KR102103108B1 - Hair Dye Composition Comprising Green Tea Extract - Google Patents

Abstract

The present invention relates to a hair dye composition comprising a green tea extract that relieves scalp irritation and minimizes hair damage while dyeing hair. The composition includes: a first agent comprising henna leaf powder, indigofera leaf powder, green tea leaf extract, and the like; a second agent comprising a low molecular weight fish collagen peptide extract powder, vitamin C powder, beta carotene powder, and the like; a first propellant comprising 1000 ppm of squalene oil, olive oil, Ulkenia amoeboidea oil, and the like; a second propellant comprising hydrolyzed collagen, nonoxynol-12, arginine, and the like; and green tea in which green tea powder is diluted in purified water.

Description

Hair dye composition comprising green tea extract {Hair Dye Composition Comprising Green Tea Extract}

The present invention relates to a hair dye composition, and more particularly, to a hair dye composition comprising a green tea extract that relieves irritation of the scalp while dyeing the hair and minimizes hair damage and irritating odor.

In general, hair is divided into hair for hair, hair for other body parts, and beard, eyebrow, eyelash, nose hair, ear hair, armpit hair, and pubic hair depending on the area. Of these, the beard, armpit hair and pubic hair are affected by the gonads. The number of hairs on the human body is about 5 million, of which about 100,000 are hairs on the head. The hair consists of three layers: hair quality, fur quality, and cuticle. The cortex is hydrophilic, susceptible to the action of drugs, and is the most important part of hair. In the hair of hair, keratin is 80-90%, melanin pigment is 3% or less, cortex is 1-8%, and trace elements are 0.6-1.0%.

Hair is colored or dyed in a variety of colors for the purpose of beauty or personality, depending on the trend of various times. Decolorant is used to decolorize hair-specific pigments, and is used in combination with hydrogen peroxide (H2O2). There are treatments on the scalp and separation from the scalp. Chemical reactions occur in the cortex by weakening and dispersing natural and artificial pigments. Hair dye is a dye that permanently or semi-permanently changes the color of hair using natural or synthetic dyes.

Conventionally, hair dyes have a problem that causes irritation of the scalp after treatment, side effects such as hair damage or facial trouble, or irritating odors of hair dyes, resulting in discomfort of the operator.

As a prior art related to the present invention, Patent Literature 1 is a first agent comprising 0.1 to 10% by weight of coffee extract, 0.03 to 10% by weight of amla powder, 0.5 to 10% by weight of machu extract, and 26.3 to 87% by weight of other additives; Consists of a second agent comprising an oxidizing agent, the other additives include 0.3 to 12% by weight of an oxidizing dye, 1 to 22% by weight of an alkali agent, 5 to 23% by weight of a base and 20 to 30% by weight of a solvent, and the second agent Discloses a hair dye composition comprising 9 to 25% by weight of oxidizing agent, 0.1 to 2% by weight of pH adjusting agent, 5 to 20% by weight of base agent and 54 to 69% by weight of solvent relative to the total amount of the second agent.

Republic of Korea Registered Patent Publication No. 10-1809561 (announced on January 18, 2018)

The present invention is to solve the above problems, and after dyeing the hair dye on the hair, to minimize irritation of the scalp and damage to the hair and the occurrence of irritating odor, and adding nutrients to the hair, so that the treatment of thick and rich hair is made The purpose is to do.

Another object of the present invention is to suppress the formation of gray hair after dyeing the hair dye on the hair, and to allow the permanent wave to be formed naturally during the permanent wave treatment.

In order to achieve the above object, the present invention is a first agent comprising 29% by weight of henna leaf powder, 25% by weight of indigofera leaf powder, 10% by weight of green tea leaf extract, 19% by weight of iris root extract, and 17% by weight of mung bean powder. ; A second agent comprising 60 to 75% by weight of a low molecular weight fish collagen peptide extract, 5 to 10% by weight of vitamin C powder, 4% by weight of beta-carotene powder, 1 to 5% by weight of pomegranate extract, and 11% by weight of soybean extract; 1000ppm squalene oil 3% by weight, olive oil 60-70% by weight, Ulkenia amoeboiide oil 0.1-2% by weight, linseed oil 0.1-2% by weight, argan tree kernel oil 0.1-2% by weight, sunflower seed oil 0.1 to 2% by weight, grape seed oil 0.1 to 2% by weight, jojoba seed oil 0.1 to 2% by weight, tocopheryl acetate 0.2 to 2% by weight, a first spray comprising a residual amount of purified water and traces of fragrance; Hydrolyzed collagen 1.2% by weight, nonoxynol-12 1.1% by weight, arginine 1.1% by weight, phytosphingosine 0.01 to 5% by weight, hydrogenated lecithin 1.2 to 1.8% by weight, methylchloroisothiazoli 0.05% by weight of rice paddy, 0.05% by weight of methyl isothiazolinone, 1.2% by weight of PEG-75 lanolin, 2.8 to 3.6% by weight of hydrolyzed keratin, 1 to 10% by weight of panthenol, 2% by weight of ceramide enpy and the balance of purified water A second spray comprising; And green tea in which 3.4 wt% of green tea powder was diluted in 96.6 wt% of purified water; Each composition, wherein the first agent, the second agent, and green tea are mixed at a mixing ratio of 1: 1 to 1.5 to 2.0 weight ratio, and then applied to the hair, and the first and second spray agents Green tea consisting of 0.5 to 0.5 weight ratios, respectively, compared to the blending ratio of 1: 1 to 1.5 to 2.0 weight ratios of the first, second and green teas, although all or selectively sprayed on the hair. It is characterized by providing a hair dye composition comprising an extract.

In addition, in the present invention, the electrolytically decomposed acidic or alkaline deep sea water is composed of 0.3 to 0.5 weight ratio compared to the total weight ratio of the first agent, the second agent and green tea, the first spray agent and the second spray agent. Can be.

In addition, in the present invention, the deep ocean water may be applied to fill the hairy insect material in the hair.

In addition, in the present invention, the egg yolk is blended with the first agent, the egg yolk may be further blended with 50 parts by weight relative to the total weight ratio of the first agent.

According to the present invention, the hair damage and scalp irritation in the dyeing process are reduced, and the green tea extract relieves the scalp irritation, while reducing the irritating odor caused by the hair dye composition by the intrinsic odor removing component of green tea, resulting in user fatigue. It has the advantage of lowering, adding nutrients to the hair so that thick and rich hair can grow, suppressing the formation of gray hair or gray hair, and allowing the permanent wave to be naturally formed during the procedure of the permanent wave.

1 is an embodiment according to the present invention, a block diagram showing a procedure for the hair treatment using a hair dye composition containing green tea extract.
2 to 4 is a photograph showing an example of the procedure to the hair of the subject to be treated with a certain number of times over a period of time using the hair dye composition containing the green tea extract according to the present invention.
Figure 5 is a photograph comparing the hair before and after the procedure after the treatment on the subject's hair at a certain number of times over a period of time using the hair dye composition containing the green tea extract according to the present invention.

Hereinafter, embodiments of the hair dye composition comprising the green tea extract according to the present invention will be described in detail.

First, in the hair dye composition of the present invention, the first agent containing the green tea extract and the second agent containing the low-molecular fish collagen peptide are mixed with a certain amount of purified water in a predetermined ratio or mixed with green tea leaves. At this time, it is good to brew a certain amount of green tea powder with hot water at about 80 ℃ for 1-2 minutes. Also, it is good to brew green tea powder with cold water or steam. For green tea, it is good to dilute 3.4 wt% of green tea powder in 96.6 wt% of purified water. In addition, the mixing ratio of the first agent: the second agent: green tea is preferably blended in a ratio of 1: 1 to 1.5 to 2.0.

Moreover, for dyeing hair, a hair dye composition in which a certain amount of green tea is mixed with a first agent and a second agent is used, but the first and second spray agents containing various natural oil extracts, alkali and acid obtained by electrolysis Deep ocean water, carbonated water, etc., may be additionally used before, during, or after the use of the hair dye composition during mixing or hair dyeing. At this time, the first injection agent and the second injection agent are all or selectively sprayed on the hair, but it is preferable that the first, second and green tea are mixed at a ratio of 0.5 to 0.5, respectively.

Next, Table 1 was prepared by blending the raw materials and contents of the first spraying agent and the second spraying agent in the hair dye composition according to the present invention. And it is prepared by mixing the raw materials and contents of the first agent and the second agent of the hair dye composition according to the present invention. In addition, green tea blended with purified water is used in the first agent and the second agent before the hair dye treatment.

In Table 1, as the hair dye composition of the present invention, the first and second agents applied to the hair, the first spray agent and the second spray agent sprayed on the hair, and the deep water used in the hair dye treatment process will be described. .

(First agent)

Henna leaf powder-Henna is attracting the most attention as a raw material for vegetable natural dyes. Henna leaf powder is usually greenish brown powder, mixed with water and used as mud. Some dyes are extracted from leaves by mixing lemon juice or essential oil. Henna has long been used as a material for temporary tattoos and hair dyeing, and contains antipyretic or antibiotic ingredients, and has also been used as a medicine to treat headaches, burns, inflammations, ulcers, and heat ups. The dye is picked from the leaves of the tropical plant Lawsonia inermis and the leaf-tipped, dried and ground into powder. In the hair dyeing method using henna, the henna leaf powder is immersed in water for a certain period of time or fermented, and then evenly applied to the hair. The henna colors the hair orange, and by repeating this process several times, the hair can be colored red wine. Moreover, henna leaf is used as a treatment for dermatitis and burns due to its sterilizing effect, and the ingredient called rhonia in henna gives natural color to the cuticle layer along with the color of the hair, giving it a elastic and voluminous hair with a treatment effect. In addition, it prevents dandruff by discharging waste products of the scalp and can be dyed with confidence because there are no side effects of chemical dyeing.

In addition, it is possible to dye natural transparent or natural orange with 100% henna leaf powder, and natural brown or natural dark brown depending on the blending ratio of henna leaf powder, indigofera leaf powder, calamus root (iris) powder, and green tea leaf extract. Dyeing is possible.

Indigofera leaf powder-Indigofera (Indigofera) is a type of legume used in indigo dyes called indigofera tintoria or true indigo. Indigofera is a natural dye that can be dyed in a natural color called tintoria. Indigo can be dyed blue, ie indigo, directly at room temperature without a mordant. However, oxidized indigo dye is insoluble and cannot be used for dyeing immediately. In order to use indigo dye for dyeing, insoluble pigments must be made water-soluble. Methods for making indigo pigments water-soluble include a method of adjusting a salt solution to an alkaline state (pH 10-12) and then chemically reducing it using a reducing agent and fermenting it by microorganisms. The reduction technology of indigo dye using a reducing agent such as hydrosulfite is relatively easy, and since it can be reduced in a short time, it has recently been introduced and utilized. On the other hand, the traditional fermentation method uses indigo pigment in a container such as a jar, adds water and an alkali agent to make it into an alkaline state at a pH of about 10-12, adds nutrients such as starch and carbon source, and maintains the temperature at around 30 ℃ every day. It is fermented while stirring. In addition, the indigo fermentation method is difficult without expert skills such as the indigo pigment and the amount of water, the degree of alkali, the ratio of the addition of nutrients, temperature management, and the success and duration of fermentation, etc. To manufacture. In addition, indigo dyeing has the advantage of being easy to do without mortar at room temperature and having good fastness, but also has the disadvantage of not being able to dye various colors by mordants like other plant-derived dyes.

Green Tea Leaf Extract-Green Tea is dried by steaming or heating the young leaves of a tea tree, and contains a large amount of polyphenols such as tannin and catechin, which have high physiological activity. Green tea leaf extract is obtained by extraction with a mixture of ethanol and butylene glycol. Green tea leaf extract reacts with excess free radicals and helps remove them. Green tea leaves contain antioxidants such as catechins and flavonoids. In particular, catechins or epigallocatechin gallate (EGCG, gallate-3-epigallocatechin) are a type of polyphenols and It has excellent antioxidant functions such as protecting itself. Moreover, epigallocatechin gallate has a strong anti-oxidative effect against skin inflammation or harmful oxygen, thereby preventing skin damage, toxin removal and wrinkles.

Changpo Root Extract-Changpo is a quintessential breeze that has the effect of making the skin, hair and scalp soft and shiny as the extract was used to wash the hair or take a bath. In particular, Asarone, an active ingredient of iris, is divided into alpha- (alpha-) and beta- (beta-), and is widely distributed in iris roots, rhizomes, and entire plants. Roots containing β-Asarone have been used in traditional medicine to treat diabetes. In addition, in a number of in vitro experiments, beta-asarone was found to have anticholinergic activity. The efficacy of the iris extract has been reported to be antioxidant, anti-inflammatory, whitening, scalp purification and cleaning efficacy. However, so far, Stigmasterol, Stearic Acid, Galocatechin, P-Hydroxybenzoic Acid, Procatechuic Acid and Vanillic Acid, which are the active ingredients derived from iris extract, ), The iris extract containing as an active ingredient can increase the collagen synthesis, thereby inhibiting skin aging, anti-oxidation, anti-wrinkle, anti-inflammatory, whitening and hair cell proliferation.

Mung bean powder-Mung bean skin contains a large amount of antioxidants such as vitexin and isobitexin, and it contains abundant amino acids such as cysteine, alanine, and arginine to help the body detoxify, thereby discharging various toxic substances to the body to metabolize. Helps smoothly. Moreover, mung bean extract has a high protein and calcium content, and contains many vitamins and essential amino acids such as leucine and lysine. In particular, mung beans are rich in antioxidants such as saponins, flavonoids, bitexins, and isovitexins, removing harmful free radicals in the body, preventing cell damage, and preventing skin aging, as well as rich minerals and vitamins of green beans It lowers the body's heat, smoothes metabolism, strengthens kidney function, and relieves edema.

Egg yolk-Egg yolk contains vitamin A and high quality protein, which is a basic material for biosynthesis, including bitelin, and provides nutrition to damaged and shiny and dry hair.

In addition, the first agent may be applied by fermenting henna leaf powder 25% by weight, indigofera leaf powder 23% by weight, green tea leaf extract 10% by weight, iris powder 19% by weight, mung bean powder 17% by weight. Moreover, the fermentation of the first agent is fermented using microorganisms, mold, yeast or lactic acid bacteria while stirring in a stirrer for 36-60 hours at 30-40 ° C. Moreover, the first agent is fermented by microorganisms in the genus Pseudojima of the antioxidant effect or selected from the group consisting of the genus Mucor, Rhizopus, Aspergillus and Monascus. It can be fermented using the fungus inside. In addition, the first agent is preferably fermented with yeast of the genus Candida or lactic acid bacteria of the genus Lactobacillus.

In addition, the egg yolk may be blended with 50% by weight relative to the total weight ratio of the first agent.

(Second agent)

Low molecular peptide fish collagen extract powder-Collagen is an albuminoid that shows the most important role as a constituent protein of vertebrate support tissue. It belongs to the water-insoluble protein Scleroprotein, and contains a lot of glycine among amino acids. Collagen is widely used in the food industry, medicine, and cosmetics industry because it is easily gelatinized and easily digested when heated with water, dilute acid, or alkali. In addition, when the collagen present in the fish skin is heated, it turns into gelatin. It can be extracted and purified and used for a wide variety of uses. Purification of gelatin from fish shells is possible in a shorter period of time compared to that of terrestrial animals.

Moreover, hard proteins are a group of simple proteins that are insoluble in water, saline solution, organic solvents, weak acids, alkalis, etc.Elastin in collagen, tendons, and arteries contained in bone, dermis, tendon, fascia, and cartilage. ), Wool, hair, wool, angle, nails, keratin such as hooves, fibroin of silk, sponge of sponge, gorgonin of coral, conchiolin of mussel shell, animal These include amyloid, which forms pathological conditions in various organs, and extilepidine, which makes fish scales. All of them are involved in the tissues having protective and supportive functions of animal bodies, and in general, strong and hard collagen is stable and difficult to invade proteases except collagenase or elastin to act as elastase. It is claimed that it is soluble in concentrated acids and alkalis, but at that time, changes in structure also occur. It does not appear in the plant world, but instead celluloses are known to play the same role.

In addition, the low molecular peptide fish collagen has excellent moisturizing effect due to the protective colloid peculiar to fish, and is very resistant to heat denaturation. Fish, especially fish scales, are wrapped in a layer of enamel with Hydroxyaoatite as the main component on the dermal layer of collagen. Removal of this enamel layer is necessary for the elution and degradation of collagen proteins. It can be seen that the content of hydroxyproline, an index component of the collagen peptide, is 8 to 10% by weight, similar to that of commercial collagen peptide products.

Vitamin C powder-Vitamin C (Vitamin C) protects the body from free radicals with antioxidants along with the formation of connective and supportive tissues, skin and gum health. Vitamin C acts as a powerful reducing agent in a water-soluble environment, collagen formation, synthesis of nerve substances such as dopamine, norepinephrine, tryptophan, carnitine and steroid synthesis, iron absorption, immune function, wound recovery, amino acids including folic acid, nucleotides, cholesterol, glucose It is also involved in metabolism. In addition, vitamin C plays an important role in protecting the skin from ultraviolet rays as well as its antioxidant effect. Vitamin C promotes damaged skin regeneration and suppresses the increase in melanin pigment to relieve freckles and freckles.

Beta-carotene powder-Beta-carotene (β-Carotene) is a beta-carotene that is contained in a lot of green-yellow vegetables such as carrots and spinach. It is a kind of carotenoid that is a natural pigment component. It is considered to be a safe source of vitamin A, as it reduces conversion rate when vitamin A is in the body. Therefore, it helps to maintain the health of the eyes and epithelial cells, the role of vitamin A, and helps to remove excess free radicals by smoothing the function of antioxidant enzymes. Moreover, beta-carotene promotes the growth and development of epithelial cells as well as the formation and function of skin and mucous membranes.

Pomegranate extract-Pomegranate extract is obtained from pomegranate (Punicagranatum L.), which is the fruit of the pomegranate tree, a broad-leaved tall tree with deciduous leaves of the Punicaceae family. The skin of pomegranate fruit contains a lot of tannins and alkaloids, so it is used medicinally as an antidiarrheal agent and used for dyeing. Stems, bark, leaves, etc. can also be used for dyeing, and can be dyed yellow by tan or aluminum or tin burrs with alkali burrs.

Soybean Extract-Soybean extract is derived from soybeans, and soybeans have been utilized as an important food resource for humans, and are rich in protein, essential fatty acids, phospholipids, vitamin E, and calcium. Is known. Soybeans are known to be effective in preventing various adult diseases such as preventing hypertension, thrombolysis, and lowering cholesterol in the blood, as well as anti-cancer, anti-mutagenic, and anti-aging, as well as brain activity and skin beauty. In addition, beans are useful foods that can be used as soy milk, tofu, and soy milk, including red pepper paste, miso, soy sauce and soy yogurt. Recently, interest in the components and functions of soybeans has been increasing. In particular, interest in isoflavone, a functional component contained in soybeans, is increasing day by day. The isoflavone content varies greatly depending on the soybean varieties and cultivation conditions, usually about 0.1 to 0.4%, of which about 30 to 50% is lost when making tofu or soy protein. Isoflavones are known to be effective in preventing and treating cancer, heart disease, high blood pressure, osteoporosis, menopausal disorders, kidney disease, and especially hair loss.

(First injection system)

Squalene Oil-Squalene oil is obtained from deep sea shark liver oil or olive oil. It's similar to the moisturizing ingredients found on human skin. Almost no pores. Moreover, squalene is an unsaturated hydrocarbon contained in shark liver, olives, rice bran, and the like. It is also produced in the body's fat glands, and is used in the body to synthesize cholesterol, steroid hormones, and vitamin D. Squalene, sold as a dietary supplement, is extracted and purified from shark liver oil. Squalene is an unsaturated hydrocarbon contained in shark liver, olives, rice bran, malt, and amaranth. It is a liquid oil with a low solidification point and has a chemical formula of C30H50. Most animals and plants, including humans, produce squalane little by little. In humans, it is mainly produced in the fat glands on the skin's surface, and is also present in adipose tissue such as the liver and small intestine. In the body, squalene is used for biosynthesis of cholesterol, steroid hormones, and vitamin D. Squalene is known to have antioxidant functions, anti-cancer effects, and detoxification of toxic substances in the body. Most of the animal experiments have been conducted, and research on humans is ongoing. Antioxidation is a function that helps to prevent aging and prevent cancer and cardiovascular diseases by inhibiting the oxidation reaction of free radicals in the body. Squalene is also widely used as a raw material for cosmetics because it plays a role in promoting the growth of cells and skin. It also has a detoxifying function that penetrates between cells and tissues, adsorbs with harmful substances such as environmental hormones and heavy metals, and then discharges them together. It is sold a lot as a health functional food and is also used as a cosmetic ingredient or vaccine adjuvant. In addition, squalene tightly fills the inside of the liquid crystal by adjusting the concentration of the oil phase, thereby helping to improve the stability of the liquid crystal, and at the same time, giving the skin a function of promoting a softening effect and a moisturizing effect.

Olive Oil-Olives are grown primarily for oil. Olive fruits and olive oil are important ingredients in Mediterranean cuisine. Olive oil contains oleic acid (82%), saturated fatty acids (10%), linoleic acid (8%), and vitamin E (7.6 mg / 100 g). Olive oil has five grades. As an olive oil, unrefined oil is oil first squeezed according to a prescribed method, edible oil is a mixture of refined oil and unrefined oil, commercial oil is made of acid, color, and odor-free kerosene, and kerosene oil has high acidity It is used as fuel for lamps in oil, and is obtained by squeezing the remaining debris after pressing in hot water. And the sulfide oil is obtained by extraction with a solvent and then repeated purification. Moreover, olive oil has a function as a flavoring agent and a moisture blocking agent.

Ulcania Amoeboidea Oil-Ulcania Amoeboidea Oil is extracted from seawater deep in the ocean. Ulcania amoeboiide oil has a structure similar to that of skin, so it has high affinity with the skin and is fast absorbed, so it is a skin moisturizer with nutrient delivery in the skin.

Flaxseed oil-Linseed oil is an oil extracted from flaxseed, and contains 30-40% fat oil, 3-9% mucus, 20% protein, and linamarine, a toxic glycoside. Dry fat oil obtained by pressing at room temperature is called linseed oil, and is a yellow transparent liquid containing unsaturated acids, such as linoleic acid, linolenic acid, and oleic acid. It is effective in reducing pores, reducing sebum, and improving acne skin. Moreover, linseed oil is used as an oil component for hair that has antioxidant properties for skin.

Arcan tree kernel oil-Argania spinosa kernel oil is an oil extracted from argan tree seeds, has excellent moisturizing effect and high vitamin content. Moreover, as skin softeners and skin moisture barrier agents, the contents of each of the moisturizing agent, oil and extract exhibit the optimum effect to enhance the skin moisturizing power and the skin moisturizing time.

In addition, sunflower seed oil is oily and does not clog pores. Grape seed oil is lighter than olive oil, but has strong anti-oxidation properties, so it is not easily damaged. Jojoba seed oil is an oil squeezed from the fruits of the jojoba tree, which is similar in composition to human sebum, so it is softly absorbed, has no scent, and has a little UV protection, so it is often used as a cream base or suntan oil. It has the property of almost not blocking pores. In addition, Tocopheryl Acetate is an antioxidant and skin conditioning agent.

The first spray is 1000 ppm of squalene oil 3% by weight, olive oil 60-70% by weight, Ulkenia amoeboiide oil 0.1-2% by weight, linseed oil 0.1-2% by weight, argan tree kernel oil 0.1-2% by weight %, Sunflower seed oil 0.1-2% by weight, grape seed oil 0.1-2% by weight, jojoba seed oil 0.1-2% by weight, tocopheryl acetate 0.2-2% by weight, residual amount of purified water and trace fragrance.

(2nd injection system)

Hydrolyzed Collagen-Hydrolysed Collagen is a collagen component extracted by hydrolyzing proteins extracted from animal bones and skin. Hydrolyzed collagen is a form of collagen that is easily absorbed by the skin. Hydrolyzed collagen is used as a hair and nail and skin conditioning agent, making skin tissue elastic and strong and effective in preventing wrinkles and preventing aging.

Nonoxynol-12-Nonoxynol-12 is a surfactant and emulsifier. Moreover, as one of the solubilizers, a small amount of oil component is transparently dissolved in water. Nonoxynol-12 is used as a soft surfactant because it has a chemical surfactant, a preservative, and a bactericidal effect.

Arginine-Arginine is a naturally occurring amino acid and is a major component of protein. There are many types of amino acids, and arginine is a component that can be synthesized in the body. Arginine has excellent anti-oxidation effect, helps maintain nutrients and softens the skin, and participates in collagen activity in the skin to help improve the skin.

Phytosphingosine-Phytosphingosine is a type of sphingoid that makes up ceramide. It is the element of all steps to make ceramide, and the combination of phytosphingosine and fatty acid is ceramide. Therefore, phytosphingosine before binding with fatty acids is inevitably more highly absorbable. It is an essential element for maintaining moisture in the skin. Efficacy of phytosphingosine includes cell aging inhibition, moisturizing, skin elasticity improvement, stratum corneum restoration effect, promotion of ceramide synthesis, anti-inflammatory, anti-bacterial, skin flora balance and antioxidant.

In addition, phytosphingosine has many benefits as a material for cosmetics, but the most popular effect is its ability to retain moisture. Moreover, phytosphingosine is a lipid that has a structural skeleton of Sphingosine, which is abundantly present in the skin of animals, including fungi, plants, and humans. In particular, it acts as a precursor of ceramide, a component of the lipid bilayer that constitutes the stratum corneum of the skin's epidermal layer, preventing moisture loss from the skin, moisturizing the skin, and easily absorbing harmful substances into the dermal layer of the skin It serves to prevent being. In addition, it is absorbed into the body and promotes the synthesis of ceramide, and has antimicrobial activity against several microorganisms including Propionibacterium acnes and Staphylococcus aureus.

Hydrogenated Lecithin-Hydrogenated Lecithin functions to form a stable liquid crystal emulsion formulation by forming a solid double layer liquid crystal, and may include 1 to 8% by weight based on the total weight of the cosmetic composition. When the hydrogenated lecithin is less than 1% by weight based on the total weight of the composition, the liquid crystal is not well formed due to insufficient emulsifying power to form a liquid crystal, and when it exceeds 8% by weight, a high surface tension and change over time Due to stability problems, the liquid crystal is not well formed.

Methylchloroisothiazolinone-Methylchloroisothiazolinone is a component used as a sterilizing preservative, and is used in combination with methylisothiazolinone (MIT, methylisothiazolinone). Methylchloroisothiazolinone is a compound that acts as an antibacterial agent to inhibit the growth of bacteria, yeast, and fungi. Rather than being used alone, methylchloroisothiazolinone and methylisothiazolinone are generally used as a mixture of methylchloroisothiazolinone and methylisothiazolinone (Methylchloroisothiazolinone and Methylisothiazolinone Mixed Solution). It has an inhibitory effect.

PEG-75 Lanolin-PEG-75 Lanolin contains protein line and collagen, and is used as a moisturizer and solvent.

Hydrolyzed Keratin-Hydrolyzed Keratin is an aqueous solution of keratin protein hydrolyzate and contains 2.8 to 3.6% nitrogen (N: 14.01) when quantified. Hydrolyzed keratin acts as a hair protection agent containing 5.0 to 10.0% by weight of the hydrolyzed component.

Panthenol-Panthenol (dipanthenol, dexpanthenol; D-, Dex) is a derivative of vitamin B5 (pantothenic acid). That is, when panthenol is absorbed by the skin, it is converted to vitamin B5. Panthenol can be more stably formulated in products than vitamin B5, and has excellent skin penetration properties. In addition, Panthenol helps to improve the skin barrier and the excellent skin moisturizing effect by preventing the formation of wet film and loss of moisture. Panthenol is a permeable, non-irritating moisturizer that improves the skin's moisturizing and stimulating functions and stimulates skin regeneration, making the skin soft and elastic, improving the skin's moisturizing, and preventing inflammation and itching.

Ceramide NP-Ceramide NP (Ceramide 3, Ceramide NP) is a synthetic N-acylated sphingolipid that is a synthetic N-acylated sphingolipid bound to phytosphingosine having a D-erythro structure and contains keratin. It is the most important substance among fats and oils and has an excellent function for moisturizing skin. Ceramide NP gives hair a shine, gloss, and elasticity and helps protect damaged hair or prevent the progression of damage. In addition, it plays a key role in strengthening the lipid barrier of the skin and forming a skin protective film against the external environment. In addition, it suppresses and stores moisture evaporation, thereby increasing the skin's soft and moist feeling. In addition, ceramide NP is a major component of skin lipids, which restores the damaged skin barrier, prevents transdermal moisture loss, provides a high moisturizing effect, and relieves atopic symptoms that are deepened due to skin barrier damage. Plays a role. In addition, ceramide and NP may include 0.1 to 2% by weight based on the total weight of the composition. When ceramide and NP are less than 0.1% by weight based on the total weight of the composition, the degree of stability of the liquid crystal type according to change over time decreases, and when it exceeds 2% by weight, crystals are accelerated, which may have a problem of decreasing the stability of the formulation.

(Deep sea water)

Next, Deep Ocean Water is the water of the sea that has a depth of 200m or more that almost no sunlight. Decomposition of organic matter is easier than production of organic matter by photosynthesis, and nutrients such as phosphorus and nitrogen are abundant, while pathogens and harmful substances coming from the ground are less. It has the characteristics of cleanliness, low moisture and water stability, and is used for various products such as inorganic ionized water, beer, soy sauce, and cosmetics.

Deep ocean water is used to fill the hair matrix. Moreover, the cortical cells of the hair are about 100 μm long, 1-6 μm in diameter and 1.2-1.6 μm thick, and a small amount of melanin pigment granules and about 0.2-0.8 μm in diameter exist in this area, and the nuclei of the cells In the center, there is a nuclear residue and is composed of macrofibers and insecticides. Moreover, the cortex is the most important part of the hair, and it has a fiber shape between the medulla and the cuticle, and occupies the highest proportion. It occupies about 85 to 90% of the total volume and is fusiform. Cells are arranged vertically and contain melanin. It is the part related to strength, elasticity, texture, texture, and color of hair. The pigment in the cortex determines the natural color of the hair and is the central part of the hair where chemical changes occur. It is a part related to permanent wave, hair coloring, etc. because it contains granular melanin pigment and is easily hydrophilic, which is easily compatible with water. It is composed of cortical cells and intercellular binding substances that are relatively regularly arranged in the length direction of the hair. In addition, a large number of fibrils are formed into fibrils formed vertically, and in wool, 90% of the net wool anhydride weight. It is also called cortex, and it is also called cortex to distinguish it from plant tissue. Fibrils are a collection of protofibrils, and individual protofibrils are composed of macromolecules of keratin proteins with 400 to 500 regular arrangements. This keratin molecule consists of about 4,000 polypeptides. Between fibrils and fibrils, there is a conjugation material called interstitial. In the cortex of wool, there are two types of tissues, the normal cortex and the lateral cortex, which have different sulfur contents and different chemical reactivity, and as the wool grows and grows with each other, the crimp appears along the long axis of the wool.

In addition, the intermediary substance (Matrix) is also referred to as a burial substance between cells as an intermediary substance of fibers. The content of sulfur is higher in cystine because it is contained in more insecticides than other parts or the whole fiber. In addition, the insect material is a layer of colloidal material under the cortical layer of spongy animals and the epidermis of tonic animals, and is also called a middle school. It is a layer of unstructured gel-like material that is not composed of cells in the middle of the cortical and upper layers of spongy animals. Pseudoblasts, osteoblasts, progenitor cells, etc. are scattered in them, and these are from the cortical or upper layers. It is a layer of gel-like material between the epidermis and the tonic of the tonic animal. It is thin in the polyp type and becomes a support film. In the jellyfish type, it forms a very thick layer and forms the so-called jelly of the jellyfish body.

In addition, deep ocean water is used to adjust the isoelectric point while dyeing hair with hair dye. Moreover, citric acid may be used in place of deep ocean water. Citric acid is one of polybasic carboxylic acids having a hydroxy group (-OH). Citric acid is obtained by citric acid fermentation using black mold. Citrate is usually obtained by fermenting at about 30 ° C for 7 to 10 days in acidic (pH 2-3).

The deep ocean water includes electrolytic deep ocean water and alkaline deep ocean water, respectively. The deep ocean water is preferably blended in a weight ratio of 0.3 to 0.5 compared to the total mixing ratio of the first agent and the second agent, the first spray agent and / or the second spray agent.

On the other hand, the hair dye composition comprising the green tea extract according to the present invention is applied to the hair after the first spraying agent and the second spraying agent are respectively blended immediately before dyeing, and after the first agent and the second agent are mixed with the green tea.

(The treatment method of hair dye composition)

Next, the hair dye composition respectively blended in FIG. 1 is applied to each subject's hair step by step.

<Deep Cleansing (S1)>

First, a sufficient amount of water is applied to the subject's hair and scalp and a bubble shampoo is applied. Bubble shampoo is a conventional shampoo, and is left at room temperature for about 10 minutes. Therefore, sweat, sebum and dust attached to the hair and scalp are adsorbed by the detergent contained in the bubble shampoo. Then, deep cleansing is performed in which hair and hair are rinsed thoroughly with washing water.

<1st application of deep sea water (S2)>

In addition, the electrolyzed alkaline deep ocean water is evenly applied to the hair to reduce the acidified hair. At this time, deep ocean water is used to fill the hair matrix (Matrix) and to match the isoelectric point while dyeing the hair with a hair dye.

<Spray of the first spray / second spray (S3)>

In addition, the first spraying agent and the second spraying agent are evenly sprayed on the hair to which the deep ocean water is applied. At this time, the first spray agent and the second spray agent may be selectively sprayed.

<1st heat treatment (S4)>

Heat treatment is performed at approximately 40-50 ° C for approximately 10 minutes using a heat treatment machine (S3). At this time, depending on the condition of the operator's hair, the process of spraying and heat treating the first spray agent and / or the second spray agent may be repeated approximately 2 to 5 times.

<Hair dye application (S5)>

A composition containing a certain amount of green tea is applied to the first agent containing the green tea extract and the second agent containing the low-molecular fish collagen peptide to the hair close to the scalp.

<Secondary application of deep sea water (S6)>

Electrolyzed acidic deep ocean water is applied to the hair to oxidize the acidified hair. Electrolyzed deep ocean water to apply acidic ionized water made at the anode to neutralize the alkaline hair to give the hair a shine.

<2nd heat treatment (S7)>

Then, heat treatment is performed at approximately 40-50 ° C for approximately 30 minutes using a heat treatment machine so that proteins are adsorbed on the hair.

<1st drying (S8)>

After the second heat treatment of the hair, it is naturally allowed to stand at room temperature for about 10 minutes to allow natural drying.

<Rinsing (S9)>

After naturally drying the hair, rinse and clean the hair and scalp using carbonated water. Carbonated water is obtained by dissolving carbon dioxide gas in water containing suitable salts, and includes natural mineral water or artificial mineral water. Inorganic salts are preferably sodium or potassium salts that are easily soluble in water. Among them, salt, sodium carbonate, and sodium hydrogen carbonate are the main components. However, calcium is a necessary ingredient because it holds carbon dioxide well. The aqueous solution of the added salts is dissolved in a thick solution, filtered and diluted in a combination bath before use.

<Secondary drying (S10)>

The hair rinsing with the carbonated water is dried using a hair dryer to complete the hair dye treatment.

(Examples and comparative examples of hair dye composition)

Next, the selective spraying of the first spraying agent and the second spraying agent separately mixed in the step of treatment with the hair dye composition containing the green tea extract according to the present invention, the first agent containing the green tea extract and the low molecular fish collagen The application of the hair dye containing the second agent containing the peptide with green tea will be described in contrast to a plurality of examples and comparative examples shown in Tables 2 and 3.

Experimental Example 1 in Table 2 sprayed both the first injection agent and the second injection agent in all the above-described procedures, and applied the hair dye containing green tea to the first agent and the second agent. In the procedure, only the first injection agent is sprayed, and the hair dye containing green tea is applied to the first agent and the second agent, and Experimental Example 3 sprays only the second injection agent in all of the above procedure, and the first agent and The second agent is applied with a hair dye containing green tea.

In Comparative Example 1 of Table 3, only the first spraying agent was sprayed in all the above-described procedures, and hair dyes containing purified water were applied to the first agent and the second agent, but the green tea extract was excluded from the first agent. Is spraying only the second spraying agent in all of the above-described procedures, and applying the hair dye containing purified water to the first agent and the second agent, except for the green tea extract in the first agent, and Comparative Example 3 in all the above-mentioned procedures The spraying of the propellant is omitted, and the hair dye containing purified water is applied to the first agent and the second agent, but the green tea extract is excluded from the first agent.

(Evaluation of hair dye recipients)

The hair dye treatment agent selected 10 men and 10 women who experienced repetitive dyeing and hair loss among men and women in their 25s and 60s, and experimented 1, experimental 2, experimental 3, and comparative 1 over 3 months in 1 month increments. , Comparative Example 2 and Comparative Example 3, respectively, was divided into 3 times. In addition, five panelists of hair dye treatment specialists were selected to evaluate the scalp, hair, and irritation of each subject.

<Scalp irritation evaluation>

◎: 자극 없음, △: 자극 보통, X: 자극 있음

◎: No irritation, △: Irritation normal, X: Irritation

In Table 4, both the first spray and the second spray were sprayed or selectively sprayed, and in Experimental Examples 1 to 3 in which green tea was mixed with the first and second agents, scalp irritation of the subjects was hardly observed. , Spray only the first spraying agent and apply the hair dye containing the first and second agents and purified water, but in Comparative Example 1 except for the green tea extract in the first agent, some of the subjects had slight irritation to the scalp. In Comparative Example 2 excluding only green tea extract from the first agent after spraying only the second spray agent and applying the hair dye containing the first agent and the second agent and purified water, some irritation to the scalp occurred in some of the subjects, and the first spray agent And without spraying the second spray agent, the first agent, the second agent, and the hair dye containing purified water were mixed, but in Comparative Example 3 except for the green tea extract in the first agent, some of the subjects were irritated to the scalp. Therefore, it can be confirmed that scalp irritation was hardly seen in the first to third experimental examples in which the first spray agent and / or the second spray agent was sprayed during the treatment of the hair dye or the green tea extract was mixed with the first agent. . However, in Comparative Examples 1 to 3, in which the green tea extract was omitted from the first agent and only the purified water was added to the first agent and the second agent without selectively spraying or spraying the first spray agent or the second spray agent, the patient was It was confirmed that scalp irritation occurred somewhat.

<Dyeing degree evaluation>

◎: 매우 우수, ○: 우수, △: 불만족

◎: Very good, ○: Excellent, △: Dissatisfied

In Table 5, in Experimental Examples 1 to 3, in which green tea was mixed with the first agent and the second agent in addition to spraying or selective spraying of both the first sprayer and the second sprayer, the degree of staining on the hair of each subject was It was evaluated very well. In Comparative Example 1, except for the green tea extract in the first agent, spraying only the first spray agent, applying the hair dye containing the first agent and the second agent and purified water, and the degree of dyeing on the hair of the subject was excellently evaluated. In Comparative Example 2, except for the green tea extract in the first agent, spraying only the second spray agent, applying the hair dye containing the first agent and the second agent and purified water, and the degree of dyeing on the hair of the subject was evaluated as excellent. In Comparative Example 3, except the green tea extract was applied to the hair dye of the first agent and the second agent and the purified water without spraying the propellant and the second spray agent, the degree of dyeing to the hair of the subject was somewhat inferior. Was evaluated. Therefore, in the first to third experiments in which the first injection agent and / or the second injection agent was sprayed during the treatment of the hair dye or the green tea extract was mixed with the first agent, the staining degree of the subjects was very excellent. . However, in Comparative Examples 1 to 3, in which the green tea extract was omitted from the first agent and only the purified water was added to the first agent and the second agent without selectively spraying or spraying the first spray agent or the second spray agent, the patient was It was confirmed that the degree of dyeing was somewhat unsatisfactory.

<Hair damage evaluation>

◎: 손상감 없이 아주 우수함, ○: 손상감 없이 우수함, △: 손상감 다소 있음

◎: Excellent without damage, ○: Excellent without damage, △: Some damage

In Table 6, Experimental Example 1 in which both the first injection agent and the second injection agent were sprayed, Experimental Example 2 in which only the first injection agent was sprayed, and Experimental Example 1 in which green tea was added to the first agent and the second agent and experiment In Example 2, it was evaluated as very excellent with almost no damage in the subject's hair, but in Experimental Example 3 in which green tea was mixed with the first agent and the second agent in addition to the spraying of the second spray agent, the damage was slightly felt in the subject's hair. It was rated as no excellence. And in Comparative Example 1 except for the green tea extract in the first agent, spraying only the first spray agent, applying the hair dye containing the first agent and the second agent and purified water, and evaluating the hair to the subject's hair, it was evaluated to be moderately intact. In Comparative Example 2 excluding only green tea extract from the first agent, spraying only the second spray agent, applying the hair dye containing the first agent and the second agent and purified water, it was evaluated as moderate with little damage to the subject's hair. In Comparative Example 3 excluding the green tea extract from the first agent, the first agent and the second agent were mixed with purified water without spraying the first and second spray agents, and the hair of the subject was evaluated to be moderately intact. Became. Therefore, in the first to third experiments in which the first injection agent and / or the second injection agent was sprayed during the treatment of the hair dye or the green tea extract was mixed with the first agent, the hair damage degree of the subjects was very excellent or excellent. It was confirmed that it appeared. However, in Comparative Examples 1 to 3, in which the green tea extract was omitted from the first agent and only the purified water was added to the first agent and the second agent without selectively spraying or spraying the first spray agent or the second spray agent, the patient was It was confirmed that the feeling of hair damage occurred somewhat.

<Stimulus evaluation>

◎: 자극 없음, △: 보통, X: 자극 있음

◎: No irritation, △: Normal, X: Irritation

In Table 7, Experimental Example 1 in which both the first and second sprayers were sprayed, Experimental Example 2 in which only the first sprayer was sprayed, Experimental Example 3 in which only the second sprayer was sprayed, and the first and second sprayers In Experimental Example 1 to Experimental Example 3 in which green tea was added to the agent, it was evaluated that almost no irritation occurred in the scalp and hair of the subject. In Comparative Example 1 excluding only the green tea extract from the first agent, spraying only the first spray agent and applying the hair dye containing the first agent and the second agent and purified water, it was evaluated that some irritation occurred in the scalp and hair of the subject. Spray only the 2 spray agent, apply the hair dye containing the first and second agents and purified water, and remove the green tea extract from the first agent. Comparative Example 2 and the first spray agent and the second spray agent without spraying the first agent and In Comparative Example 3, in which the hair dye containing the second agent and purified water was mixed and the green tea extract was excluded from the first agent, irritation was generated in the scalp and hair of the subject. Therefore, during the treatment of the hair dye, the first spray agent and / or the second spray agent was sprayed, or in the first to third experiments in which the green tea extract was blended with the first agent, irritation was hardly generated in the scalp and hair of the subjects. Could confirm. However, in Comparative Example 2 and Comparative Example 3, in which only the second spraying agent was sprayed, or the green tea extract was omitted in the first agent and only purified water was mixed in the first agent and the second agent without spraying, irritation was observed in the scalp and hair in the subject. It was confirmed that it occurred.

As described above, in the hair dye composition comprising the green tea extract of the present invention, when the first spray agent and the second spray agent are sprayed prior to the application of the hair dye and the hair spray agent in which the green tea is mixed with the first agent and the second agent, the scalp There was almost no irritation or irritation, and excellent results were also obtained in the evaluation of the degree of hair dying and damage to hair. Moreover, before applying the first spray agent and / or the second spray agent, when the acidic deep sea water is applied after the application of the alkaline deep sea water and the hair dye containing the first agent and the second agent, the hair becomes rich and hair loss It was evaluated that the thickness of the hair became thicker as well as preventing it.

This is the result of performing an iterative procedure using the hair dye composition of the present invention in the photograph of the operator of FIG. 2, and the hair becomes thicker as a result of performing the procedure up to the third procedure over a period of time after the first procedure on the first visited operator As it became rich, it was possible to see the effect of preventing hair loss. In addition, in the photograph of the operator of FIG. 3, the hair was thickened and enriched in the operator with many white hairs through repeated treatments using the hair dye composition of the present invention, thereby preventing hair loss and suppressing the occurrence of gray hair. In addition, in the photograph of the subject of FIG. 4, it was possible to see the effect of changing into elastic hair without strength, thin, cracked, and thick hair becoming thick and rich through repetitive treatment using the hair dye composition of the present invention. In addition, in FIG. 5, it was possible to see the effect of changing the thinned hair into thick and elastic hair through repeated procedures using the hair dye composition of the present invention.

Moreover, the green tea extract mixed with the first agent and the first agent and the second agent caused little irritation to the scalp of the operator, and the green tea extract contained in the first agent reduced the irritating odor and reduced user fatigue. It was evaluated to have an effect of lowering psychological stability. In addition, there was little damage to the operator's hair due to the small molecule fish collagen peptide contained in the second agent and squalene oil contained in the first injection agent.

In the above description, the present invention has been illustrated and described in connection with specific embodiments, but it is understood in the art that various modifications and changes are possible without departing from the spirit and scope of the invention as indicated by the claims. Anyone who has it will know it easily.

Claims (4)

A first agent comprising 29% by weight of henna leaf powder, 25% by weight of indigofera leaf powder, 10% by weight of green tea leaf extract, 19% by weight of iris root extract and 17% by weight of mung bean powder;
A second agent comprising 60 to 75% by weight of a low molecular weight fish collagen peptide, 5 to 10% by weight of a vitamin C powder, 4% by weight of a beta-carotene powder, 1 to 5% by weight of a pomegranate extract, and 11% by weight of a soybean extract;
1000ppm of squalene oil 3% by weight, olive oil 60-70% by weight, Ulkenia amoeboiide oil 0.1-2% by weight, linseed oil 0.1-2% by weight, argan tree kernel oil 0.1-2% by weight, sunflower seed oil 0.1-2% by weight, 0.1-2% by weight of grape seed oil, 0.1-2% by weight of jojoba seed oil, 0.2-2% by weight of tocopheryl acetate, a first spray comprising a trace amount of purified water and a small amount of fragrance;
Hydrolyzed collagen 1.2% by weight, nonoxynol-12 1.1% by weight, arginine 1.1% by weight, phytosphingosine 0.01 ~ 5% by weight, hydrogenated lecithin 1.2-1.8% by weight, methylchloroisothiazoli 0.05% by weight of rice paddy, 0.05% by weight of methyl isothiazolinone, 1.2% by weight of PEG-75 lanolin, 2.8 to 3.6% by weight of hydrolyzed keratin, 1 to 10% by weight of panthenol, 2% by weight of ceramide enpy and the balance of purified water A second spray comprising; And
Green tea diluted with 96.6% by weight of purified water and 3.4% by weight of green tea powder; Each composition,
After mixing the first agent, the second agent and the green tea and applying it to the hair, the first and second spray agents are sprayed onto the hair, and the hair dye composition comprising a green tea extract.
The method of claim 1, wherein the electrolyzed acidic or alkaline deep ocean water is applied to the hair, 0.3 to 0.5 compared to the total weight ratio of the first agent, the second agent and green tea, the first spray agent and the second spray agent. Hair dye composition comprising a green tea extract, consisting of a weight ratio.
The hair dye composition of claim 2, wherein the deep ocean water is applied to fill the hairy insect material in the hair.
The hair dye composition of claim 1, wherein the egg yolk is further blended with the first agent, and the egg yolk is further blended with 50 parts by weight based on the total weight ratio of the first agent.

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