composed of soybean oil, sunflower seed oil, and seed oil. The soybean oil contains 0.1 to 3 parts by weight based on the cosmetic composition, the sunflower seed oil comprises 1 to 10 parts by weight based on the cosmetic composition, the seed oil seed oil is 0.01 to 3 parts by weight based on the cosmetic composition It is preferable to include.

The cosmetic composition may further include dimethicone and collagen tocopheryl acetate as additives. The dimethicone is 0.1 to 3 parts by weight based on the cosmetic composition, the collagen is 0.1 to 3 parts by weight based on the cosmetic composition, the tocopheryl acetate is 0.1 to 3 parts by weight based on the cosmetic composition desirable.

[Ultra mineral water]

First, in the present invention, chojeong mineral water refers to the carbonated water of the cold mineral spring leaching in Chojeong-ri, Naesu-eup, Cheongwon-gun, Chungcheongbuk-do, Korea, the chojeong mineral water was confirmed by the National Institute of Geological Minerals in 1969, the United States Food and Drug Administration (1980) Carbonated water officially approved by the FDA.

The ultra mineral water contains up to 1200 ppm of free carbon dioxide in the dissolved state, and germanium is 8 to 22 ppm, which is 1000 times higher than commercially available bottled water, and is rich in 20 kinds of minerals, preventing various diseases. It is known for its excellent efficacy in treating and treating, especially its excellent mineral balance.

On the other hand, when you soak in a carbonated hot spring (피부 泉), the skin feels supple and refreshing from the inside of the body, which makes the carbonated bubbles generated in the carbonated water move finely on the skin to easily discharge the waste accumulated in the pores, In addition, as carbon dioxide is absorbed into the body, capillaries expand and blood volume increases, which speeds up oxygen delivery.

Such carbonated water is slightly acidic by the carbonic acid gas contained therein, and as the carbonic acid gas is absorbed into the body over the skin barrier layer, the capillaries expand to facilitate oxygen supply and to easily discharge the waste accumulated in the pores of the skin. There is a characteristic.

Therefore, the ultra-fine mineral water used in the embodiment of the present invention preferably contains 500 to 700 ppm of calcium carbonate (CaCO ₃ ) and at least 20 to 300 ppm of calcium (Ca) and 2 to 50 ppm of magnesium (Mg) as main minerals. More preferably, a small amount of germanium (Ge), manganese (Mn), selenium (Se), or the like is further included.

The calcium carbonate reacts with water to generate carbon dioxide, so that carbonic acid bubbles move finely on the skin to easily discharge the waste accumulated in the pores of the skin, while carbon dioxide is absorbed into the body and the capillaries of the skin are expanded and blood volume is increased. Increased oxygen delivery speeds up the skin, activates skin cells, contributes to maintaining skin health, and activates the skin's moisturizing factors.

In addition, the calcium promotes metabolism, activates skin cells, contributes to maintaining skin health, activates the skin's moisturizing factor, and magnesium plays a key role in cellular metabolism, and waste discharge It is known to have an effect of promoting stimulation and activating moisturizing factors.

In addition, the selenium helps to improve immunity, contributes to skin cell activation, antioxidant activity, and skin disease improvement, and germanium releases harmful substances into the body and promotes metabolic activity, thereby greatly affecting genes and life phenomena. It is known that releasing oxygen contained in organic germanium supplies a large amount of oxygen into blood vessels, thereby expanding capillaries, improving blood flow to the scalp, and reactivating cells to activate intracellular reactions.

Therefore, in the present invention, the ultra-mineral mineral water is selected by ultra-mineral mineral water containing an appropriate amount of calcium carbonate and minerals according to AOAC (Association of Official Agricultural Chemists) analysis method, which is a mineral component analysis method after harvesting, Is filtered to filter (millipore filter, 0.45um) to remove foreign matter is prepared as purified ultra mineral water.

[Golden Extract]

(1) the characteristics of gold

Gold is a root of perennial herbaceous golden herb (Scutellaria baicalensis), which contains baicalein, baicalin, wogonin, wogonoside, benzoic acid, β-sitosterol, etc. It is known to have the effect of sedation, anti-inflammatory effect, and golden extract is used in skin moisturizers for the purpose of skin moisturizing effect.

(2) Preparation of Golden Extract

 Clean and trim the dried gold and chop it up finely, and add 5 times (volume ratio) of gold to the round flask attached to the reflux cooling tube vertically and mix. Extract the reflux 3 times at 80 ℃ with heating mantle. The extracted extract was concentrated under reduced pressure in a constant temperature water bath (Oilbath, Buchi B-485, Switzerland) at 80 ° C. using a reduced pressure concentrator (Rotavapor, Buchi RE-111, Switzerland) and lyophilized.

[Centella extract]

(1) Characteristics of Centella

 Centella Asjatica is a perennial plant belonging to the family Apiaceae, mainly distributed in Korea, Japan, China, India, South Africa, and the South Pacific. Madecasoside, Asiaticoside, Asiantic acid, It contains ingredients such as madecaic acid, and has the effect of enhancing immunity, antimicrobial and antioxidant effects, and excellent moisturizing action to relieve itching and irritation of the skin.

(2) Preparation of Centella asiatica Extract

The leaves and stems of the dried herbaceous leaf were pulverized in powder form, and extracted with repeated reflux at room temperature using 10% (volume ratio) of 60% ethanol as the solvent, followed by concentration under reduced pressure and lyophilization.

[Root Extract]

(1) the characteristics of the root

Pueraria thunbergiana is a perennial vine plant belonging to the legume family. Brown root contains 10 ~ 15% starch, 9 kinds of saponin, and flavonoids which are effective in inhibiting active oxygen.

(2) Preparation of Root Extract

After cleaning and drying the dried roots in powder form, 10 times (volume ratio) of 80% ethanol of the roots were extracted with repeated reflux at room temperature using a solvent, concentrated under reduced pressure and lyophilized.

Sea Grape Extract

(1) Characteristics of Sea Grapes

The sea grape (Caulerpa Lentillifera) is a kind of seaweed, and its shape is similar to grapes, so it is also called sea grape, also called green caviar. Sea grapes are known to be rich in minerals and have excellent sulfate and moisturizing effects.

(2) Preparation of Sea Grape Extract

Clean and dried sea grapes are chopped and pulverized into powder form.Then, they are immersed in an alcohol (extraction solvent) having 10 times the volume (volume ratio) of 1 to 4 carbon atoms (extract solvent) for 3 to 20 days to extract the active ingredient, and then concentrated under reduced pressure. And lyophilization.

[Golden cocoon extract]

(1) Characteristics of Golden Cocoon

Silk from silkworm cocoons consists of two proteins, fibroin and sericin, of which fibroin forms the fiber we call silk, and sericin is the protein that surrounds two strands of fibroin.

Normally, sericin is removed through the refining process of silk, and after this sericin is removed, silk's unique gloss and touch appear. Sericin makes up about 25% of the total silk protein, but is mostly discarded through the above refining process. In this case, when the refined wastewater containing sericin is discharged into the stream, it may cause eutrophication of the stream and cause pollution.

Therefore, many studies have been attempted to recover the discarded sericin and use it as a renewable resource. According to the amino acid composition of sericin, serine occupies about 30% and has a high hydrophilic amino acid content. The amino acid composition of sericin is similar to the natural moisturizing factor (NMF) of the human body, and it is known as an excellent material for skin moisturizing effect.In addition to the moisturizing effect, sericin is produced by sulfated effect, lipid peroxidation and inhibition of tyrosinase activity. It is known to have a whitening effect and skin cancer suppressing effect.

On the other hand, the golden cocoon is a yellow cocoon made by "Golden Silk", a breed that the Rural Development Administration hybridized Japanese breeding Jam 311 (JS169) and Chinese breeding Jam 312 (CS186). Breed for yellow silk production, it is known to contain more sericin than silkworm cocoons.

(2) extraction of sericin

The silkworm cocoon and the volume ratio of distilled water were 1: 15-25, and refine | purified at the high temperature of 80-120 degreeC for 1 to 3 hours, and after separating all the sericin attached to the golden silkworm cocoon, extracted sericin aqueous solution Hydrolysis was carried out using an alcalase enzyme, flavorzyme enzyme and protamex enzyme, and the hydrolyzed sericin aqueous solution was separated using a tubular ultrafiltration membrane having a molecular weight of 4,000. After concentration through the process, the sericin powder was obtained by thawing the concentrated sericin solution in a freezing chamber of -4 ℃ or less after a certain time.

[Natural oils]

The cosmetic composition of the present invention further comprises natural oils composed of soybean oil, sunflower seed oil, and seed oil.

Natural oils contained in the cosmetic composition, basically has the effect of protecting the skin and blocking moisture evaporation.

Further, the soybean oil is obtained by pressing or solvent extraction method in soybean (Glycine max Merrill) seed soybean, the main component is a mixed glyceride of linoleic acid, oleic acid, palmitic acid and linolenic acid. It is. In particular, it contains a lot of unsaturated fatty acids, such as linoleic acid and oleic acid, these fatty acids are essential fatty acids, known to have a sulfate effect.

In addition, sunflower seed oil contains vitamins A and E, which are antioxidants, which prevents skin aging and improves cell regeneration.

In addition, the seed seed oil (Seabucton seed oil) is an oil extracted from the fruit of the hawthorn, the fruit of the hawthorn is very high in vitamin C and E content, it has a sulfate effect to prevent skin aging and moisturize the skin And skin soothing effect.

In addition, the cosmetic composition of the present invention may further comprise dimethicone, collagen and tocopheryl acetate as a functional additive.

The dimethicone is a silicone-based compound, which protects the skin by forming a film on the skin and has excellent skin moisturizing effect by blocking moisture evaporation. Moreover, when applied to cosmetics, the dimethicone has an effect that does not apply to the skin and is not sticky to the skin. have.

In addition, the collagen (collagen) is a triple-helix structure in which three polypeptide chains are twisted, especially a protein having a high content of hydroproline, and is effective for skin aging and moisturizing. In particular, fish collagen is a collagen extracted from fish scales and shells, and may be preferably used in that its molecular weight is lower than that of meat collagen and its melting point is low.

In addition, the tocopheryl acetate, also known as vitamin E acetate (lipid E acetate) as a fat-soluble compound, serves to protect the skin from harmful oxygen, and to inhibit the oxidation of unsaturated fatty acids constituting cell membranes. Has an effect.

[Production of Cosmetic Composition]

The cosmetic composition of the present invention may be formulated in a cream form, and the following describes a process for preparing the cosmetic composition formulated in a cream form.

(1) Paid Dissolution Step

First, oil solubility is a process of evenly emulsifying different oil components.

That is, natural oils containing 0.1 to 3 parts by weight of soybean oil, 1 to 10 parts by weight of sunflower seed oil, 0.01 to 3 parts by weight of seed oil, and 0.1 to 3 parts by weight of dimethicone and 0.1 to 3 parts by weight of tocopheryl acetate. After mixing 1 to 2 parts by weight, 0.5 to 1.5 parts by weight of a viscosity modifier and 0.1 to 0.5 parts by weight of surfactant, it is heated to 80 ° C to 100 ° C and dissolved to prepare a first emulsion.

(2) Viscosity Dispersion Stage in Super Mineral Water

After heating 50 to 60 parts by weight of ultra mineral water at 80 ° C. to 100 ° C., 0.1 to 0.5 parts by weight of a thickener and 0.05 to 0.15 parts by weight of an emulsifier are gradually added to uniformly disperse the thickener in the ultra mineral water.

(3) Water melting stage

In the state of maintaining the ultrafine mineral water in which the thickener is completely dispersed at 80 ° C to 100 ° C, 1 to 10 parts by weight of golden extract and 0.1 to 3 parts by weight of collagen are dissolved in the ultrafine mineral water.

(4) Mixing step of oils and ultra mineral water

In the aqueous phase dissolving step, the first extract prepared in the oil phase dissolving step is mixed with ultra-precipitated mineral water in which the golden extract and collagen are dissolved, followed by stirring at 2,500 rpm or more to prepare a second emulsion.

(5) Natural extract input step

After cooling the second emulsion emulsified in the mixing step of oils and ultra mineral water to 40 ° C. to 50 ° C., 0.01 to 3 parts by weight of Centella asiatica extract, 0.1 to 5 parts by weight of brown root extract, sea grape extract in the cooled second emulsion A natural extract consisting of 0.1-5 parts by weight and 0.01-3 parts by weight of golden cocoon extract is added thereto, followed by stirring at 2,000 rpm or more to uniformly disperse the natural extract in a second emulsion.

(6) cooling, filtration and aging step

The second emulsion in which the natural extract is evenly dispersed is cooled to 30 ° C. or lower, and then aged and stored by filtration with 100 to 200 mesh.

Claims (5)

Natural oils containing 0.1 to 3 parts by weight of soybean oil, 1 to 10 parts by weight of sunflower seed oil and 0.01 to 3 parts by weight of tree seed oil, 0.1 to 3 parts by weight of dimethicone, and 0.1 to 3 parts by weight of tocopheryl acetate. An oil phase dissolving step of preparing a first emulsion by mixing with 2 parts by weight, 0.5 to 1.5 parts by weight of a viscosity modifier and 0.1 to 0.5 parts by weight of a surfactant, and then heating to 80 ° C to 100 ° C for dissolution.
After heating 50 to 60 parts by weight of ultra mineral water to 80 ° C. to 100 ° C., a thickener uniformly dispersing the thickener in the ultra mineral water while adding 0.1 to 0.5 parts by weight of a thickener and 0.05 to 0.15 parts by weight of an emulsifier. The dispersion phase,
In the state of maintaining the ultrafine mineral water in which the thickener is completely dispersed in the thickener dispersion step at 80 ℃ ~ 100 ℃, the aqueous solution to dissolve by mixing 1-10 parts by weight of gold extract and 0.1-3 parts by weight of collagen The dissolution step,
In the water-dissolving step, the first extract prepared in the oil-phase dissolving step is mixed with the ultra-preliminary mineral water in which the golden extract and collagen are dissolved, and then stirred at 2,500 rpm or more to emulsify to prepare a second emulsion. Steps,
After cooling the second emulsion emulsified in the mixing step of the oils and the ultra mineral water to 40 ° C. to 50 ° C., 0.01 to 3 parts by weight of Centella asiatica extract, 0.1 to 5 parts by weight, and brown grape extract in the cooled second emulsion. Natural extract comprising 0.1 ~ 5 parts by weight of extract and 0.01 ~ 3 parts by weight of golden cocoon extract was added, followed by stirring at 2,000 rpm or more to disperse the natural extract evenly into the second emulsion;
Cooling the second emulsion in which the natural extract is evenly dispersed in the natural extract input step below 30 ℃, and then filtered through 100 ~ 200 mesh aging step of ultra-fine mineral water, characterized in that it comprises a aging step Method of producing a cosmetic composition for improving skin moisture containing. delete delete delete delete